CA2528677A1 - Compositions and methods for consolidating unconsolidated subterranean formations - Google Patents
Compositions and methods for consolidating unconsolidated subterranean formations Download PDFInfo
- Publication number
- CA2528677A1 CA2528677A1 CA002528677A CA2528677A CA2528677A1 CA 2528677 A1 CA2528677 A1 CA 2528677A1 CA 002528677 A CA002528677 A CA 002528677A CA 2528677 A CA2528677 A CA 2528677A CA 2528677 A1 CA2528677 A1 CA 2528677A1
- Authority
- CA
- Canada
- Prior art keywords
- surfactant
- resin composition
- ether
- combinations
- resin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/02—Well-drilling compositions
- C09K8/04—Aqueous well-drilling compositions
- C09K8/06—Clay-free compositions
- C09K8/12—Clay-free compositions containing synthetic organic macromolecular compounds or their precursors
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/56—Compositions for consolidating loose sand or the like around wells without excessively decreasing the permeability thereof
- C09K8/57—Compositions based on water or polar solvents
- C09K8/575—Compositions based on water or polar solvents containing organic compounds
- C09K8/5751—Macromolecular compounds
- C09K8/5756—Macromolecular compounds containing cross-linking agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
- C09K8/60—Compositions for stimulating production by acting on the underground formation
- C09K8/80—Compositions for reinforcing fractures, e.g. compositions of proppants used to keep the fractures open
Abstract
The present invention described a resin composition comprising from about 5%
to about 30% phenol, from about 40% to about 70% phenol formaldehyde, from about 10% to about 40% furfuryl alcohol, from about 0.1% to about 3% of a silane coupling agent, and from about 1% to about 15% of a surfactant and methods of using of that resin in consolidating subterranean formation fines.
to about 30% phenol, from about 40% to about 70% phenol formaldehyde, from about 10% to about 40% furfuryl alcohol, from about 0.1% to about 3% of a silane coupling agent, and from about 1% to about 15% of a surfactant and methods of using of that resin in consolidating subterranean formation fines.
Claims (26)
1. A method of consolidating particulates in a subterranean region comprising the steps of:
applying a preflush fluid to the subterranean region;
applying a resin composition to the subterranean region wherein the resin comprises:
from about 5% to about 30% phenol;
from about 40% to about 70% phenol formaldehyde;
from about 10% to about 40% furfuryl alcohol;
from about 0.1% to about 3% of a silane coupling agent; and, from about 1% to about 15% of a surfactant; and, applying an after-flush fluid to the subterranean region.
applying a preflush fluid to the subterranean region;
applying a resin composition to the subterranean region wherein the resin comprises:
from about 5% to about 30% phenol;
from about 40% to about 70% phenol formaldehyde;
from about 10% to about 40% furfuryl alcohol;
from about 0.1% to about 3% of a silane coupling agent; and, from about 1% to about 15% of a surfactant; and, applying an after-flush fluid to the subterranean region.
2. The method of claim 1 wherein the unconsolidated region is an area surrounding a wellbore.
3. The method of claim 2 wherein the resin is applied such that the area surrounding the wellbore is saturated to a depth from about 1 to about 3 feet.
4. The method of claim 1 wherein the unconsolidated region is an area surrounding a fracture.
5. The method of claim 4 wherein the resin is applied such that the area surrounding the fracture is saturated to a depth is from about 0.25 to about 2 inches.
6. The method of claim 1 wherein the preflush fluid comprises an aqueous liquid and a surfactant.
7. The method of claim 6 wherein the aqueous liquid is fresh water, salt water, brine, or mixtures thereof.
8. The method of claim 6 wherein the surfactant comprises ethoxylated nonyl phenol phosphate ester, a cationic surfactant, a non-ionic surfactant, an alkyl phosphonate surfactant, or combinations thereof.
9. The method of claim 1 wherein the silane coupling agent is N-2-(aminoethyl)-3-aminopropyltrimethoxysilane, 3-glycidoxypropyltrimethoxysilane, n-beta-(aminoethyl)-gamma-aminopropyl trimethoxysilane, or combinations thereof.
10. The method of claim 1 wherein the surfactant is ethoxylated nonyl phenol phosphate ester, a cationic surfactant, a non-ionic surfactant, an alkyl phosphonate surfactant, or combinations thereof.
11. The method of claim 1 wherein the resin composition has a viscosity of below 100 cP.
12. The method of claim 1 wherein the resin composition further comprises a solvent.
13. The method of claim 12 wherein the solvent comprises 2-butoxy ethanol, butylglycidyl ether, dipropylene glycol methyl ether, dipropylene glycol dimethyl ether, dimethyl sulfoxide, dimethyl formamide, diethyleneglycol methyl ether, diethylene glycol dimethyl ether, ethyleneglycol butyl ether, diethyleneglycol butyl ether, gamma-butyrolactone, butylene carbonate, propylene carbonate, ethylene carbonate, methanol, butyl alcohol, d'limonene, fatty acid methyl esters, or combinations thereof.
