CN102564811A - Sulfur hexafluoride gas sampling device - Google Patents

Sulfur hexafluoride gas sampling device Download PDF

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Publication number
CN102564811A
CN102564811A CN2012100025866A CN201210002586A CN102564811A CN 102564811 A CN102564811 A CN 102564811A CN 2012100025866 A CN2012100025866 A CN 2012100025866A CN 201210002586 A CN201210002586 A CN 201210002586A CN 102564811 A CN102564811 A CN 102564811A
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gas
hydrogen fluoride
last
sulfur hexafluoride
sampling
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CN2012100025866A
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CN102564811B (en
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李建国
汪献忠
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Henan Relations Co Ltd
Henan Relations Electronics Co Ltd
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Henan Relations Co Ltd
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Abstract

The invention discloses a sulfur hexafluoride gas sampling device, comprising a base and a shell which is provided with an external equipment interface and is arranged on the base. A gas washing bottle, a sampling bottle and a multi-way valve with at least four connection openings are arranged in the shell; a hydrogen fluoride gas colorimetric mechanism is arranged outside the shell; the four connection openings of the multi-way valve are respectively connected with the connection opening of the external equipment of the shell, the gas washing bottle, the sampling bottle and the hydrogen fluoride gas colorimetric mechanism through a gas guide pipe; and an operation handle for opening and closing each connection opening of the multi-way valve is externally arranged on the shell. The hydrogen fluoride gas colorimetric mechanism disclosed by the invention has the advantages of compact and reasonable structure, beautiful and elegant appearance, simple and clear operation process, convenience for maintenance, flexibility in use and relatively individual functions, and has functions of carrying out hydrogen fluoride gas colorimetric detection, displaying pressure of a sampled gas on a pressure meter during sampling, assisting in heating in a process of vacuumizing the sampling device and the like. Therefore, the vacuumization is accelerated and residual matters in a container of the sampling device are released completely, so as to achieve a real numerical value which is the same of the numerical value of an original gas when the sampling is carried out.

Description

The sulfur hexafluoride gas ST
Technical field
The present invention relates to a kind of gas sample pick-up unit, relate in particular to a kind of sulfur hexafluoride gas ST.
Background technology
The stable performance of sulfur hexafluoride (SF6) aerochemistry has good insulation performance and arc extinction performance, is widely used in the middle of the high voltage electric equipment.Parameters such as the kind of the purity of sulfur hexafluoride gas, dew point, micro-water content, decomposition product and content have direct influence to the safe and reliable work of high voltage electric equipment; Therefore; The relevant criterion of State Grid's industry such as GB8905-1996 " The guide for processing and measuring SF6 gas in power apparatus ", DL/T639-1997 " sulfur hexafluoride electrical equipment operation, test and maintainer's security protection detailed rules and regulations " all regulation want regularly the check and analysis of taking a sample of the sulfur hexafluoride gas in the high voltage electric equipment.
At present; To electrical equipment, gas-holder and the gas storage steel cylinder etc. that the use sulfur hexafluoride gas general sampling steel cylinder that adopts of taking a sample; This sampling steel cylinder is easy entrained air in sampling process, and has gaseous impurities at the steel cylinder inwall, will cause sulfur hexafluoride gas sample like this and decompose and secondary pollution; Take the laboratory after the sampling and analyze the data nature, have bigger error with regard to out of true.
Summary of the invention
The present invention is in order to solve weak point of the prior art, the sulfur hexafluoride gas ST that provide a kind of and guarantee that sample is undistorted, the functions such as hydrogen fluoride gas detection in collection gas washing, gas sample and the gas is melted into a whole.
For solving the problems of the technologies described above; The present invention adopts following technical scheme: the sulfur hexafluoride gas ST; Comprise the housing that is provided with on base and the base with external equipment connector; Be provided with Drexel bottle, sampling jar in the said housing and have the multiport valve of four connectors at least; Housing is provided with hydrogen fluoride gas colorimetric mechanism outward, and four connectors of multiport valve are connected with external equipment connector, Drexel bottle, sampling jar and the hydrogen fluoride gas colorimetric mechanism of housing through a wireway respectively, and housing is provided with the operating grip of each connector keying of control multiport valve outward.
