CA2247259A1 - Catalyst testing process and apparatus - Google Patents
Catalyst testing process and apparatusInfo
- Publication number
- CA2247259A1 CA2247259A1 CA002247259A CA2247259A CA2247259A1 CA 2247259 A1 CA2247259 A1 CA 2247259A1 CA 002247259 A CA002247259 A CA 002247259A CA 2247259 A CA2247259 A CA 2247259A CA 2247259 A1 CA2247259 A1 CA 2247259A1
- Authority
- CA
- Canada
- Prior art keywords
- pellets
- spots
- cells
- treated
- reactants
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/10—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using catalysis
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00281—Individual reactor vessels
- B01J2219/00286—Reactor vessels with top and bottom openings
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00306—Reactor vessels in a multiple arrangement
- B01J2219/00313—Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks
- B01J2219/00315—Microtiter plates
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00351—Means for dispensing and evacuation of reagents
- B01J2219/00364—Pipettes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00497—Features relating to the solid phase supports
- B01J2219/00527—Sheets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00585—Parallel processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00596—Solid-phase processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00603—Making arrays on substantially continuous surfaces
- B01J2219/00659—Two-dimensional arrays
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/0068—Means for controlling the apparatus of the process
- B01J2219/00686—Automatic
- B01J2219/00691—Automatic using robots
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/0068—Means for controlling the apparatus of the process
- B01J2219/00702—Processes involving means for analysing and characterising the products
- B01J2219/00704—Processes involving means for analysing and characterising the products integrated with the reactor apparatus
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
- B01J2219/00747—Catalysts
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- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B30/00—Methods of screening libraries
- C40B30/08—Methods of screening libraries by measuring catalytic activity
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- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B40/00—Libraries per se, e.g. arrays, mixtures
- C40B40/18—Libraries containing only inorganic compounds or inorganic materials
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/21—Hydrocarbon
- Y10T436/214—Acyclic [e.g., methane, octane, isoparaffin, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/24—Nuclear magnetic resonance, electron spin resonance or other spin effects or mass spectrometry
Abstract
A multicell holder (10) e.g. a honeycomb or plate, or a collection of individual support particles, is treated with solutions/suspensions of catalyst ingredients to produce a plurality of cells, spots, or pellets (12) each having a different composition. The plurality of cells, spots, or pellets are dried, calcined or treated to stabilize the ingredients and contacted with a potentially reactive feed stream or batch of reactants. The reaction occurring in each cell (12) is measured or analyzed to determine the relative efficacy of the catalysts in each combination. The measurement or analysis is done through a number of different methods including infrared thermography (14), spectroscopy of products or residual reactants or sampling for further analysis.
Robotic techniques can be employed in producing the cells, spots or pellets (12).
Robotic techniques can be employed in producing the cells, spots or pellets (12).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CA002465957A CA2465957A1 (en) | 1996-02-28 | 1997-02-25 | Catalyst testing process and apparatus |
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US1245796P | 1996-02-28 | 1996-02-28 | |
US60/012,457 | 1996-06-17 | ||
US08/664,836 US6063633A (en) | 1996-02-28 | 1996-06-17 | Catalyst testing process and apparatus |
US08/664,836 | 1996-06-17 | ||
PCT/US1997/002756 WO1997032208A1 (en) | 1996-02-28 | 1997-02-25 | Catalyst testing process and apparatus |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002465957A Division CA2465957A1 (en) | 1996-02-28 | 1997-02-25 | Catalyst testing process and apparatus |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2247259A1 true CA2247259A1 (en) | 1997-09-04 |
CA2247259C CA2247259C (en) | 2004-08-31 |
Family
ID=26683580
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA002247259A Expired - Fee Related CA2247259C (en) | 1996-02-28 | 1997-02-25 | Catalyst testing process and apparatus |
Country Status (8)
Country | Link |
---|---|
US (11) | US6063633A (en) |
EP (1) | EP0883806B2 (en) |
JP (1) | JP2000506265A (en) |
CN (1) | CN100430725C (en) |
AU (1) | AU1967997A (en) |
CA (1) | CA2247259C (en) |
DE (1) | DE69725429T3 (en) |
WO (1) | WO1997032208A1 (en) |
Families Citing this family (201)
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US6030917A (en) | 1996-07-23 | 2000-02-29 | Symyx Technologies, Inc. | Combinatorial synthesis and analysis of organometallic compounds and catalysts |
US6419881B1 (en) | 1994-10-18 | 2002-07-16 | Symyx Technologies, Inc. | Combinatorial arrays of organometallic compounds and catalysts |
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US5985356A (en) | 1994-10-18 | 1999-11-16 | The Regents Of The University Of California | Combinatorial synthesis of novel materials |
US6063633A (en) * | 1996-02-28 | 2000-05-16 | The University Of Houston | Catalyst testing process and apparatus |
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-
1997
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- 1997-02-25 EP EP97907768A patent/EP0883806B2/en not_active Expired - Lifetime
- 1997-02-25 CA CA002247259A patent/CA2247259C/en not_active Expired - Fee Related
- 1997-02-25 JP JP9531028A patent/JP2000506265A/en not_active Ceased
- 1997-02-25 WO PCT/US1997/002756 patent/WO1997032208A1/en active IP Right Grant
- 1997-02-25 CN CNB971920168A patent/CN100430725C/en not_active Expired - Fee Related
- 1997-02-25 AU AU19679/97A patent/AU1967997A/en not_active Abandoned
-
2000
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- 2000-07-10 US US09/613,879 patent/US6630111B1/en not_active Expired - Lifetime
- 2000-07-10 US US09/613,082 patent/US6623969B1/en not_active Expired - Lifetime
- 2000-07-10 US US09/613,084 patent/US6605470B1/en not_active Expired - Lifetime
- 2000-07-10 US US09/613,877 patent/US6623970B1/en not_active Expired - Lifetime
- 2000-07-10 US US09/612,857 patent/US6623968B1/en not_active Expired - Lifetime
- 2000-07-10 US US09/612,853 patent/US6623967B1/en not_active Expired - Lifetime
- 2000-11-28 US US09/727,890 patent/US6514764B1/en not_active Expired - Lifetime
-
2001
- 2001-12-21 US US10/029,891 patent/US6908768B2/en not_active Expired - Fee Related
-
2005
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DE69725429T3 (en) | 2011-06-30 |
EP0883806A4 (en) | 2001-09-12 |
US6605470B1 (en) | 2003-08-12 |
US6623969B1 (en) | 2003-09-23 |
US6630111B1 (en) | 2003-10-07 |
US6908768B2 (en) | 2005-06-21 |
US6623968B1 (en) | 2003-09-23 |
CN100430725C (en) | 2008-11-05 |
US6514764B1 (en) | 2003-02-04 |
EP0883806B1 (en) | 2003-10-08 |
US6333196B1 (en) | 2001-12-25 |
DE69725429T2 (en) | 2004-05-19 |
US6623970B1 (en) | 2003-09-23 |
EP0883806A1 (en) | 1998-12-16 |
CA2247259C (en) | 2004-08-31 |
US20020127725A1 (en) | 2002-09-12 |
CN1226966A (en) | 1999-08-25 |
WO1997032208A1 (en) | 1997-09-04 |
EP0883806B2 (en) | 2010-11-24 |
JP2000506265A (en) | 2000-05-23 |
DE69725429D1 (en) | 2003-11-13 |
US20050158865A1 (en) | 2005-07-21 |
AU1967997A (en) | 1997-09-16 |
US6623967B1 (en) | 2003-09-23 |
US6063633A (en) | 2000-05-16 |
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