CA1114187A - Process for producing coated seed - Google Patents

Process for producing coated seed

Info

Publication number
CA1114187A
CA1114187A CA330,265A CA330265A CA1114187A CA 1114187 A CA1114187 A CA 1114187A CA 330265 A CA330265 A CA 330265A CA 1114187 A CA1114187 A CA 1114187A
Authority
CA
Canada
Prior art keywords
coating
water
soluble binder
coating powder
seed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA330,265A
Other languages
French (fr)
Inventor
Shuji Kitamura
Michihiro Nakayama
Masashi Watanabe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Application granted granted Critical
Publication of CA1114187A publication Critical patent/CA1114187A/en
Expired legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S47/00Plant husbandry
    • Y10S47/09Physical and chemical treatment of seeds for planting

Abstract

ABSTRACT OF THE DISCLOSURE

The present invention provides coated seeds, the coating of which has sufficient hardness for machine-seeding and adequate disintegration characteristics in soil. Each coated seed comprises a process for producing a coated seed, which comprises mixing a coating powder with an aqueous solution of a water-soluble binder, drying the resulting mixture, powdering the mixture, and then coating a seed using the resulting surface-treated coating powder, wherein the amount of the water-soluble binder is 0.1 to 20% by weight based on the weight of the coating powder.

Description

1 The present invention relates to the prepara-tion of coated seeds. Hitherto, increasing the bulk of seeds by coating them with an inorganic substance has been carried out for the ease of mechanical sowing ;~
and handling, and for the long~term storage. Specifically, there have been employed processes in which seeds are coated, on a coating machine, with a powder material (e.g. diatomaceous earth, calcium carbonate, talc, silica, ~aolin-clay, zeolite, bentonite, vermiculite) through a water-soluble binder [e.g. starch, polyvinyl alcohol (PVA), carboxymethyl cellulose (CMC), methyl cellulose (MC), gelatin].
When such well-~nown processes are, however, applied to the coating of fine seeds such as flower - 15 seeds, it is common that coated seeds having not only nonuniform particle size but also soft coating layer are only obtained. Consequently, there are troubles such as breaking of coating layers on mechanical sowing, automatlc filling or transportation.
Further, coated seeds should be easy to disintegrate by mois~ure in soil.
As a result of extensive study to solve the foregoing problems, the inventors found that coated seeds having a narrow particle size distribution and moderate hardness can be produced by coating seeds . , .

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With a coating powder previousl~ surface-treated with a water-soluble binder.

The present invention provides a process for producing -a coated seed,which comprises mixing a coating powder with an aqueous solution of water-soluble binder, drying the resulting mixture, powdering the mixture, and then coating a seed using the resulting surface-treated coating powder, wherein the amount of thewater-soluble binder is 0.1 to 20~ by weight based on the weight of the coating powder.

The present invention also provides a coated seed com-prising a seed and a coating thereon of a coating powder, said coating powder having been previously treated by mixing the powder with an aqueous solution of a water-soluble binder, drying the resulting mixture and powdering the mixture, said resulting treated coating powder being bonded by a water-solu- ;
ble binder to said seed to form a coating thereon, wherein the amount of the water-soluble binder is 0.1 to 20% by weight 20 based on the weight of the coating powder.

The water-soluble binders used in the present invention include starch, PVA, CMC, MC, gelatin, pullulan and the like. The amount of the binder usecl is 0.1 to 20% by weight, 25 preferably 0.5 to 5% by weight, based on the weight of the ~;
coating powder.

The coating powders used in the presentinvent-on in-clude, for example, diatomaceous earth, aluminum hydroxide, `~
calcium hydroxide, magnesium hydroxide, barium hydroxide, cal-cium sulfate, calcium sulfite, basic magnesium carbonate, kaolin-clay, dolomite, talc, zeolite, illite, halloysite, bentonite, vermiculite, microlite, peat moss and the like. ``
These powders may be used alone or in combination. Of these, diatomaceous earth, kaolin-clay, dolomite, talc and bentonite are particularly preferred. The mean particle size of these ;':
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powders is preferably 10 ~ or less, particularly preferably 1 ~ or less.