Said hydrogen fluoride gas colorimetric mechanism comprises the last test tube device and following test tube device that is fixedly connected with housing; Be inserted with the hydrogen fluoride color comparison tube between last test tube device and the following test tube device, hydrogen fluoride color comparison tube top is provided with the test tube handle that is used with last test tube device.
The said test tube device of going up comprises the upper fixed seat with last vertical through holes and last horizontal pore; Be communicated with a connector and the last vertical through holes of multiport valve respectively inside and outside the last horizontal pore of upper fixed seat; The test tube handle is removably connected with motion bar through jackscrew; Last motion bar is plugged in the last vertical through holes of upper fixed seat, is provided with the last gas passage that is communicated with the last horizontal pore of upper fixed seat in the last motion bar, and last motion bar is arranged with the 3rd compression spring that cooperates with the upper fixed seat roof pressure outward;
Said test tube device down comprises the lower fixed seat with following vertical through holes and following horizontal pore; Be communicated with Drexel bottle and following vertical through holes respectively inside and outside the following horizontal pore of lower fixed seat; Valve inside under being provided with down motion bar in the following vertical through holes of lower fixed seat and being positioned under the motion bar; Be provided with the following gas passage that is communicated with the following horizontal pore of lower fixed seat in the following motion bar; The vertical section of following gas passage and last gas passage is corresponding up and down to be provided with, and following motion bar is arranged with the 4th compression spring that cooperates with the lower fixed seat roof pressure outward.
Said external equipment connector and hydrogen fluoride gas colorimetric mechanism are located at the housing sidepiece; Multiport valve is located at the case top inboard; Operating grip is located at the case top outside; Sampling jar is located at housing central authorities, and Drexel bottle is the toroidal cavity that forms between inner walls and the sampling jar outer wall, and hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle.
Be provided with pressure vacuum gauge and constant temperature switch in the said base; The base plate of base is provided with socket; Pressure vacuum gauge is connected with sampling jar through a piezometric tube, is provided with the heating element of tubular between sampling jar outer wall and the Drexel bottle inwall, and the top board of base is bolted with carrying bolt; The carrying bolt top is provided with the sampling jar pressing plate; Sampling jar pressing plate and sampling jar are provided with heat-preservation cotton between the bottom, be provided with in the heat-preservation cotton be close to the sampling jar bottom be used to guarantee to vacuumize or take a sample keep the temperature sensor of temperature constant state, the constant temperature switch is connected with temperature sensor through lead.
Said housing sidepiece is provided with handle.
Said case top is provided with the check device of control operation handle return.
Said check device comprises non-return button and the register pin that protrudes from the housing upper plate respectively, the non-return guide pin bushing that is located at the upper plate lower surface and register pin guide pin bushing, be located under the non-return guide pin bushing split pin and two ends are fixedly connected on the non-return connecting link on non-return button and the register pin; The non-return button passes the non-return guide pin bushing and is connected with split pin; The non-return connecting link is between non-return guide pin bushing and split pin; Between non-return connecting link and split pin, be arranged with first compression spring on the non-return button; The register pin bottom is located in the register pin guide pin bushing, and the bottom shutoff of register pin guide pin bushing is provided with second compression spring between register pin guide pin bushing bottom and the register pin bottom surface; The operating grip bottom surface is provided with dial plate, and the register pin upper end is provided with the oblique tongue that turns clockwise and pass through with dial plate.
Wireway between said multiport valve and the hydrogen fluoride gas colorimetric mechanism is provided with throttling valve.
Said multiport valve is the five-way valve with five connectors, and one of them connector shutoff is a closed condition.
Adopt technique scheme, have following beneficial effect:
1, the external equipment connector of housing is the unique external connector of this ST, is used to vacuumize, operations such as gas sample and appearance gas output detection; Through the rotating operation handle make four interfaces of multiport valve open and close successively with vacuumize, operations such as hydrogen fluoride test, gas washing, sampling, so just realize institutional operations such as hydrogen fluoride gas detection, gas washing and gas sample to sulfur hexafluoride gas.
