CA2420034C - Jet pump system for forming an aqueous oil sand slurry - Google Patents

Jet pump system for forming an aqueous oil sand slurry Download PDF

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Publication number
CA2420034C
CA2420034C CA002420034A CA2420034A CA2420034C CA 2420034 C CA2420034 C CA 2420034C CA 002420034 A CA002420034 A CA 002420034A CA 2420034 A CA2420034 A CA 2420034A CA 2420034 C CA2420034 C CA 2420034C
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CA
Canada
Prior art keywords
oil sand
slurry
jet pump
jet
crushed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CA002420034A
Other languages
French (fr)
Other versions
CA2420034A1 (en
Inventor
Jim Mcturk
Ron Cleminson
Andrew Rosser
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Murphy Oil Co Ltd
Canadian Oil Sands LP
Imperial Oil Resources Ltd
Nexen Inc
Petro Canada Oil and Gas
Canadian Oil Sands Commercial Trust
Canadian Oil Sands Ltd
ConocoPhillips Oilsands Partnership II
Mocal Energy Ltd Japan
Original Assignee
Murphy Oil Co Ltd
Imperial Oil Resources Ltd
Nexen Inc
Petro Canada Oil and Gas
Canadian Oil Sands Commercial Trust
Canadian Oil Sands Ltd
ConocoPhillips Oilsands Partnership II
AEC Oil Sands LP
Mocal Energy Ltd Japan
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Murphy Oil Co Ltd, Imperial Oil Resources Ltd, Nexen Inc, Petro Canada Oil and Gas, Canadian Oil Sands Commercial Trust, Canadian Oil Sands Ltd, ConocoPhillips Oilsands Partnership II, AEC Oil Sands LP, Mocal Energy Ltd Japan filed Critical Murphy Oil Co Ltd
Priority to CA002420034A priority Critical patent/CA2420034C/en
Priority to US10/371,156 priority patent/US6821060B2/en
Publication of CA2420034A1 publication Critical patent/CA2420034A1/en
Application granted granted Critical
Publication of CA2420034C publication Critical patent/CA2420034C/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/50Mixing liquids with solids
    • B01F23/59Mixing systems, i.e. flow charts or diagrams
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/20Jet mixers, i.e. mixers using high-speed fluid streams
    • B01F25/21Jet mixers, i.e. mixers using high-speed fluid streams with submerged injectors, e.g. nozzles, for injecting high-pressure jets into a large volume or into mixing chambers
    • B01F25/211Jet mixers, i.e. mixers using high-speed fluid streams with submerged injectors, e.g. nozzles, for injecting high-pressure jets into a large volume or into mixing chambers the injectors being surrounded by guiding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/805Mixing plants; Combinations of mixers for granular material
    • B01F33/8052Mixing plants; Combinations of mixers for granular material involving other than mixing operations, e.g. milling, sieving or drying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/83Mixing plants specially adapted for mixing in combination with disintegrating operations
    • B01F33/831Devices with consecutive working receptacles, e.g. with two intermeshing tools in one of the receptacles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00Other mixers; Mixing plants; Combinations of mixers
    • B01F33/80Mixing plants; Combinations of mixers
    • B01F33/836Mixing plants; Combinations of mixers combining mixing with other treatments
    • B01F33/8361Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating
    • B01F33/83612Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating by crushing or breaking

Abstract

As-mined oil sand is crushed to -5 inch by a sequentially arranged pair of double roll crushers. The crushed oil sand is fed into a hopper feeding a jet pump. Water or recycled slurry is fed under pressure as motive fluid to the jet pump. The motive fluid jet(s) produced internally by the jet pump are operative to fluidize the oil sand and the components of the slurry mix turbulently in the jet pump's tubular mixer. It is found that the slurry issuing from the jet pump is aerated and largely free of lumps.

Description

1 "JET PUMP SYSTEM FOR FORMING
2 AN AQUEOUS OIL SAND SLURRY"
The present invention relates to a process and apparatus for mixing oil 6 sand with water and air to produce a slurry suitable for pumping and 7 pipelining.

