CA2407191C - A gravity separator for multi-phase effluents - Google Patents
A gravity separator for multi-phase effluents Download PDFInfo
- Publication number
- CA2407191C CA2407191C CA2407191A CA2407191A CA2407191C CA 2407191 C CA2407191 C CA 2407191C CA 2407191 A CA2407191 A CA 2407191A CA 2407191 A CA2407191 A CA 2407191A CA 2407191 C CA2407191 C CA 2407191C
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- Prior art keywords
- separator
- phase
- effluent
- supernatant
- weir plate
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0211—Separation of non-miscible liquids by sedimentation with baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
Abstract
The invention relates to a gravity separator for an effluent made up of a multi-phase fluid mixture comprising at least a heavy first phase and a supernatant second phase. According to the invention, said separator includes adjustment means for adjusting its geometrical separation characteristics.
Description
A GRAVITY SEPARATOR FOR MULTI-PHASE EFFLUENTS
The invention relates to a gravity separator for mufti-phase effluents. A preferred application of the invention relates to a separator for effluent from an oil well, said effluent typically comprising three phases: ari aqueous phase, a liquid hydrocarbon phase, and a gaseous hydrocarbon phase.
After a hydrocarbon well has been drilled and made safe, production is started from the well for a relatively short time in order to identify clearly the types and magnitudes of its various components, and in order to estimate the production capacities of the well.
These tests, commonly referred to as "well testing", use means for separating out the various phases of the effluent (water, oil, and gas). Since the various phases are of different densities, separation takes place continuously in a vertical separator, in which the phases settle out. Downstream from the separator, the aqueous phase is discharged, optionally after undergoing additionalpurific.ation, and the hydrocarbons are~burnt off .
At the beginning of the testing step, the composition of the effluent varies enormously. Insofar as the well is initially filled with aqueous residues from the drilling fluid and from the completion fluid, the effluent that is collected is essentially made up of water. Then, gradually, the percentage of aqueous residue decreases, and the composition of the effluent becomes enriched with oil and with gas.
Since state-of-the-art separators are dimensioned to treat effluents whose phase ratio remains substantially stable over time, it is not possible to use them for the effluent at the beginning of the testing step.
Therefore, ways are sought to dispose of the effluent directly.
For that purpose, a first solution is known that consists in sending the effluent directly to burners without any separation step being performed.
Unfortunately, the burners known from the state of the art are effective only for mixtures in which the hydrocarbon content is at least 70o to 80%. As a result;
when the effluent is sent directly to such burners, the environment is polluted to a relatively large extent because of unburnt hydrocarbons. That solution poses serious pollution problems and is thus unacceptable.
Another known solution consists in recovering the effluent and in storing it temporarily in containers, until the oil that it contains separates from the aqueous phase and floats on the surface of it in said containers.
The oil phase is then recovered, and it is sent to the burners while the resulting cleaned aqueous phase is disposed of. Although that method gives rise to lower risks for the environment, it requires the site to be equipped with separators and additional pipes, constituting costly and voluminous equipment.
Another method consists in building an independent installation for treating effluent when its multi-phase ratio is not stable. Although that method is ecologically very satisfactory, it increases problems related to the cost of treatment installations and to the space they take up. Logistics problems are then particularly numerous. .
An object of the invention is to solve the problem of pollution related to treating an effluent whose multi-phase ratio varies over time, without it being necessary to collect waste which must then be treated subsequently.
To this end, the invention provides a gravity separator for an effluent made up of a multi-phase fluid mixture comprising at least a heavy first phase and a supernatant second phase, said separator including adjustment means for adjusting its geometrical separation characteristics.
By adjusting its geometrical separation characteristics, it is possible to treat effluent whose phase ratio is not~constant over time. As a result, when used for effluent from an oil well, the separator of the invention makes it possible to treat said effluent throughout the period during which the ratios of the three phases, namely water, oil, and gas, are not stabilized.
It is thus possible to treat the effluent in the separator regardless of how the volume ratios of the various phases fluctuate as a function of time. Insofar as the separator of the.,inv'ention is followed by a burner, the burner~receives a mixture whose hydrocarbon content makes, it possible to burn off the hydrocarbons without any discha~ge,that is harmful to the environment, and a cleaned aqueous phase ,is recovered without an additional separator being necessary.
The separator of the invention thus makes it possible to preserve-the environment without it being necessary tocollec~'waste that must then be treated by an auxiliary~;installation:
' In an . ad.vai~.tageous:embodiment of the invention, ~ the adjustmentmeans ~ for 'adjusting its geometrical separation characterist'lcs, make it possible to .give preference to separating out"certain.phases of the effluent , taken on their own or-in combination.
This makes ~.t,,possible to act on the separation characterist~ics~in order to give preference to the retention time of one phase in particular, depending on whether a higher level of purity is desired on one or other of the phases. This is particularly advantageous if very Clean'water;is,to be obtained, so that, for example, it is possible .to discharge said water directly without polluting the environment.
The invention will be well understood on reading the following description given with reference to the -. 35 accompanying.drawings. The list of accompanying drawings is as follows : . ' Figure 1 is a view of an embodiment of a separator of the invention;
Figure 2 is a cross-section view of said separator;
Figure 3 is a view of another embodiment of a separator of the invention;
Figure 4 is a view of another embodiment of a separator of the invention;
Figure 5a is a section view of a detail of an embodiment of a separator of the invention;
Figure 5b is a perspective view of the same detail;
Figure 6 is a view of a detail of another embodiment of a separator of the invention; and Figure 7 is an example of a drive device associated with an embodiment of a separator of the invention.