2, operating grip is rotated to hydrogen fluoride test shelves; Use the test tube handle that the hydrogen fluoride color comparison tube is installed between test tube device and the following test tube device; Can carry out the hydrogen fluoride test jobs, the hydrogen fluoride test jobs is carried out at the realization scene, and the exhaust emissions of hydrogen fluoride color comparison tube is in fixing container (Drexel bottle); Realize nontoxic discharging, concentrate reclaiming clean to handle.
3, constant temperature switch and operating grip are used and vacuumize and the hydrogen fluoride test jobs; Pressure vacuum gauge is measured the vacuum tightness in the sampling jar when vacuumizing, and when vacuumizing operation, need open heating element simultaneously sampling jar and Drexel bottle are heated; Carrying bolt and sampling jar top board play the good supporting effect; Heat-preservation cotton plays the effect into the sampling jar insulation, and temperature sensor plays the effect of perception heating element heating-up temperature, realizes vacuumizing or taking a sample the maintenance temperature constant state.
4, handle is convenient to housing is fetched; Throttling valve plays and in the hydrogen fluoride color comparison tube, charges into the effect that gas keeps constant rate.
5, multiport valve is a five-way valve, and one of them connector is subsequent use connector, and shutoff at ordinary times is a closed condition, and in the time of other wireway shutoff, this connector can use.
6, check device be for prevent to reverse operating grip emit the appearance gas in the sampling jar or take a sample before get into air in the appearance gas cylinder and influence sampling quality; Check device can be pressed non-return button reversing operating grip and directly emit a kind gas to the sampling shelves when the appearance gas that detection is fetched simultaneously.
Compact conformation of the present invention is reasonable, good looking appearance is generous, simple to operate clear, easy to maintenance, use maneuverability, function opposite independent; And provide that the hydrogen fluoride gas color comparison tube detects for oneself, during sampling tensimeter show the pressure of sample gas, function such as auxiliary heating when ST is vacuumized; Acceleration vacuumizes, thoroughly discharges residuals in the ST container; Reaching the real numerical value the same with Primordial Qi of value during sampling, is a rare sampling and experimental facilities.Each wireway and sampling jar inwall are through special inertia Passivation Treatment; Make it that sulfur hexafluoride gas and analyte thereof are not had compatibility and adsorbability after the processing; Thereby guaranteed the time of day of sample, significant to the occasion that is not easy at the scene to carry out the sulfur hexafluoride gas attributional analysis with chromatogram or mass spectrum.The gas that uses in the electrical equipment to use sulfur hexafluoride gas such as isolating switch, transformer, mutual inductor, combined electrical apparatuses is taken a sample and is detected, and also is applicable to the gas that stores in sulfur hexafluoride gas steel cylinder and the gas-holder is taken a sample and detected.
Description of drawings
Fig. 1 is a structural representation of the present invention;
Fig. 2 is an A-A cut-open view in the middle of Fig. 1;
Fig. 3 is the left view of Fig. 1;
Fig. 4 is a B-B cut-open view in the middle of Fig. 3;
Fig. 5 is the longitudinal sectional view at the external equipment connector place of housing of the present invention;
Fig. 6 is a fundamental diagram of the present invention;
Fig. 7 is the structural representation of check device in the middle of the present invention;
Fig. 8 is the right view of Fig. 7;
Fig. 9 is a C-C cut-open view in the middle of Fig. 7;
Figure 10 is a D-D cut-open view in the middle of Fig. 7;
Figure 11 is the structural representation of hydrogen fluoride gas colorimetric mechanism in the middle of the present invention.