14. The method of claim 1 wherein the aqueous liquid in the preflush solution comprises fresh water, salt water, brine, or mixtures thereof.
15. The method of claim 1 wherein the surfactant in the preflush solution comprises ethoxylated nonyl phenol phosphate ester, cationic surfactant, non-ionic surfactant, alkyl phosphonate surfactant, or mixtures thereof.
16. The method of claim 1 wherein the after-flush fluid comprises fresh water, salt water, brine, or mixtures thereof:
17. The method of claim 1 wherein the after-flush fluid comprises nitrogen.
18. The method of claim 1 further comprising the step of, after applying the after-flush fluid, waiting a chosen period of time.
19. The method of claim 18 wherein the chosen period of time is from about 6 to about 48 hours.
20. A resin composition comprising:
from about 5% to about 30% phenol;
from about 40% to about 70% phenol formaldehyde;
from about 10% to about 40% furfuryl alcohol;
from about 0.1% to about 3% of a silane coupling agent; and, from about 1% to about 15% of a surfactant; and, a solvent.
from about 5% to about 30% phenol;
from about 40% to about 70% phenol formaldehyde;
from about 10% to about 40% furfuryl alcohol;
from about 0.1% to about 3% of a silane coupling agent; and, from about 1% to about 15% of a surfactant; and, a solvent.
21. The resin composition of claim 20 wherein the silane coupling agent is N-2-(aminoethyl)-3-aminopropyltrimethoxysilane, 3-glycidoxypropyltrimethoxysilane, n-beta- (aminoethyl)-gamma-aminopropyl trimethoxysilane, or combinations thereof.
22. The resin composition of claim 20 wherein the surfactant is ethoxylated nonyl phenol phosphate ester, a cationic surfactant, a non-ionic surfactant, an alkyl phosphonate surfactant, or combinations thereof.
23. The resin composition of claim 20 further comprising a solvent.
24. The resin composition of claim 23 wherein the solvent comprises 2-butoxy ethanol, butylglycidyl ether, dipropylene glycol methyl ether, dipropylene glycol dimethyl ether, dimethyl sulfoxide, dimethyl formamide, diethyleneglycol methyl ether, diethylene glycol dimethyl ether, ethyleneglycol butyl ether, diethyleneglycol butyl ether, gamma-butyrolactone, butylene carbonate, propylene carbonate, ethylene carbonate, methanol, butyl alcohol, d'limonene, fatty acid methyl esters, or combinations thereof.
25. The resin composition of claim 20 wherein the resin further comprises a hydrolyzable ester.
26. The resin composition of claim 25 wherein the hydrolyzable ester comprises dimethylglutarate, dimethyladipate and dimethylsuccinate, sorbitol, catechol, dimethylthiolate, methyl salicylate, dimethyl salicylate, dimethylsuccinate, ter-butylhydroperoxide, or mixtures thereof.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/603,492 US7013976B2 (en) | 2003-06-25 | 2003-06-25 | Compositions and methods for consolidating unconsolidated subterranean formations |
US10/603,492 | 2003-06-25 | ||
PCT/GB2004/002727 WO2005001243A2 (en) | 2003-06-25 | 2004-06-24 | Compositions and methods for consolidating unconsolidated subterranean formations |
Publications (2)
Publication Number | Publication Date |
---|---|
CA2528677A1 true CA2528677A1 (en) | 2005-01-06 |
CA2528677C CA2528677C (en) | 2010-08-03 |
Family
ID=33539746
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CA2528677A Expired - Fee Related CA2528677C (en) | 2003-06-25 | 2004-06-24 | Compositions and methods for consolidating unconsolidated subterranean formations |
Country Status (4)
Country | Link |
---|---|
US (1) | US7013976B2 (en) |
CA (1) | CA2528677C (en) |
MX (1) | MXPA05014051A (en) |
WO (1) | WO2005001243A2 (en) |
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-
2003
- 2003-06-25 US US10/603,492 patent/US7013976B2/en not_active Expired - Fee Related
-
2004
- 2004-06-24 CA CA2528677A patent/CA2528677C/en not_active Expired - Fee Related
- 2004-06-24 MX MXPA05014051A patent/MXPA05014051A/en active IP Right Grant
- 2004-06-24 WO PCT/GB2004/002727 patent/WO2005001243A2/en active Application Filing
Also Published As
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WO2005001243A2 (en) | 2005-01-06 |
CA2528677C (en) | 2010-08-03 |
US20040261997A1 (en) | 2004-12-30 |
WO2005001243A3 (en) | 2005-05-12 |
MXPA05014051A (en) | 2006-03-17 |
US7013976B2 (en) | 2006-03-21 |
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