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1 As is well-known to the skilled in the art, additives such as growth hormone compounds, fungicides and colouring agents may be added to these powders.
In carrying out the process of the present -invention, for example, an aqueous solution of the water-soluble binder is mixed thoroughly with the coating powder, and the mixture is dried by heating to obtain a solid substance. The concentration of the aqueous solution is not particularly limited, but generally it is preferably 0.1 to 10% by weight. The solid substance obtained is powdered to a mean particle size of preferably 10 ~ or less, particularly preferably 1 ~ or less, and then used for coating seeds. In carrying out this surface treatment on an industrial scaie, methods of treating a slurry comprising the powder, binder and water by a spray-drier, or methods using a Henschel mlxer or kneader are properly selected.
In order to display the characteristics of the present invention suf~iciently, the surface of the coating powder is uniformly treated with the water-soluble binder. For this purpose, the concentration and amount of the aqueous solution of the water-soluble -~ -binder are properly varied depending upon the particle ~
size, surface state and shape of the coating powder. -The coating powder thus sur~ace-treated is applied to the coating of seeds by the usual ways. ;`
The coating machines used in the present invention include for example sugar coating machines, centrifugal ~,.

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1 fluidizing coating machines, fluidized bed coating machines and the like.
Of course, the process of the present invention may also be applied to the coating of seeds of different shapes.
The coated seeds obtained by the present invention have the following characteristics: (1) They are easy in handling and helpful in saving the amount of seeds by mechanical sowing, shortening sowing time 10 and saving labour for thinning; (2) the shell life of ~
the coated seeds can be prolonged by properly controlling ;
the moisture content and the thickness of the coating layer; (3) coated seeds having a higher surface hardness can be obtained with less amount of the water-soluble binder because the binder displays a larger effect than in the conventional coating processes; (4) and the coating layer easily disintegrates after sowing by the action of moisture in soiI with no effect on germination and growth like in the sowing of uncoated seeds.
The present invention will be illustrated in more detail with reference to the following e~amples, which are only given for the purpose of illustration and not to be interpreted as limiting the invention thereto.
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Example 1 -~ (1) Surface treatment of diatomaceous earth ;
Diatomaceous earth (250 8) and an aqueous -- , :
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1 solution (250 cc) co~taining 2% by weight of CMC (Cellogen ~ a~h?a~k ~
6A, ~ ee~ Daiichi Kogyo Seiyaku Co.) were together kneaded into paste. The paste was then dried at 105C
for 3 hours in a hot-air drier, powdered to a mean particle size of 5 ~ by a pulverizer to obtain a coating material of the surface-treated diatomaceous earth.
(2) Coating The seeds of petunia (6 g) were placed in a sugar-coating pan and tumbled with the above surface- ~ -10 treated diatomaceous earth (250 g) by the alternate ;
addition of the diatomaceous earth, while an aqueous solution (250 cc) containing 1% by weight of CMC was sprayed thereto (spraying pressure, 0.5 kg/cm2; spray nozzle, 0.2 mm~). The tumbling was stopped when the size of the seeds reached about 3 times as large as the initial size. The coated seeds were withdrawn ;
from the pan and dried at 35C for 15 hours in a hot-air drier to obtain a product. The results obtained are shown in Table 1.
~` '':
20 Example 2 ~ -(1) Surface treatment of kaolin-clay Kaolin-clay (250 g) and an aqueous solution (250 cc) containing 1.% by weight of pullulan (mean molecular weight, 100,000) were together kneaded into paste. ;
The paste was then dried at 105C for 3 hours in a hot-air drier, powdered to a mean particle size of 5 by a pulverizer to obtain a coating material of the ~: .
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1 surface-treated kaolin-clay.
(2) Coating The seeds of petunia (6 g) were placed in a sugar-coating pan and tumbled with the above sur~ace-treated kaolin clay (250 g) by the alternate additionof the kaoIin-clay, while an aqueous solution (250 cc) containing 1% by weight of pullulan was sprayed thereto (spraying pressure, o.4 kg/cm2; spray nozzle, 0.2 mm~).
The tumbling was stopped when the size of seeds reached ;~
about 3 times as large as the initial size. The coated seeds were withdrawn from the pan and dried at 35C
for 15 hours in a hot-air drier to obtain a product.
The results obtained are shown in Table 1.

Comparative example 1 Coating was carried out in the same manner as in Example 1 except that the seeds were coated with untreated diatomaceous earth (250 g) while spraying -an aqueous solution (250 cc) containing 3% by weight of CMC (Cellogen 6 A, produced by Daiichi Kogyo Seiyaku Co.) (spraying pressure, 0.7 kg/cm2; spray nozzle, 0.2 mm~). The results obtalned are shown in Table 1.

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Comparative example 2 Coating was carried out in the same manner as in Example 1 except that the seeds were coated with ~
25 untreated diatomaceous earth (250 g) while spraying ~ -an aqueous solution (250 cc) containing 5% by weight " ., ~ .

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1 of CMC (Cellogen 6 A, produced by Daiichi Kogyo Seiyaku Co.) (spraying pressure, 1.0 kg/cm2; spray nozzle, 0.2 mm~). The results obtained are shown in Table 1.