Embodiment
Like Fig. 1~shown in Figure 11; The sulfur hexafluoride gas ST comprises the housing with external equipment connector 23 that is provided with on base 1 and the base 1, is provided with Drexel bottle 4, sampling jar 5 in the housing 3 and has the multiport valve 6 of five connectors; A connector shutoff of multiport valve 6 is a closed condition; The housing 3 outer hydrogen fluoride gas colorimetric mechanisms that are provided with, a connector of multiport valve 6 is connected with external equipment connector 2 through wireway 7, and a connector is connected with Drexel bottle 4 through wireway 8; A connector is connected with sampling jar 5 through wireway 9; A connector place is provided with throttling valve 27, and throttling valve 27 is connected with hydrogen fluoride gas colorimetric mechanism through wireway 10, the operating grip 11 that housing 3 outer each connectors that are provided with control multiport valve 6 open and close; Housing 3 tops are provided with the check device 28 that prevents that operating grip 11 from returning automatically, and housing 3 outside portions are provided with handle 29.External equipment connector 2 is located at housing 3 sidepieces with hydrogen fluoride gas colorimetric mechanism; Multiport valve 3 is located at housing 3 inside top; Operating grip 11 is located at housing 3 top outer, and sampling jar 5 is located at housing 3 central authorities, and Drexel bottle 4 is an annular closed cavity; Between housing 3 and sampling jar 5, hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle 4 through a joint short tube 30.
Check device 28 comprises the non-return button 33 that protrudes from housing 3 upper plates 32 respectively and register pin 34, non-return guide pin bushing 35 that is located at upper plate 32 lower surfaces and register pin guide pin bushing 36, be located under the non-return guide pin bushing 35 split pin 37 and two ends are fixedly connected on the non-return connecting link 38 on non-return button 33 and the register pin 34; Non-return button 33 passes non-return guide pin bushing 35 and is connected with split pin 37; Non-return connecting link 38 is between non-return guide pin bushing 35 and split pin 37; Between non-return connecting link 38 and split pin 37, be arranged with first compression spring 39 on the non-return button 33; First compression spring 39 plays non-return connecting link 38 is fixed on the boss of non-return button 33, and register pin 34 bottoms are located in the register pin guide pin bushing 36, the 36 bottom shutoff of register pin guide pin bushing; Be provided with second compression spring 40 between register pin guide pin bushing 36 bottoms and register pin 34 bottom surfaces; Operating grip 11 bottom surfaces are provided with dial plate 41, and register pin 34 upper ends are provided with the oblique tongue 42 that turns clockwise and pass through with dial plate 41, and tiltedly tongue 42 plays the effect that makes dial plate 41 one-directional rotation; Promptly can be when dial plate 41 clockwise rotates along the inclined-plane rotation of oblique tongue 42, tiltedly tongue 42 forms with register pin 34 one manufacturings.
Be provided with pressure vacuum gauge 12 and constant temperature switch 13 in the base 1; The base plate 14 of base 1 is provided with socket 15; Pressure vacuum gauge 12 is connected with sampling jar 5 through a piezometric tube 16 and communicates; Be provided with the heating element 17 of tubular between sampling jar 5 outer walls and Drexel bottle 4 inwalls, heating element 17 is close to the sampling jar outer wall, and the top board 18 of base 1 is bolted with carrying bolt 19; Carrying bolt 19 tops are provided with sampling jar pressing plate 20; Be provided with heat-preservation cotton 21 between sampling jar pressing plate 20 and sampling jar 5 bottoms, be provided with in the heat-preservation cotton 21 and be close to sampling jar 5 bottoms and be used to guarantee vacuumize the temperature sensor 22 that keeps temperature constant state and keep the temperature sensor 31 of temperature constant state with being used to guarantee to take a sample, constant temperature switch 13 is connected with temperature sensor 31 with temperature sensor 22 through lead respectively.
Hydrogen fluoride gas colorimetric mechanism comprises the last test tube device 23 and following test tube device 24 that is fixedly connected with housing 3; Be inserted with hydrogen fluoride color comparison tube 25 between last test tube device 23 and the following test tube device 24, hydrogen fluoride color comparison tube 25 tops are provided with the test tube handle 26 that is used with last test tube device 23.