The separator of the invention makes it possible to treat effluent whose characteristics are as follows:
- At the beginning of the transitional stage, the effluent contains a very small proportion of gaseous hydrocarbons. The majority of the separator must 20. therefore be dedicated to separating the liquid-liquid phase, while the space left for the gas~phase can be minimized. In addition, most of the liquid-liquid phase is itself made up essentially of water, very little oil being supernatant on.said phase.
- At the end of the transitional stage and during the separation stage, the effluent is made up mostly of oil and of gas. In contrast, the percentage of water in the effluent is reduced considerably. It is thus necessary to maximize the space available in the separator~for the oil phase. and then for the gas phase.
Figure 1 shows an embodiment of a separator 1 of the invention, in which the phases settle out by gravity. By way of example, this separator 1 is substantially cylindrical in shape, and is the size of a tank that can be transported by truck. When treating effluent from an oil well, it must be possible to move the separator from site to site, and it thus necessary to have a separator of limited size.
As is known and not shown, a solids separator followed by a heat exchanger, and a burner are disposed respectively upstream and downstream from said separator 1.
In the embodiment shown in Figure 1, the separator 1 is provided with a separation or "weir" plate 5 whose height is adjustable as a function of the composition of the effluent. The weir plate 5 defines a first compartment for a heavy first phase, namely water, and a second compartment fed by overflow with the lower-density oil phase that floats on the aqueous phase. The weir plate 5 is made up of a support 5a and of various telescopic leaves 5b which can be deployed vertically towards the top of the separator 1.
As shown in Figure 2, the outlines of the support 5a.
follow the inside walls of the substantially-cylindrical separator 1. The moving leaves 5b are of substantially rectangular shape, and they are carried bythe support 5a. The shape of the support 5a and the dimensions of the rectangular leaves 5b are complementary so as to occupy the entire width of the separator 1. In this way, the weir plate assembly 5 constitutes a genuinely fluid-tight obstacle over a certain height, inside the separator 1.
The leaves 5b can thus be deployed gradually so as to form a weir plate of variable height. As a result, the further the telescopic weir plate 5 is deployed, the higher the maximum possible level of water and the longer the retention time for which the effluent is retained in the separator.
The leaves 5a of the telescopic weir plate 5 are in contact with one another. Whenever it is necessary to increase the height of the weir plate 5 slightly, the first leaf is deployed and is placed in vertical alignment with the other leaves. As a function of the desired height of the weir plate, the leaves 5b are successively deployed and each new leaf vertically increments the leaf most recently put in place.
In the low position, all of the leaves 5b are retracted inside the support 5a from which they do not project. In the embodiment shown, taking account of the overall size of the support and of the leaves, the nominal height of the weir plate, with all leaves retracted, represents substantially 30% of the height of the separator.
In the same embodiment, and in the high position, once all of the leaves 5b have been deployed, the height of the weir plate 5 represents substantially 650 of the total height of the separator 1. Provision is made for said leaves 5b to overlap so as to guarantee that suitable sealing is provided between all of the leaves without hindering the displacement of said leaves relative to one another..
The separator 1 is provided with three outlet ducts.
The water .phase .anal the oil phase are recovered respectively via the ducts 2 and 3 placed at the bottom of the separator. The gaseous phase is recovered via a duct 4 which, by way of example, conveys the gases to a burner (not shown). By way of example, the burner is a flare.
The first removal duct 2 for removing the aqueous phase is connected to an aqueous phase recovery duct 1a which is situated in the bottom portion of the separator 1, upstream from the weir plate 5. A
turbidimeter (not shown) makes it possible to determine the percentage of oil in the discharged water at the outlet of the separator 1. In one embodiment, the water is then sent via the duct 2 to an additional re-treatment unit that is not shown and that is known from the state of the art.
The second removal duct 3 for removing the oil phase is connected to an oil recovery duct 1b which is also situated at the bottom portion of the separator 1. A
sensor on the removal duct 3 makes it possible to determine the percentage of water in the oil leaving the separator 1.
It is possible to regulate the flow rate of the water sent to the removal duct 2 so that the level of the liquid phases does not exceed the height of the telescopic weir plate 5. Similarly, the flow rate of oil sent to the burner is regulated so that, inside the separator, said oil can always flow away by flowing over the telescopic weir plate 5.
Typically, at the start of the transitional stage, since the percentage of water in the effluent is particularly high, the weir plate 5 is at its maximum height. This, together with the regulation of the flow rate of water leaving the separator guarantees maximum water retention time and therefore particularly effective . separation of the water and oil phases.
Thereafter, the percentage of water in the effluent decreases, while the percentage of oil therein increases.
Thus, the capacity of the compartment dedicated to water, i.e. the height of the telescopic weir plate 5, is gradually reduced.
The separator 1 of the invention thus makes it possible to respond to changes in the composition of the effluent, such as those indicated above, The separation characteristics of the separator can be adjusted as a function of the composition of the effluent. Thus, regardless of how the volume ratios of the various phases of the effluent vary as a function of time, the separator adapts itself continuously to match said ratios so as to separate said phases.
With the separator of the invention, it is possible to treat a petroleum effluent during the transitional stage when the ratios of the oil, water, and gas phases have not yet become stable. As a result, the separator of the invention makes it possible to treat effluent continuously, as soon as it leaves the well, without giving rise to environrriental pollution or to waste that needs to be,treated separately.
Figure 3 shows another embodiment of a separator of.
the invention. In this embodiment, the separator 1 does-not include a telescopic weir plate 5, since the separation is not performed by causing the oil phase to flow over said weir plate 5. Both the water phase and the oil phase sari thus extend over the entire length of the separator 1.. This solution makes it possible to increase the water retention capacity of the separator 1.