The surface-minable oil sands in the Fort McMurray region of Northern 11 Alberta have now been commercially exploited for about 30 years.

12 Initially, the as-mined oil sand was deposited on conveyor belts and 13 transported to a facility known as an extraction plant. Here the oil sand was 14 crushed, screened to remove oversize and then introduced into a large, horizontal, rotating drum (referred to as a'tumbfer'), together with hot water 16 (95 C), a process aid (NaOH) and steam. The tumbler had internal lifters 17 which would lift and cascade the mixture as it advanced lengthwise through 18 the tumbler chamber. A thick hot slurry containing entrained air bubbles 19 would be formed.

During residence in the tumbler:

21 = lumps of oil sand would be fragmented and would disintegrate;

22 = bitumen would separate from the sand and enter the water phase of 23 the slurry as small flecks; and 24 = some bitumen flecks would coalesce and attach to air bubbles.
{ET112332.DOC;1 }

1 The sum of these actions is referred to in the industry as 'conditioning'.

2 The resulting conditioned slurry would then be diluted with additional 3 hot water and would be introduced into a large, open-topped, cylindrical 4 flotation vessel having a conical bottom. This vessel is known as the primary separation vessel or PSV. In the PSV, the sand would settle under the 6 influence of gravity, be concentrated in the cone and leave as an underflow 7 stream of wet tailings. The aerated bitumen would rise and be recovered as 8 an overflow stream of froth. A watery mixture called 'middlings' would be 9 withdrawn from the mid-section of the PSV and would be further processed to recover residual bitumen.

11 As the mining areas got further from the extraction plant, a new system 12 -was implemented. The as-mined oil sand was crushed and mixed with.hot 13 water at the mine site. The produced slurry, containing entrained air, was 14 then pumped through a pipeline. It had been discovered that the slurry would 'condition' suitably, if given adequate retention time, as it moved through the 16 pipeline. It could then be fed directly to the PSV. The degree of bitumen 17 recovery in the PSV was found to be sufficient to be viable.

18 In connection with this new 'at the mine site' system, it was necessary 19 to develop means for forming a pumpable, pipelineable slurry from the dry as-mined oil sand, which comprises large frozen lumps, rocks and the like.

21 At applicants' facility, two distinct slurry preparation systems were 22. sequentially developed and installed on a commercial basis.

(ETI 12332.DOC;1 ) 1 The first slurry preparation system was disclosed in our U.S. Patent 2 No. 5,039,227. This system involved a vertical tower arrangement 3 comprising:

4 = an open-topped cylindrical vessel (called a 'cyclofeeder'), having a conical bottom and central bottom outlet, for forming slurry;

6 = a set of vibrating screens which were positioned beneath the 7 bottom outlet and which were adapted to reject +2 inch material from 8 the slurry;

9 = a tall pump box positioned beneath the screens for receiving the screened slurry; and 11 = a pump for pumping siurry from the pump box into a pipeline.

12 The as-mined oil sand would first be crushed to -24 ches: The crushed oil 13 sand and added water would then be poured into the cyclofeeder chamber, 14 where they would add to a rotating vortex of slurry recycled from the pump box and pumped tangentially into the vessel chamber. Air would be entrained 16 in the vortex. The resulting slurry dropped onto the screens. The rejected 17 oversize material was dumped on the ground or was conveyed to another 18 crusher and subjected to a repetition of the same process. The wet-screened 19 slurry was collected in the pump box, ready for pumping down the pipeline, and a portion was pumped back to the cyclofeeder to form the vortex.