Last test tube device comprises the upper fixed seat 43 with last vertical through holes and last horizontal pore 54; Be communicated with wireway 10 and last vertical through holes respectively inside and outside the last horizontal pore 54 of upper fixed seat 43; Test tube handle 26 is removably connected with motion bar 45 through jackscrew 44; Last motion bar 45 is plugged in the last vertical through holes of upper fixed seat 43; Be provided with the last gas passage 46 that is communicated with the last horizontal pore 54 of upper fixed seat 43 in the last motion bar 45, last motion bar 45 outer the 3rd compression springs 47 that cooperate with upper fixed seat 43 roof pressures that are arranged with;
Following test tube device comprises the lower fixed seat 48 with following vertical through holes and following horizontal pore 53; Be communicated with Drexel bottle 4 and following vertical through holes respectively inside and outside the following horizontal pore 53 of lower fixed seat 48; Valve inside 50 under being provided with down motion bar 49 in the following vertical through holes of lower fixed seat 48 and being positioned under the motion bar 49; Be provided with the following gas passage 51 that is communicated with the following horizontal pore 53 of lower fixed seat 48 in the following motion bar 49; The vertical section of following gas passage 51 and last gas passage 46 is corresponding up and down to be provided with, following motion bar 49 outer the 4th compression springs 52 that cooperate with lower fixed seat 48 roof pressures that are arranged with.
Operating grip 11 has " hydrogen fluoride test shelves ", " gas washing shelves ", " sampling shelves " and " closing shelves " with clockwise setting; Constant temperature switch 13 has " chromatogram shelves ", " closing shelves " and " vacuumizing shelves "; Temperature sensor 22 is connected with " vacuumizing shelves ", and temperature sensor 31 is connected with " chromatogram shelves ".
Before the sulfur hexafluoride sampling, earlier ST to be vacuumized operation, should make it connect external power supply when ST vacuumizes and carry out auxiliary heating.Concrete steps are following:
(1), external equipment connector 2 usefulness flexible pipes are connected with the air intake opening of vacuum pump and lock, guarantee impermeability;
(2), take out circumscripted power line, an end inserts in supply socket 15, the other end of ST and plugs suitable external power supply;
(3), vacuum pump connects suitable power source, start vacuum pump and move to stable;
(4), slowly open vacuum pump air intake opening switch, connecting line is vacuumized, according to the impermeability of vacuum tightness situation of change inspection connecting line;
(5), constant temperature switch 13 is pulled to " vacuumize shelves ", the 17 pairs of sampling jars of heating element 5 in ST this moment heat with Drexel bottle 4;
(6), then operating grip 11 is threaded to " gas washing " shelves; External equipment connector 2, wireway 7, multiport valve 6, wireway 8 and Drexel bottle 4 are communicated with; Drexel bottle 4 is vacuumized, and when about certain hour final vacuum degree reached regulation, Drexel bottle 4 vacuumized and finishes;
(7), again operating grip is revolved 11 to " sampling " shelves; External equipment connector 2, wireway 7, multiport valve 6, wireway 9 and sampling jar 5 are communicated with, and sampling jar 5 are vacuumized, when pressure vacuum gauge is shown as authorised pressure; Continue to take out a few minutes to vacuum tightness again when dropping to the authorised pressure left and right sides; Then sampling jar 5 vacuumizes and finishes, and then operating grip 11 is rotated to " closing shelves ", closes vacuum pump again;
(8), ST vacuumizes and should external equipment connector 2 be put dustproof pipe cap after qualified, with ST surface wiped clean, and ST is positioned in the suitcase;
(9), application of vacuum finishes, and in time fills in the vacuum pumping release, puts into the clip closed condition.