The~recovery,duct 1a for recovering the aqueous phase is situated'.atlth.e bottom portion of the separator 1, substantially~at.its~end remote from the inlet duct via which the effluent is fed into said separator. 4In this way, said recovery.duct 1a is situated in a zone in which the two liquidwphases of the effluent are well separated.'-.The removal.duct,2 for.removing he aqueous ' phase is'connected,to.~said recovery duct.la. In order to avoid~~any turbulence,:.~which would hinder separation.of the. liquid phases;,.~a~rhaffle .lc can'be=placed immediately'' above the water recovery. duct, la, for example.
The removal.duct.3 for removing the hydrocarbon phase is also situated at the bottom portion of the separator 1 - ~.
A ~ecove~ry duct. 1b ~is connected to said removal duct 3. The recovery duct lb is made up of a telescopic tube comprising coaxial cylinders that are capable of moving progressively'relative to one another in a vertical direction~:inside the separator 1.
The recovery duct 1b is terminated by a suction intake or~"collector" 6~ embodiments of which are shown in more detail in Figures 5a, 5b, and 6. The recovery duct 1b is then deployed to an extent that can be caused w 35 to vary in order to~position the~collector 6 in the middle of the.oil~.phase regardless of the mufti-phase ratio of the effluent. During the transitional stage, the duct 1b is thus extended to its maximum extent so as to place the collector 6 high in the separator, in the oil phase, and so as to maximize the volume of the separator that is available for the aqueous phase. Then, as a function of the variation in the composition of the effluent, the recovery duct 1b is gradually lowered.
The position of the collector 6 is adjusted so that the percentage of water in the oil phase at the outlet of the separator does not exceed 30%. This is to guarantee that the burners at the outlet of the separator operate effectively, and thus to prevent any discharge of unburnt hydrocarbons into the environment.
Figure 4 shows a preferred embodiment of.a separator of the invention.
In this embodiment, the recovery duct 1b for recovering the oil is~constituted by a bellows of substantially cylindrical shape and made of flexible materials such as plastics materials. In the embodiment shown and for reasons of compactness, related to the materials of the bellows lb,.the nominal height of the bellows corresponds substantially to 30% of.the height of the separator l, whereas, once it is totally expanded, the bellows 1b has a height representing substantially 65% of the height of said separator 1.
A suction intake or "collector" 6 as shown in any one of Figures 5a, 5b, and 6 is situated at the end portion of the bellows 1b.
The use of a flexible bellows offers numerous advantages: it is a light-weight and low-cost system that, in addition, does not suffer from the sealing and sliding problems encountered with a telescopic deployment system. Advantageously, a guide device is provided that is constituted, for example, by four guide stakes.
As described above for the telescopic recovery duct, the bellows 1b is allowed to expand to various extents as a function of the mufti-phase ratio of the effluent, so that the collector 6 is always positioned in the middle of the oil phase. During the transitional stage, the bellows 1b is thus at its maximum height, leaving the maximum possible volume available for the aqueous phase.
Then, while the effluent is varying, the height of said bellows 1b is adjusted so as to recover oil whose water content is compatible with good burner efficiency at the burners at the outlet of the separator, i.e. a water content that does not exceed 30% in the oil phase.
Figures 5a and 5b show a first embodiment of a collector 6 in separators of the invention. This collector is made up mainly of a cover 6a overlying a collar 6b. In this way, the oil is sucked in radially through the empty space between the cover 6a and the collar 6b. This particular geometrical shape makes it possible to reduce turbulence on taking oil into the recovery duct 1b, thereby avoiding the risks of water or gas being sucked in, and the risks of a vortex being generated.
The space between the two portions 6a and 6b i.s small enough to make it easy to position the collector 6~
at the "cleanest" level in the oil phase, so as to recover the oil without running the above-mentioned risks.
Figure 6 shows another embodiment of a collector 6.
This collector is substantially in the form of a cylinder supporting a duck bill opening. Suction takes place radially, and the collector 6 can be positioned angularly so as to situate it as well as possible in the supernatant oil phase.
The position of the collector 6 in the oil phase can be adjusted at any time during the separation process.
For example, the collector 6 is firstly positioned in the middle of the oil phase. Then, secondly, the position is re-adjusted. For this purpose, in order to take account of the thickness of the collector 6, the decision is taken to place said collector in the oil phase in a zone ranging from 5% above the interface between the two l0 liquids to 5o below the level of the liquid. This makes it possible to maintain a water percentage of less than 30o in the oil at the outlet of the separator, which percentage is compatible with state-of-the-art burners. ..
The position of the collector is re-adjusted as a function of variation in measurements made at the outlet of the separator.
Figure 7 shows an actuator device for actuating the various above-described systems. This device makes it possible to drive the recovery duct 1b, be it in the form of a bellows, in the form of a telescopic tube, or in the form of a telescopic weir plate 5.
As shown in Figure 7, the actuator device is made up of pneumatic, hydraulic, or electrical actuator means 8 connected via a stepdown gearbox 10 to a worm screw 11 situated inside the separator 1. The worm screw 11 serves to drive a threaded rod 12 which (as shown in Figure 7) is itself connected to the collector 6 or to the first weir leaf 5b.
In another embodiment, the drive means of the actuator device are situated outside the separator and are connected tee a drive device constituted by a lever arm connected to the recovery duct 1b (i.e. the bellows or the cylinders of the telescopic tube) or to the weir leaves 5b. The drive device then has means for gearing down the movement in translation.