{ET] 12332.DOC;] }

1 The second slurry preparation system was disclosed in our U.S. Patent 2 No. 5,772,127. It too was a vertical tower arrangement. It involved:

3 = a downwardly descending zig-zag arrangement of troughs into 4 which oil sand and water would be poured, to mix and form a slurry containing entrained air;

6 = a set of screens for separating + 4 inch oversize from the slurry;
7 = an impactor for breaking up some of the screen reject material;

8 = a screen for screening the impactor product to produce oversize 9 rejects and underflow;

= a tall pump box positioned to receive the wet-screened slurry and 11 the impactor underflow; and . .
12 " = a pump for pumping slurry from the pump *box int a, pipeline.

13' The as-mined oil sand was crushed to'-24 inches. The crushed oil sand and 14 water were fed into the trough, where they mixed and formed the slurry. Air would concurrently be entrained in the slurry. The slurry was wet-screened to 16 reject +4 inch material. The screen reject was impacted and then screened.
17 The impactor product was directed into the pump box. The impactor reject 18 was dumped onto the ground.

19 The second slurry preparation system was better than the first in that the amount of reject (and the oil lost with it) was significantly reduced.

21 The two slurry preparation systems had certain problematic 22 characteristics, namely:

23 = they were massive and essentially non-movable (the first system 24 was 34 meters tall, the second was 32 meters tall):

{ET112332.DOC;1 }

1 = they both dumped rejects on the ground - these rejects had to be 2 continually removed with loaders and trucks, to make room for new 3 reject material and to suitably dispose of the removed material; and 4 = due to their immobility, the system could not follow the mining 5 shovels and therefore the cost of trucking the as-mined oil sand from 6 the shovel to the slurry preparation tower increased steadily as the 7 shovels moved further away.
8 There has therefore existed a long-standing need to provide a re-9 locatable, smaller, lighter, simpler slurry preparation system. It is the objective of this invention to provide such a system.

13 In accordance with the invention, as-mined oil sand is first crushed to a 14 pumpable size. This is preferably done using a sequentially arranged pair of double roll crushers operative to crush the as-mined oil sand in stages, to a 16 final size of about -5 inches or less. The entire stream of pre-crushed oil 17 sand is then fed into a mass flow hopper. The hopper is connected to a 18 conventional jet pump and feeds the oil sand into its fluidization chamber.

19 The jet pump comprises:

= a body forming the fluidization chamber;

21 = a main nozzle, connected to a source of pressurized motive fluid, 22 the nozzle being operative to deliver a jet of fluid from one end of the 23 fluidization chamber;

{ET112332.DOC;1 }

1 = a tubular mixer, aligned in spaced downstream relationship to the 2 main nozzle, so as to receive the jet into its inlet end, the mixer 3 extending through the other end of the body;

4 = optionally, one or more dilution nozzles, also connected to a source of pressurized motive fluid, are positioned in the fluidization 6 chamber. The dilution nozzles are operative to inject jets of motive 7 fluid to assist in fluidizing oil sand entering the chamber from the 8 hopper; and 9 = a slurry line, connected to the outlet end of the mixer, for conveying away produced slurry.

11 In operation, the motive fluid jet from the main nozzle extends through 12 the open space in the fluidization chamber, between:'it and'the mixer, and 13 enters the bore of the mixer. In the course of doing so, it entrains oil sand 14 entering from the hopper. The dilution nozzles emit fluid jets which help to fluidize the oil sand entering the chamber. The motive fluid and oil sand mix 16 as they move through the bore of the mixer. Lumps are disintegrated.
17 Entrained air contacts and aerates bitumen. These actions continue in the 18 downstream slurry line.

19 Surprisingly, our testing indicates that the lumps of oil sand have been largely or entirely disintegrated by the time the product slurry leaves the jet 21 pump. We believe that the combination of acceleration, shear, mixing and 22 heat inputs cause this remarkable and almost instantaneous disintegration.
23 The jet pump produces a slurry that can be directly fed into and pumped 24 through the downstream slurry line.

{ ET112332.DOC;1 }

1 Furthermore, our testing indicates that the slurry leaving the jet pump is 2 well advanced to being fully conditioned. Instead of having to pump the slurry 3 for 10-15 minutes through several kilometers of pipeline to condition it 4 sufficiently to feed it to a PSV, it appears that the jet pump slurry is fully conditioned in less than a minute of pipeline travel.