Vacuumize and can carry out test of hydrogen fluoride gas colorimetric and gas sample operation after operation is accomplished, concrete steps are:
(1) correctly connects the external equipment connector 2 of sample tap to the ST of sulfur hexafluoride electrical equipment, guarantee impermeability;
(2), new hydrogen fluoride color comparison tube 25 is carried out opening and cut off processing;
(3), will be the hydrogen fluoride color comparison tube 25 of opening be installed on test tube device 23 and the following test tube device 24, the direction of arrow of hydrogen fluoride color comparison tube 25 is down during installation.Hydrogen fluoride color comparison tube 25 is disposable, holds mouthful the back successfully and installs and uses, and new hydrogen fluoride color comparison tube 25 need be installed when using at every turn at once;
An end that will not have arrow when (4), hydrogen fluoride color comparison tube 25 is installed is put in down in the gas passage 51; Light downwards pressure of hand; Following motion bar 49 overcomes the elastic force of the 4th spring 52, and following motion bar 49 lower end unseat the valve cores 50 make down gas passage 51 be communicated with Drexel bottle 4;
The another hand upwards gently draws test tube handle 26; Motion bar 45 overcomes the elastic force of the 3rd compression spring 47 in the drive, and hydrogen fluoride color comparison tube 25 is vertically placed, and unclamps test tube handle 26 again; Hydrogen fluoride color comparison tube 25 arrow ends are put in the gas passage 46; Pinching hydrogen fluoride color comparison tube 25 middle part left rotation and right rotation with finger then, that it is aligned is straight, makes air-flow guiding arrow outwardly, and then hydrogen fluoride color comparison tube 25 installs;
(5), operating grip 11 is threaded to " hydrogen fluoride test shelves "; External equipment connector 2, wireway 7, multiport valve 6, wireway 10 and hydrogen fluoride color comparison tube 25 are communicated with; Slowly open external equipment sample tap valve then and kind gas is arranged through getting final product; Throttling valve 27 plays and vacuumizes or gas keeps constant rate under certain pressure when taking a sample effect; Timing is a few minutes approximately, promptly accomplish hydrogen fluoride test (need not carry out the hydrogen fluoride test like the scene of taking a sample, operating grip 11 directly is threaded to " gas washing shelves " and carry out gas washing and get final product);
(6), with operating grip 11 dextrorotations to " gas washing shelves ", after timing some seconds, accomplish gas washing (carried out the hydrogen fluoride test like the scene of taking a sample, need not carry out gas washing, then can directly handle be threaded to the sampling shelves and carry out sampling operation);
(7), (or carrying out hydrogen fluoride test back) behind the gas washing; Operating grip 11 is threaded to " sampling shelves "; When ST upward pressure table shows that the demonstration reading of the electrical equipment upward pressure table of being taken a sample with quilt is identical; 11 dextrorotations of ST operating grip to " close shelves " position, are closed sampling air intake valve on the electrical equipment then, removed the sampling inlet pipe connection;
(8), take behind kind gas ST external interface to be put dust cap, with ST surface wiped clean, be positioned in the suitcase;
(9), gas sample finishes, with the sampling record card of filling in, put into the clip closed condition.
After the sampling, the chamber gas appearance stratographic analysis step that experimentizes is following:
(1), is connected through decompressor in the middle of the external equipment connector 2 that will fill kind gas and the chromatograph interface and locks the assurance impermeability;
(2), the socket of ST 15 connects the 220V power supplys, closed power switch, and constant temperature switch 13 pulled as for " chromatogram shelves " state;
(3), the chromatograph preheating, about about 30 minutes of timing, chromatograph is in normal operating conditions;
(4), press the non-return button 33 of the stratographic analysis indication on the ST; Non-return button 33 moves down through the elastic force that non-return connecting link 38 drive register pins 34 overcome second compression spring 40; Register pin 34 moves down with oblique tongue 42, and when oblique tongue 42 was lower than the dial plate 41 of operating grip 11 bottom surfaces, register pin 34 no longer stopped dial plate 41; So just can operating grip 11 be threaded to counterclockwise " sampling shelves " position, can carry out stratographic analysis;
(5), after the laboratory chromatogram detects and accomplishes; Successively with ST constant temperature switch 13 pull as for " close shelves ", operating grip 11 dextrorotations to " close shelves "; Break off the ST power switch, print and preserve the detection data, close the chromatograph switch at last, stratographic analysis is accomplished;
(6), stratographic analysis should put pipe cap with the ST external interface after finishing, with ST surface wiped clean, be positioned in the suitcase.