The separator of the invention thus makes it possible to adapt the geometrical characteristics of the separation to match any effluent composition. In addition, as well as making geometrical adjustments to the separation means, it is possible to vary the flow rates of the various phases at the respective outlets of the separator, and thus to give preference to water retention time or to oil retention time, or to the retention times of both of the liquid phases. In this way, at the outlets of the separator, it is possible to recover either very pure water, or else oil that is free of any water.
Whatever the mufti-phase ratio of the effluent, by continuously adjusting the geometrical characteristics of the telescopic plate 5 or of the recovery ducts lb, it is possible to achieve effective separation of said phases, and thus to optimize use of the burners at the outlet of the separator. The environment is thus protected from any harmful discharge, while also avoiding having to treat additional waste in auxiliary and costly installations.
1n addition, by not fundamentally changing the component parts of a separator known from the state of the art, the separator of the invention is particularly low-cost and easy to make.
The separator can also be used after the transitional stage, once the composition of the effluent has become stable, because it is then necessary merely to lock the level of the weir plate or of the recovery duct.
. As a result, the separator of the invention.can also be used for effluents whose mufti-phase ratio is constant.
The separator of the invention can thus be used under a particularly ,vide range of conditions.
The invention relates to a gravity separator for mufti-phase effluents. A preferred application of the invention relates to a separator for effluent from an oil well, said effluent typically comprising three phases: ari aqueous phase, a liquid hydrocarbon phase, and a gaseous hydrocarbon phase.
After a hydrocarbon well has been drilled and made safe, production is started from the well for a relatively short time in order to identify clearly the types and magnitudes of its various components, and in order to estimate the production capacities of the well.
These tests, commonly referred to as "well testing", use means for separating out the various phases of the effluent (water, oil, and gas). Since the various phases are of different densities, separation takes place continuously in a vertical separator, in which the phases settle out. Downstream from the separator, the aqueous phase is discharged, optionally after undergoing additionalpurific.ation, and the hydrocarbons are~burnt off .
At the beginning of the testing step, the composition of the effluent varies enormously. Insofar as the well is initially filled with aqueous residues from the drilling fluid and from the completion fluid, the effluent that is collected is essentially made up of water. Then, gradually, the percentage of aqueous residue decreases, and the composition of the effluent becomes enriched with oil and with gas.
Since state-of-the-art separators are dimensioned to treat effluents whose phase ratio remains substantially stable over time, it is not possible to use them for the effluent at the beginning of the testing step.
Therefore, ways are sought to dispose of the effluent directly.
For that purpose, a first solution is known that consists in sending the effluent directly to burners without any separation step being performed.
Unfortunately, the burners known from the state of the art are effective only for mixtures in which the hydrocarbon content is at least 70o to 80%. As a result;
when the effluent is sent directly to such burners, the environment is polluted to a relatively large extent because of unburnt hydrocarbons. That solution poses serious pollution problems and is thus unacceptable.
Another known solution consists in recovering the effluent and in storing it temporarily in containers, until the oil that it contains separates from the aqueous phase and floats on the surface of it in said containers.
The oil phase is then recovered, and it is sent to the burners while the resulting cleaned aqueous phase is disposed of. Although that method gives rise to lower risks for the environment, it requires the site to be equipped with separators and additional pipes, constituting costly and voluminous equipment.
Another method consists in building an independent installation for treating effluent when its multi-phase ratio is not stable. Although that method is ecologically very satisfactory, it increases problems related to the cost of treatment installations and to the space they take up. Logistics problems are then particularly numerous. .
An object of the invention is to solve the problem of pollution related to treating an effluent whose multi-phase ratio varies over time, without it being necessary to collect waste which must then be treated subsequently.
To this end, the invention provides a gravity separator for an effluent made up of a multi-phase fluid mixture comprising at least a heavy first phase and a supernatant second phase, said separator including adjustment means for adjusting its geometrical separation characteristics.
By adjusting its geometrical separation characteristics, it is possible to treat effluent whose phase ratio is not~constant over time. As a result, when used for effluent from an oil well, the separator of the invention makes it possible to treat said effluent throughout the period during which the ratios of the three phases, namely water, oil, and gas, are not stabilized.
It is thus possible to treat the effluent in the separator regardless of how the volume ratios of the various phases fluctuate as a function of time. Insofar as the separator of the.,inv'ention is followed by a burner, the burner~receives a mixture whose hydrocarbon content makes, it possible to burn off the hydrocarbons without any discha~ge,that is harmful to the environment, and a cleaned aqueous phase ,is recovered without an additional separator being necessary.
The separator of the invention thus makes it possible to preserve-the environment without it being necessary tocollec~'waste that must then be treated by an auxiliary~;installation:
' In an . ad.vai~.tageous:embodiment of the invention, ~ the adjustmentmeans ~ for 'adjusting its geometrical separation characterist'lcs, make it possible to .give preference to separating out"certain.phases of the effluent , taken on their own or-in combination.
This makes ~.t,,possible to act on the separation characterist~ics~in order to give preference to the retention time of one phase in particular, depending on whether a higher level of purity is desired on one or other of the phases. This is particularly advantageous if very Clean'water;is,to be obtained, so that, for example, it is possible .to discharge said water directly without polluting the environment.
The invention will be well understood on reading the following description given with reference to the -. 35 accompanying.drawings. The list of accompanying drawings is as follows : . ' Figure 1 is a view of an embodiment of a separator of the invention;
Figure 2 is a cross-section view of said separator;
Figure 3 is a view of another embodiment of a separator of the invention;
Figure 4 is a view of another embodiment of a separator of the invention;
Figure 5a is a section view of a detail of an embodiment of a separator of the invention;
Figure 5b is a perspective view of the same detail;
Figure 6 is a view of a detail of another embodiment of a separator of the invention; and Figure 7 is an example of a drive device associated with an embodiment of a separator of the invention.