6 Should a higher density slurry be desirable, a screened slipstream can 7 be withdrawn from the slurry line and introduced into the fluid going to the jet 8 pump main nozzle. Our testing has indicated that denser fluid going to the 9 nozzle increases oil sand capture, producing a dense slurry (e.g. 1.6 S.G.).

The system is also characterized by the following additional i l advantages:

12 =,,the size and weight of the present slurry preparation systemis only 13 a fraction of the prior art towers. It is feasible to periodically relocate 14 the hopper and jet pump assembly to keep it near to the mine face;
= there are no rejects from the system and consequently no oil losses 16 with rejects; and 17 = there is no need for slurry screens.

18 In one embodiment, a process is provided for preparing an aerated 19 aqueous oil sand slurry comprising: crushing as-mined oil sand to pumpable size; feeding the crushed oil sand to a jet pump; supplying motive fluid under 21 pressure to the jet pump to form a fluid jet which entrains and mixes with the 22 oil sand and forms an aerated slurry; and discharging the slurry into a 23 downstream product line.

{ST1I2332.DOC;1 }

1 In another embodiment, an apparatus is provided for preparing an 2 aqueous aerated oil sand slurry from as-mined oil sand, comprising: crusher 3 means for crushing the as-mined oil sand to pumpable size; a hopper; means 4 for feeding the crushed oil sand into the hopper; a jet pump comprising a body forming a fluidization chamber, a main nozzle extending into the fluidization 6 chamber and a tubular mixer spaced downstream from the main nozzle and 7 extending out of the body; the hopper being connected to the jet pump body 8 so as to feed oil sand into the fluidization chamber; means for supplying 9 motive fluid under pressure to the main nozzle to form a fluid jet which entrains and mixes with the oil sand to form an aerated aqueous oil sand 11 slurry; and conduit means connected to the downstream end of the mixer for :..12 , conveying ;the slurry produced by the jet purnp.

13_ Figure 1 is a plan view showing a test pilot slurry preparation system in 16 accordance with the invention;

17 Figure 2 is a simplified schematic representation of the slurry 18 preparation system of Figure 1;

19 Figure 3 is a sectional side view showing the main nozzle and inlet to the mixer, with arrows indicating the paths of oil sand and motive fluid;

21 Figure 4 is a plan view in section of a known jet pump;

22 Figures 5 and 6 are perspective views of a jet pump connected to a 23 mass flow hopper; and 24 Figure 7 is a schematic of the slurry preparation system of Figure 1.
{ ET112332.DOC;1 }

2 The invention will be described with respect to the slurry preparation 3 test pilot system 1 shown in Figures 1 and 7 and in reference to Figures 1 to 4 7.

The test pilot system 1 comprised a conveyor 2 which for -12 inch pre-6 crushed oil sand to a double roll ABONT'" crusher 3, which crushed it to -3 7 inch. The crushed oil sand was then fed by a second conveyor 4 to a mass 8 flow hopper 5.

9 The hopper 5 was mounted to the body 6 of a top-loading GENFLOTM
jet pump 7. Oil sand flowed by gravity into the fluidization chamber 8 of the jet 11 pump 7. Dilution nozzles 9 injected water under pressure in the form of jets 12 into the chamber 8, to fluidize and mix with the oil sand. Water (or, in some 13 runs, recycled slurry) was supplied under pressure to main nozzle 10 and 14 dilution nozzles 9 by pumps 11, 11 a through motive fluid supply lines 12, 12a.
The motive water left the main nozzle 10 in the form of a powerful jet. The 16 water jet crossed an entrainment zone 13 in the fluidization chamber 8 and 17 entered the inlet 14 of the bore 16 of a coaxial tubular mixer 15. The jet 18 induced the oil sand and water mixture in chamber 8 to be drawn into the bore 19 16. The water and oil sand formed an aqueous slurry which mixed turbulently as it proceeded through the bore 16. The slurry contained entrained air. The 21 mixer 15 was connected at its outlet end with a downstream pump 17 and 22 product line 18. And inline screen 19 and recycle line 20 were connected 23 between the product line 18 and the fluid supply line 12. If desired, a fine 24 solids slurry could be recycled to the main nozzle 10 to increase fluid density in the product line 18.