Comparative example 3 Coating was carried out in the same manner as in Example 2 except that the seeds were coated with untreated kaolin-clay (250 g) while spraying an aqueous solution (250 cc) containing 2% by weight of pullulan (mean molecular weight, 100,000) (spraying pressure, 0.5 kg/cm2; spray nozzle, 0.2 mm~). The results obtained are shown in Table 1. ~-Comparative example 4 ~.
Coating was carried out in the same manner as in Example 2 except that the seeds were coated with untreated kaolin-clay (250 g) while spraying an aqueous solution (250 cc) containing 4% by weight of pullulan -(mean molecular weight, 100,000) (spraying pressure, o.6 kg/cm2; spray nozzle, 0.2 mm~). The results obtained are shown in Table 1.
The coated petunia seeds obtained by the present invention were very good in germination with the same rate of germination as in uncoated petunia seeds.
Also, difference in growth was not observed.

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Claims (9)

THE EMBODIMENTS OF THE INVENTION IN WHICH AN EXCLUSIVE
PROPERTY OR PRIVILEGE IS CLAIMED ARE DEFINED AS FOLLOWS:
1. A process for producing a coated seed, which comprises mixing a coating powder with an aqueous solution of a water-soluble binder, drying the resulting mixture, pow-dering the mixture, and then coating a seed using the re-sulting surface-treated coating powder, wherein the amount of the water-soluble binder is 0.1 to 20% by weight based on the weight of the coating powder.
2. A process according to claim 1, wherein the coating powder is one member selected from diatomaceous earth, aluminum hydroxide, calcium hydroxide, mangesium hydroxide, barium hydroxide, calcium sulfate, calcium sulfite, basic magnesium carbonate, kaolin-clay, dolomite, talc, zeolite, illite, hall-oysite, bentonite, vermiculite, microlite and peat moss.
3. A process according to claim 1, wherein the water-soluble binder is one member selected from starch, polyvinyl alcohol, carboxymethyl cellulose, methyl cellulose, gelatin and pullulan.
4. A process according to claim 1, wherein the aqueous solution of the water-soluble binder is in a concentration of 0.1 to 10% by weight.
5. A process according to claim 1, wherein the pow-dering is carried out so as to make a mean particle size of the mixture 10 ~ or less.
6. A process according to claim 1, wherein the coating is carried out using a water-soluble binder.
7. A coated seed comprising a seed and a coating there-on of a coating powder, said coating powder having been pre-viously treated by mixing the powder with an aqueous solution of a water-soluble binder, drying the resulting mixture and powdering the mixture, said resulting treated coating powder being bonded by a water-soluble binder to said seed to form a coating thereon, wherein the amount of the water-soluble binder is 0.1 to 20% by weight based on the weight of the coating powder.
8. A coated seed according to claim 7, wherein the coating powder is one member selected from diatomaceous earth, aluminum hydroxide, calcium hydroxide, magnesium hydroxide, barium hydroxide, calcium sulfate, calcium sulfite, basic mag-nesium carbonate, kaolin-clay, dolomite, talc, zeolite, illite, halloysite, bentonite, vermiculite, microcite and peat moss.
9. A coated seed according to claim 7, wherein the water-soluble binder is one member selected from starch, polyvinyl alcohol, carboxymethyl cellulose, methyl cellulose, gelatin and pullulan.
CA330,265A 1978-07-12 1979-06-21 Process for producing coated seed Expired CA1114187A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP8539178A JPS5521705A (en) 1978-07-12 1978-07-12 Preparation of coated seed
JP85391/78 1978-07-12

Publications (1)

Publication Number Publication Date
CA1114187A true CA1114187A (en) 1981-12-15

Family

ID=13857451

Family Applications (1)

Application Number Title Priority Date Filing Date
CA330,265A Expired CA1114187A (en) 1978-07-12 1979-06-21 Process for producing coated seed

Country Status (8)

Country Link
US (1) US4250660A (en)
JP (1) JPS5521705A (en)
CA (1) CA1114187A (en)
DE (1) DE2928064A1 (en)
FR (1) FR2430713A1 (en)
GB (1) GB2025200B (en)
NL (1) NL7905071A (en)
SE (1) SE446807B (en)

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Also Published As

Publication number Publication date
SE446807B (en) 1986-10-13
JPS5521705A (en) 1980-02-16
NL7905071A (en) 1980-01-15
JPS5653323B2 (en) 1981-12-18
SE7906049L (en) 1980-01-13
GB2025200B (en) 1982-10-27
FR2430713B1 (en) 1983-05-20
FR2430713A1 (en) 1980-02-08
US4250660A (en) 1981-02-17
GB2025200A (en) 1980-01-23
DE2928064A1 (en) 1980-01-24

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