The separator of the invention makes it possible to treat effluent whose characteristics are as follows:
- At the beginning of the transitional stage, the effluent contains a very small proportion of gaseous hydrocarbons. The majority of the separator must 20. therefore be dedicated to separating the liquid-liquid phase, while the space left for the gas~phase can be minimized. In addition, most of the liquid-liquid phase is itself made up essentially of water, very little oil being supernatant on.said phase.
- At the end of the transitional stage and during the separation stage, the effluent is made up mostly of oil and of gas. In contrast, the percentage of water in the effluent is reduced considerably. It is thus necessary to maximize the space available in the separator~for the oil phase. and then for the gas phase.
Figure 1 shows an embodiment of a separator 1 of the invention, in which the phases settle out by gravity. By way of example, this separator 1 is substantially cylindrical in shape, and is the size of a tank that can be transported by truck. When treating effluent from an oil well, it must be possible to move the separator from site to site, and it thus necessary to have a separator of limited size.
As is known and not shown, a solids separator followed by a heat exchanger, and a burner are disposed respectively upstream and downstream from said separator 1.
In the embodiment shown in Figure 1, the separator 1 is provided with a separation or "weir" plate 5 whose height is adjustable as a function of the composition of the effluent. The weir plate 5 defines a first compartment for a heavy first phase, namely water, and a second compartment fed by overflow with the lower-density oil phase that floats on the aqueous phase. The weir plate 5 is made up of a support 5a and of various telescopic leaves 5b which can be deployed vertically towards the top of the separator 1.
As shown in Figure 2, the outlines of the support 5a.
follow the inside walls of the substantially-cylindrical separator 1. The moving leaves 5b are of substantially rectangular shape, and they are carried bythe support 5a. The shape of the support 5a and the dimensions of the rectangular leaves 5b are complementary so as to occupy the entire width of the separator 1. In this way, the weir plate assembly 5 constitutes a genuinely fluid-tight obstacle over a certain height, inside the separator 1.
The leaves 5b can thus be deployed gradually so as to form a weir plate of variable height. As a result, the further the telescopic weir plate 5 is deployed, the higher the maximum possible level of water and the longer the retention time for which the effluent is retained in the separator.
The leaves 5a of the telescopic weir plate 5 are in contact with one another. Whenever it is necessary to increase the height of the weir plate 5 slightly, the first leaf is deployed and is placed in vertical alignment with the other leaves. As a function of the desired height of the weir plate, the leaves 5b are successively deployed and each new leaf vertically increments the leaf most recently put in place.
In the low position, all of the leaves 5b are retracted inside the support 5a from which they do not project. In the embodiment shown, taking account of the overall size of the support and of the leaves, the nominal height of the weir plate, with all leaves retracted, represents substantially 30% of the height of the separator.
In the same embodiment, and in the high position, once all of the leaves 5b have been deployed, the height of the weir plate 5 represents substantially 650 of the total height of the separator 1. Provision is made for said leaves 5b to overlap so as to guarantee that suitable sealing is provided between all of the leaves without hindering the displacement of said leaves relative to one another..
The separator 1 is provided with three outlet ducts.
The water .phase .anal the oil phase are recovered respectively via the ducts 2 and 3 placed at the bottom of the separator. The gaseous phase is recovered via a duct 4 which, by way of example, conveys the gases to a burner (not shown). By way of example, the burner is a flare.
The first removal duct 2 for removing the aqueous phase is connected to an aqueous phase recovery duct 1a which is situated in the bottom portion of the separator 1, upstream from the weir plate 5. A
turbidimeter (not shown) makes it possible to determine the percentage of oil in the discharged water at the outlet of the separator 1. In one embodiment, the water is then sent via the duct 2 to an additional re-treatment unit that is not shown and that is known from the state of the art.
The second removal duct 3 for removing the oil phase is connected to an oil recovery duct 1b which is also situated at the bottom portion of the separator 1. A
sensor on the removal duct 3 makes it possible to determine the percentage of water in the oil leaving the separator 1.
It is possible to regulate the flow rate of the water sent to the removal duct 2 so that the level of the liquid phases does not exceed the height of the telescopic weir plate 5. Similarly, the flow rate of oil sent to the burner is regulated so that, inside the separator, said oil can always flow away by flowing over the telescopic weir plate 5.
Typically, at the start of the transitional stage, since the percentage of water in the effluent is particularly high, the weir plate 5 is at its maximum height. This, together with the regulation of the flow rate of water leaving the separator guarantees maximum water retention time and therefore particularly effective . separation of the water and oil phases.
Thereafter, the percentage of water in the effluent decreases, while the percentage of oil therein increases.
Thus, the capacity of the compartment dedicated to water, i.e. the height of the telescopic weir plate 5, is gradually reduced.
The separator 1 of the invention thus makes it possible to respond to changes in the composition of the effluent, such as those indicated above, The separation characteristics of the separator can be adjusted as a function of the composition of the effluent. Thus, regardless of how the volume ratios of the various phases of the effluent vary as a function of time, the separator adapts itself continuously to match said ratios so as to separate said phases.
With the separator of the invention, it is possible to treat a petroleum effluent during the transitional stage when the ratios of the oil, water, and gas phases have not yet become stable. As a result, the separator of the invention makes it possible to treat effluent continuously, as soon as it leaves the well, without giving rise to environrriental pollution or to waste that needs to be,treated separately.
Figure 3 shows another embodiment of a separator of.
the invention. In this embodiment, the separator 1 does-not include a telescopic weir plate 5, since the separation is not performed by causing the oil phase to flow over said weir plate 5. Both the water phase and the oil phase sari thus extend over the entire length of the separator 1.. This solution makes it possible to increase the water retention capacity of the separator 1.