DMSLega1053707\00019\2360994v I

1 The following data and results characterized two typical runs of the 2 pilot.

Data Line # 12976 15169 Dilution Water flowrate I/s 14.58 15.23 Process Water flowrate I/s 61.5 79.5 Density in Slurry product line t/m3 1.41 1.60 Density in motive fluid line t/m3 1.0 1.39 Main nozzle pressure kpa 849.4 974.8 Jet pump discharge pressure kpa 126.0 115.6 Process Water temperature deg C 43 57.4 4: Although a preferred embodiment' has been stlown and described, it 5 will be appreciated by those skilled in the art that various changes and 6 modifications might be made without departing from the scope of the 7 invention, as defined in the appended claims.

(ET112332.DOC;1 }

Claims (7)

1. A process for preparing an aerated aqueous oil sand slurry comprising:

crushing as-mined oil sand to pumpable size;
feeding the crushed oil sand to a jet pump;

supplying motive fluid under pressure to the jet pump to form a fluid jet which entrains and mixes with the oil sand and forms an aerated slurry; and discharging the slurry into a downstream product line.
2. The process as set forth in claim 1 comprising:

recycling part of the formed slurry back to the jet pump to control the density of the slurry.
3. The process as set forth in claim 1 or 2 wherein:

the as-mined oil sad in crushed a size of less than 5 inches.
4. The process as set forth in claim 1, 2 or 3 wherein the motive fluid is water.
5. Apparatus for preparing an aqueous aerated oil sand slurry from as-mined oil sand, comprising:

crusher means for crushing the as-mined oil sand to pumpable size;
a hopper;

means for feeding the crushed oil sand into the hopper;

a jet pump comprising a body forming a fluidization chamber, a main nozzle extending into the fluidization chamber and a tubular mixer spaced downstream from the main nozzle and extending out of the body;

the hopper being connected to the jet pump body so as to feed oil sand into the fluidization chamber;

means for supplying motive fluid under pressure to the main nozzle to form a fluid jet which entrains and mixes with the oil sand to form an aerated aqueous oil sand slurry; and conduit means connected to the downstream end of the mixer for conveying the slurry produced by the jet pump.
6. The apparatus as set forth in claim 5 wherein the jet pump comprises dilution nozzles extending into the fluidization chamber;

said apparatus comprising means for supplying motive fluid under pressure to the dilution nozzles to assist in fluidizing oil sand entering the chamber.
7. The apparatus as set forth in claim 5 or 6 wherein:

the crusher means comprises a pair of sequentially arranged double roll crushers.
CA002420034A 2003-02-18 2003-02-18 Jet pump system for forming an aqueous oil sand slurry Expired - Lifetime CA2420034C (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CA002420034A CA2420034C (en) 2003-02-18 2003-02-18 Jet pump system for forming an aqueous oil sand slurry
US10/371,156 US6821060B2 (en) 2003-02-18 2003-02-24 Jet pump system for forming an aqueous oil sand slurry

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CA002420034A CA2420034C (en) 2003-02-18 2003-02-18 Jet pump system for forming an aqueous oil sand slurry
US10/371,156 US6821060B2 (en) 2003-02-18 2003-02-24 Jet pump system for forming an aqueous oil sand slurry

Publications (2)

Publication Number Publication Date
CA2420034A1 CA2420034A1 (en) 2004-08-18
CA2420034C true CA2420034C (en) 2007-09-25

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CA (1) CA2420034C (en)

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US20040165960A1 (en) 2004-08-26
CA2420034A1 (en) 2004-08-18

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