The present invention in use should be noted that following item:
(1), connecting tube transpassivation, protective treatment between inner each parts of ST, forbid dust, dirty entering.
(2), keep ST surface clean, clean and tidy, answer wiped clean after each the use, and in time be put in the suitcase.
(3), when ST does not use, external equipment connector 2 should in time put the sealing and dustproof cap, loads onto used hydrogen fluoride color comparison tube 25 at last test tube device 23 and following test tube device 24.
(4), ST belongs to cleaning apparatus, should note waterproof and dustproof and protection against the tide.
(5), ST vacuumizes and the external power supply of should pegging graft when carrying out kind complexion analysis of spectrum, notices that constant temperature switch 13 selects shelves, must not make a mistake and mix up.
(6), ST for a long time not the clean dry nitrogen of time spent application of pure wash, and the nitrogen that charges into the certain pressure clean, dry in the sampling jar is sealed up for safekeeping.
(7),, gas-holder or steel cylinder should take care when being carried out high-pressure sampling.

Claims (10)

1. sulfur hexafluoride gas ST; Comprise the housing that is provided with on base and the base with external equipment connector; It is characterized in that: be provided with Drexel bottle, sampling jar in the said housing and have the multiport valve of four connectors at least; Housing is provided with hydrogen fluoride gas colorimetric mechanism outward; Four connectors of multiport valve are connected with external equipment connector, Drexel bottle, sampling jar and the hydrogen fluoride gas colorimetric mechanism of housing through a wireway respectively, and housing is provided with the operating grip of each connector keying of control multiport valve outward.
2. sulfur hexafluoride gas ST according to claim 1; It is characterized in that: said hydrogen fluoride gas colorimetric mechanism comprises the last test tube device and following test tube device that is fixedly connected with housing; Be inserted with the hydrogen fluoride color comparison tube between last test tube device and the following test tube device, hydrogen fluoride color comparison tube top is provided with the test tube handle that is used with last test tube device.
3. sulfur hexafluoride gas ST according to claim 2; It is characterized in that: the said test tube device of going up comprises the upper fixed seat with last vertical through holes and last horizontal pore; Be communicated with a connector and the last vertical through holes of multiport valve respectively inside and outside the last horizontal pore of upper fixed seat; The test tube handle is removably connected with motion bar through jackscrew; Last motion bar is plugged in the last vertical through holes of upper fixed seat, is provided with the last gas passage that is communicated with the last horizontal pore of upper fixed seat in the last motion bar, and last motion bar is arranged with the 3rd compression spring that cooperates with the upper fixed seat roof pressure outward;
Said test tube device down comprises the lower fixed seat with following vertical through holes and following horizontal pore; Be communicated with Drexel bottle and following vertical through holes respectively inside and outside the following horizontal pore of lower fixed seat; Valve inside under being provided with down motion bar in the following vertical through holes of lower fixed seat and being positioned under the motion bar; Be provided with the following gas passage that is communicated with the following horizontal pore of lower fixed seat in the following motion bar; The vertical section of following gas passage and last gas passage is corresponding up and down to be provided with, and following motion bar is arranged with the 4th compression spring that cooperates with the lower fixed seat roof pressure outward.
4. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs; It is characterized in that: said external equipment connector and hydrogen fluoride gas colorimetric mechanism are located at the housing sidepiece; Multiport valve is located at the case top inboard, and operating grip is located at the case top outside, and sampling jar is located at housing central authorities; Drexel bottle is the toroidal cavity that forms between inner walls and the sampling jar outer wall, and hydrogen fluoride gas colorimetric mechanism lower end is communicated with Drexel bottle.
5. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs; It is characterized in that: be provided with pressure vacuum gauge and constant temperature switch in the said base; The base plate of base is provided with socket; Pressure vacuum gauge is connected with sampling jar through a piezometric tube, is provided with the heating element of tubular between sampling jar outer wall and the Drexel bottle inwall, and the top board of base is bolted with carrying bolt; The carrying bolt top is provided with the sampling jar pressing plate; Sampling jar pressing plate and sampling jar are provided with heat-preservation cotton between the bottom, be provided with in the heat-preservation cotton be close to the sampling jar bottom be used to guarantee to vacuumize or take a sample keep the temperature sensor of temperature constant state, the constant temperature switch is connected with temperature sensor through lead.
6. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs, it is characterized in that: said housing sidepiece is provided with handle.
7. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs, it is characterized in that: said case top is provided with the check device of control operation handle return.
8. sulfur hexafluoride gas ST according to claim 7; It is characterized in that: split pin and two ends that said check device comprises non-return button and the register pin that protrudes from the housing upper plate respectively, the non-return guide pin bushing that is located at the upper plate lower surface and register pin guide pin bushing, be located under the non-return guide pin bushing are fixedly connected on the non-return connecting link on non-return button and the register pin; The non-return button passes the non-return guide pin bushing and is connected with split pin; The non-return connecting link is between non-return guide pin bushing and split pin; Between non-return connecting link and split pin, be arranged with first compression spring on the non-return button; The register pin bottom is located in the register pin guide pin bushing, and the bottom shutoff of register pin guide pin bushing is provided with second compression spring between register pin guide pin bushing bottom and the register pin bottom surface; The operating grip bottom surface is provided with dial plate, and the register pin upper end is provided with the oblique tongue that turns clockwise and pass through with dial plate.
9. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs, it is characterized in that: the wireway between said multiport valve and the hydrogen fluoride gas colorimetric mechanism is provided with throttling valve.
10. according to claim 1 or 2 or 3 described sulfur hexafluoride gas STs, it is characterized in that: said multiport valve is the five-way valve with five connectors, and one of them connector shutoff is a closed condition.
CN 201210002586 2011-02-10 2012-01-06 Sulfur hexafluoride gas sampling device Active CN102564811B (en)

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CN201110035338 2011-02-10
CN201110035338.7 2011-02-10
CN 201210002586 CN102564811B (en) 2011-02-10 2012-01-06 Sulfur hexafluoride gas sampling device

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CN103698162A (en) * 2013-12-25 2014-04-02 国家电网公司 Sulfur hexafluoride gas sampling detection device
CN107831043A (en) * 2017-12-05 2018-03-23 上海新漫传感技术研究发展有限公司 The sampler of tritiated water sampling bottle and tritiated water sampler
CN109297958A (en) * 2018-11-13 2019-02-01 国网四川省电力公司成都供电公司 It is a kind of for monitoring the colour developing prior-warning device of SF6 Electric Power Equipment Insulation gas decomposition product in real time
CN115824303A (en) * 2022-12-02 2023-03-21 苏州搏技光电技术有限公司 High-precision temperature and pressure cavity structure

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CN201575947U (en) * 2009-09-01 2010-09-08 陕西电力科学研究院 Environment-friendly anti-pollution SF6 collection and detection device
CN202485945U (en) * 2011-02-10 2012-10-10 河南省日立信股份有限公司 Sulfur hexafluoride gas sampler

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US4887472A (en) * 1987-12-02 1989-12-19 Douwes Vastgoed B.V. Sampler
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CN103698162A (en) * 2013-12-25 2014-04-02 国家电网公司 Sulfur hexafluoride gas sampling detection device
CN107831043A (en) * 2017-12-05 2018-03-23 上海新漫传感技术研究发展有限公司 The sampler of tritiated water sampling bottle and tritiated water sampler
CN107831043B (en) * 2017-12-05 2024-01-12 上海新漫传感科技有限公司 Tritiated water sampling bottle and sampling device of tritiated water sampler
CN109297958A (en) * 2018-11-13 2019-02-01 国网四川省电力公司成都供电公司 It is a kind of for monitoring the colour developing prior-warning device of SF6 Electric Power Equipment Insulation gas decomposition product in real time
CN115824303A (en) * 2022-12-02 2023-03-21 苏州搏技光电技术有限公司 High-precision temperature and pressure cavity structure
CN115824303B (en) * 2022-12-02 2024-01-16 苏州搏技光电技术有限公司 High-precision temperature and pressure cavity structure

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