The~recovery,duct 1a for recovering the aqueous phase is situated'.atlth.e bottom portion of the separator 1, substantially~at.its~end remote from the inlet duct via which the effluent is fed into said separator. 4In this way, said recovery.duct 1a is situated in a zone in which the two liquidwphases of the effluent are well separated.'-.The removal.duct,2 for.removing he aqueous ' phase is'connected,to.~said recovery duct.la. In order to avoid~~any turbulence,:.~which would hinder separation.of the. liquid phases;,.~a~rhaffle .lc can'be=placed immediately'' above the water recovery. duct, la, for example.
The removal.duct.3 for removing the hydrocarbon phase is also situated at the bottom portion of the separator 1 - ~.
A ~ecove~ry duct. 1b ~is connected to said removal duct 3. The recovery duct lb is made up of a telescopic tube comprising coaxial cylinders that are capable of moving progressively'relative to one another in a vertical direction~:inside the separator 1.
The recovery duct 1b is terminated by a suction intake or~"collector" 6~ embodiments of which are shown in more detail in Figures 5a, 5b, and 6. The recovery duct 1b is then deployed to an extent that can be caused w 35 to vary in order to~position the~collector 6 in the middle of the.oil~.phase regardless of the mufti-phase ratio of the effluent. During the transitional stage, the duct 1b is thus extended to its maximum extent so as to place the collector 6 high in the separator, in the oil phase, and so as to maximize the volume of the separator that is available for the aqueous phase. Then, as a function of the variation in the composition of the effluent, the recovery duct 1b is gradually lowered.
The position of the collector 6 is adjusted so that the percentage of water in the oil phase at the outlet of the separator does not exceed 30%. This is to guarantee that the burners at the outlet of the separator operate effectively, and thus to prevent any discharge of unburnt hydrocarbons into the environment.
Figure 4 shows a preferred embodiment of.a separator of the invention.
In this embodiment, the recovery duct 1b for recovering the oil is~constituted by a bellows of substantially cylindrical shape and made of flexible materials such as plastics materials. In the embodiment shown and for reasons of compactness, related to the materials of the bellows lb,.the nominal height of the bellows corresponds substantially to 30% of.the height of the separator l, whereas, once it is totally expanded, the bellows 1b has a height representing substantially 65% of the height of said separator 1.
A suction intake or "collector" 6 as shown in any one of Figures 5a, 5b, and 6 is situated at the end portion of the bellows 1b.
The use of a flexible bellows offers numerous advantages: it is a light-weight and low-cost system that, in addition, does not suffer from the sealing and sliding problems encountered with a telescopic deployment system. Advantageously, a guide device is provided that is constituted, for example, by four guide stakes.
As described above for the telescopic recovery duct, the bellows 1b is allowed to expand to various extents as a function of the mufti-phase ratio of the effluent, so that the collector 6 is always positioned in the middle of the oil phase. During the transitional stage, the bellows 1b is thus at its maximum height, leaving the maximum possible volume available for the aqueous phase.
Then, while the effluent is varying, the height of said bellows 1b is adjusted so as to recover oil whose water content is compatible with good burner efficiency at the burners at the outlet of the separator, i.e. a water content that does not exceed 30% in the oil phase.
Figures 5a and 5b show a first embodiment of a collector 6 in separators of the invention. This collector is made up mainly of a cover 6a overlying a collar 6b. In this way, the oil is sucked in radially through the empty space between the cover 6a and the collar 6b. This particular geometrical shape makes it possible to reduce turbulence on taking oil into the recovery duct 1b, thereby avoiding the risks of water or gas being sucked in, and the risks of a vortex being generated.
The space between the two portions 6a and 6b i.s small enough to make it easy to position the collector 6~
at the "cleanest" level in the oil phase, so as to recover the oil without running the above-mentioned risks.
Figure 6 shows another embodiment of a collector 6.
This collector is substantially in the form of a cylinder supporting a duck bill opening. Suction takes place radially, and the collector 6 can be positioned angularly so as to situate it as well as possible in the supernatant oil phase.
The position of the collector 6 in the oil phase can be adjusted at any time during the separation process.
For example, the collector 6 is firstly positioned in the middle of the oil phase. Then, secondly, the position is re-adjusted. For this purpose, in order to take account of the thickness of the collector 6, the decision is taken to place said collector in the oil phase in a zone ranging from 5% above the interface between the two l0 liquids to 5o below the level of the liquid. This makes it possible to maintain a water percentage of less than 30o in the oil at the outlet of the separator, which percentage is compatible with state-of-the-art burners. ..
The position of the collector is re-adjusted as a function of variation in measurements made at the outlet of the separator.
Figure 7 shows an actuator device for actuating the various above-described systems. This device makes it possible to drive the recovery duct 1b, be it in the form of a bellows, in the form of a telescopic tube, or in the form of a telescopic weir plate 5.
As shown in Figure 7, the actuator device is made up of pneumatic, hydraulic, or electrical actuator means 8 connected via a stepdown gearbox 10 to a worm screw 11 situated inside the separator 1. The worm screw 11 serves to drive a threaded rod 12 which (as shown in Figure 7) is itself connected to the collector 6 or to the first weir leaf 5b.
In another embodiment, the drive means of the actuator device are situated outside the separator and are connected tee a drive device constituted by a lever arm connected to the recovery duct 1b (i.e. the bellows or the cylinders of the telescopic tube) or to the weir leaves 5b. The drive device then has means for gearing down the movement in translation.
The separator of the invention thus makes it possible to adapt the geometrical characteristics of the separation to match any effluent composition. In addition, as well as making geometrical adjustments to the separation means, it is possible to vary the flow rates of the various phases at the respective outlets of the separator, and thus to give preference to water retention time or to oil retention time, or to the retention times of both of the liquid phases. In this way, at the outlets of the separator, it is possible to recover either very pure water, or else oil that is free of any water.
Whatever the mufti-phase ratio of the effluent, by continuously adjusting the geometrical characteristics of the telescopic plate 5 or of the recovery ducts lb, it is possible to achieve effective separation of said phases, and thus to optimize use of the burners at the outlet of the separator. The environment is thus protected from any harmful discharge, while also avoiding having to treat additional waste in auxiliary and costly installations.
1n addition, by not fundamentally changing the component parts of a separator known from the state of the art, the separator of the invention is particularly low-cost and easy to make.
The separator can also be used after the transitional stage, once the composition of the effluent has become stable, because it is then necessary merely to lock the level of the weir plate or of the recovery duct.
. As a result, the separator of the invention.can also be used for effluents whose mufti-phase ratio is constant.
The separator of the invention can thus be used under a particularly ,vide range of conditions.
Claims (9)
1/ A gravity separator for an effluent made up of a multi-phase fluid mixture comprising at least a heavy first phase and a supernatant second phase, said separator being characterized in that it includes adjustment means (5, 1b) which geometrical shapes, when driven by actuator means (8), are modified during use of said gravity separator, said adjustment means making it thus possible to adjust the ratio of the heavy first phase in the supernatant second phase when this latter is removed from said separator.
2/ A separator according to claim 1, in which the adjustment means comprises a separation plate or "weir plate" (5) that serves to define a first compartment for the first phase of the effluent, and a second compartment fed by the second phase flowing over said weir plate, said separator being characterized in that the geometrical characteristics of said weir plate (5) are adjustable as a function of variation in the ratios of said phases in said effluent.
3/ A separator according to claim 2, characterized in that the weir plate (5) comprises a support (5a) and telescopic leaves (5b), said leaves (5b) being deployable vertically towards the top of the separator (1).
4/ A separator according to claim 3, characterized in that the support (5a) and the leaves (5b) occupy the entire width of the separator (1), so as to form a fluid-tight obstacle over an adjustable height, inside said separator (1).
5/ A separator according to claim 1, wherein the adjustment means comprises recovery means (1b, 6) for recovering the supernatant phase in said separator, said separator being characterized in that the geometrical characteristics of said recovery means (1b, 6) that passes through the heavy phase, are adjustable as a function of variation in the multi-phase ratio of the effluent.
6/ A separator according to claim 5, characterized in that the recovery means (1b, 6) for recovering the supernatant phase are constituted by a telescopic tube (1b) made up of coaxial cylinders that move progressively relative to one another in a vertical direction as a function of the mufti-phase ratio of the effluent.
7/ A separator according to claim 5, characterized in that the recovery means (1b, 6) for recovering the supernatant phase are constituted by a flexible bellows (1b) that can be deployed as a function of the multi-phase ratio of the effluent.
8/ A separator according to claim 7, characterized in that guide means support the bellows so as to guide it vertically inside said separator (1).
9/ A separator according to any one of claims 5 to 8, characterized in that the recovery means (1b, 6) for recovering the supernatant phase are provided with a suction intake or "collector" (6) that is radial and/or directional.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR00/05666 | 2000-05-03 | ||
| FR0005666A FR2808456B1 (en) | 2000-05-03 | 2000-05-03 | GRAVITY SEPARATOR FOR MULTIPHASIC EFFLUENTS |
| PCT/EP2001/004719 WO2001083073A1 (en) | 2000-05-03 | 2001-04-26 | A gravity separator for multi-phase effluents |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2407191A1 CA2407191A1 (en) | 2001-11-08 |
| CA2407191C true CA2407191C (en) | 2010-08-17 |
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ID=8849858
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2407191A Expired - Lifetime CA2407191C (en) | 2000-05-03 | 2001-04-26 | A gravity separator for multi-phase effluents |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6881329B2 (en) |
| AU (1) | AU2001265905A1 (en) |
| CA (1) | CA2407191C (en) |
| EG (1) | EG22376A (en) |
| FR (1) | FR2808456B1 (en) |
| WO (1) | WO2001083073A1 (en) |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| FR2808455B1 (en) * | 2000-05-03 | 2003-02-14 | Schlumberger Services Petrol | INSTALLATION AND METHOD FOR SEPARATING MULTIPHASIC EFFLUENTS |
| US7024951B2 (en) * | 2002-04-12 | 2006-04-11 | Schlumberger Technology Corporation | Method of sampling from a multiphase fluid mixture, and associated sampling apparatus |
| EP1593418A1 (en) * | 2004-05-06 | 2005-11-09 | Services Petroliers Schlumberger | A gravity separator for a multi-phase effluent |
| GB0419994D0 (en) * | 2004-09-09 | 2004-10-13 | Kvaerner Process Systems As | Method and apparatus for improving the performance of a separator |
| CA2601817A1 (en) * | 2005-02-09 | 2007-08-09 | Giraffe Liquid Management Systems, Inc. | Adjustable height inlet/outlet liquid level management tools and systems |
| US8641813B2 (en) * | 2005-07-07 | 2014-02-04 | Expro Meters, Inc. | System and method for optimizing a gas/liquid separation process |
| SE530632C2 (en) * | 2005-09-19 | 2008-07-22 | Claes Olofsson | Oil recovery unit, e.g. for oil spills, comprises container with inflow(s) at its lower part, pump, holes in discharge channel, lower discharge for water surrounding mixture/emulsion, and upper discharge for oil bed |
| US8291979B2 (en) * | 2007-03-27 | 2012-10-23 | Schlumberger Technology Corporation | Controlling flows in a well |
| US7814976B2 (en) * | 2007-08-30 | 2010-10-19 | Schlumberger Technology Corporation | Flow control device and method for a downhole oil-water separator |
| US8006757B2 (en) * | 2007-08-30 | 2011-08-30 | Schlumberger Technology Corporation | Flow control system and method for downhole oil-water processing |
| NO330854B1 (en) * | 2009-10-23 | 2011-08-01 | Future Engineering As | Process for continuous use of a vacuum water separation circuit integrated with a hydraulic oil reservoir |
| US8449821B2 (en) * | 2010-05-25 | 2013-05-28 | Honeywell International Inc. | Slug mitigation by increasing available surge capacity |
| IT1401274B1 (en) | 2010-07-30 | 2013-07-18 | Nuova Pignone S R L | SUBMARINE MACHINE AND METHODS FOR SEPARATING COMPONENTS OF A MATERIAL FLOW |
| US8992838B1 (en) | 2011-02-02 | 2015-03-31 | EcoVapor Recovery Systems, LLC | Hydrocarbon vapor recovery system |
| US9776155B1 (en) | 2012-02-02 | 2017-10-03 | EcoVapor Recovery Systems, LLC | Hydrocarbon vapor recovery system with oxygen reduction |
| US9334109B1 (en) | 2012-02-02 | 2016-05-10 | EcoVapor Recovery Systems, LLC | Vapor recovery systems and methods utilizing selective recirculation of recovered gases |
| NL2013793B1 (en) * | 2014-11-13 | 2016-10-07 | Advanced Tech & Innovations B V | A continuous through-flow settling vessel, and a method of adaptive separation of a mixture from gas and/or oil exploration. |
| CN108331571A (en) * | 2017-01-18 | 2018-07-27 | 黄学锋 | Single well metering device gas-liquid separating method and device |
| CN110141888A (en) * | 2019-04-22 | 2019-08-20 | 江苏云端重工科技有限公司 | A kind of ground crude oil greasy filth washing spray separator |
| CN110669562B (en) * | 2019-10-12 | 2021-11-30 | 道骐科技有限公司 | Preparation method of lubricating oil |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US306169A (en) * | 1884-10-07 | Feedeick w | ||
| US289877A (en) * | 1883-12-11 | Storage-basin for water-works | ||
| US2826306A (en) * | 1953-09-10 | 1958-03-11 | Phillips Petroleum Co | Water-organic separator tank |
| US3971719A (en) * | 1974-12-09 | 1976-07-27 | Exxon Production Research Company | Three-phase separator |
| US4233154A (en) * | 1978-12-29 | 1980-11-11 | Kobe, Inc. | Method for treating petroleum well pumping power fluid |
| US4551246A (en) * | 1982-09-30 | 1985-11-05 | International Resources Management, Inc. | Flotation apparatus utilizing a novel floc barrier and current diverting means |
| US4867872A (en) * | 1986-07-28 | 1989-09-19 | Protectaire Systems Co. | Automatically adjustable weir and environmentally protected sensor |
| IT1233081B (en) * | 1989-08-08 | 1992-03-14 | Gi Pi S A S Di Alfonso Gallett | BLUSHING DEVICE FOR CONTAINMENT TANKS OF RANTI REFRIGE FLUIDS WITH SUSPENSION OILS FOR OIL REMOVERS |
| US4980070A (en) * | 1989-09-15 | 1990-12-25 | Mayfran International Incorporated | Floating oil separator and process |
| JPH0615262A (en) * | 1990-10-19 | 1994-01-25 | Daniel L Bowers Co | Device and method for separating fine particle from liquid having floating fine particle therein |
| DE9101241U1 (en) * | 1991-02-04 | 1991-05-02 | Boedrich & Strecker Anlagenbau, 7209 Deilingen, De | |
| JP2635482B2 (en) * | 1992-06-22 | 1997-07-30 | 広和機械設計工業株式会社 | Surface liquid discharge device |
| US5378376A (en) * | 1993-07-06 | 1995-01-03 | Wisconsin Oven Corporation | Sludge collector employing floating weir |
| FR2717401B1 (en) * | 1994-03-16 | 1996-06-07 | Rhone Poulenc Chimie | Method and device for extracting, within a closed reactor, the phase of lower density, from a two-phase system with the presence of an interface. |
| US5897773A (en) * | 1997-01-31 | 1999-04-27 | Rhodes; Laurence Mark | Skimming apparatus |
-
2000
- 2000-05-03 FR FR0005666A patent/FR2808456B1/en not_active Expired - Fee Related
-
2001
- 2001-04-26 WO PCT/EP2001/004719 patent/WO2001083073A1/en active Application Filing
- 2001-04-26 US US10/258,634 patent/US6881329B2/en not_active Expired - Lifetime
- 2001-04-26 AU AU2001265905A patent/AU2001265905A1/en not_active Abandoned
- 2001-04-26 CA CA2407191A patent/CA2407191C/en not_active Expired - Lifetime
- 2001-04-30 EG EG20010444A patent/EG22376A/en active
Also Published As
| Publication number | Publication date |
|---|---|
| US20030159986A1 (en) | 2003-08-28 |
| CA2407191A1 (en) | 2001-11-08 |
| EG22376A (en) | 2002-12-31 |
| WO2001083073A1 (en) | 2001-11-08 |
| US6881329B2 (en) | 2005-04-19 |
| FR2808456B1 (en) | 2003-02-14 |
| FR2808456A1 (en) | 2001-11-09 |
| AU2001265905A1 (en) | 2001-11-12 |
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