CN103114347A - Continuous fiber-manufacturing device - Google Patents

Continuous fiber-manufacturing device Download PDF

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Publication number
CN103114347A
CN103114347A CN2013100740957A CN201310074095A CN103114347A CN 103114347 A CN103114347 A CN 103114347A CN 2013100740957 A CN2013100740957 A CN 2013100740957A CN 201310074095 A CN201310074095 A CN 201310074095A CN 103114347 A CN103114347 A CN 103114347A
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annular
roller
continuous fiber
turning cylinder
liquid
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CN2013100740957A
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CN103114347B (en
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孙道恒
邱小椿
黄少华
吴德志
刘益芳
陈燕君
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Xiamen University
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Xiamen University
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Abstract

The invention discloses a continuous fiber-manufacturing device, relates to an electrostatic spinning device, and provides the fiber-manufacturing device capable of overcoming the shortcomings that liquid supply is not continuous and large in jet flow size difference, and surface solution solidifies and the like, and capable of guaranteeing uniformity of diameters of fiber and continuity of electrospinning nanometer fiber. The continuous fiber-manufacturing device is provided with a motor, a connector, a rotating shaft, an inducing rolling wheel, a needle tip array, an annular liquid-storage groove, a direct-current high-voltage power supply, a collection plate and a liquid-supplying device. An output shaft of the motor is connected with the rotating shaft through the connector. The inducing rolling wheel is connected with the rotating shaft in a rotating mode. Gear rings are arranged on the surface of the inducing rolling wheel. The needle tip array is arranged on the surface of the inducing rolling wheel. Annular racks are arranged inside the annular liquid-storage groove and are meshed with the gear rings of the inducing rolling wheel. The positive electrode of the direct-current high-voltage power supply is connected with an annular solution groove, and the negative of the direct-current high-voltage power supply is connected with the collection plate. The collection plate is arranged above the annular solution groove. The collection plate is grounded. The liquid-supplying device is communicated with the annular liquid-storage groove through a liquid-conveying pipe.

Description

Continuous fiber manufacturing installation
Technical field
The present invention relates to a kind of electrostatic spinning apparatus, especially relate to a kind of continuous fiber manufacturing installation.
Background technology
The characteristics such as simple, with low cost and pure physics stretching that electrostatic spinning possesses skills, the following main flow manufacturing technology that very likely becomes nanofiber.Traditional electrostatic spinning efficient is extremely low, and the commercial Application and the commercialization that have seriously restricted nanofiber are promoted.
Along with the maturation of electrostatic spinning technique and going deep into of nanofiber application study, for low this bottleneck of productive rate, the scientific research personnel has carried out a large amount of correlative studys both at home and abroad, and has made some progress.
Chinese patent CN200720076954.6 discloses a kind of high-performance multineedle electrostatic spinning jet device, this device is the natural expansion to traditional single spraying head, yet through long-term experiment, find that the design of Multi needle spray silk exists that spinning head stops up, electric field influences each other between the spinning head, institute's making alive is higher, spinning quality is poor and need to be to problems such as force (forcing) pumps.Nigeria researcher (O.O.Dosunmu, G.G.Chase, W.Kataphinan, D.H.Reneker.Electrospinning of polymer nanofibres from multiple jets on a porous tubular surface.Nanotechnology2006,17:1123-1127) by antipriming pipe nozzle batch electrospinning, utilize the polymer solution of pneumatic shuttle in will managing slowly outside the extrusion cavities, under the effect of high voltage electric field, produce beam jet be ejected into peripheral around the cylindrical reception of layer of metal online.The method needs air pump to assist feed flow, and structure is comparatively complicated, and has the easy blockage problem of pore.(the Theron A such as Yarin, Zussman E, Yarin A L.Electrostatic field – assisted alignment of electrospun nanofibres.Nanotechnology, 2001,12 (3): 384-390.) the Israel researcher proposes a kind of Dualayer solution system that will contain ferromagnetic fluid and places the in batches technology of electrospinning of magnetic field and electric field realization, although this technology can solve the syringe needle blockage problem, but in polymer solution, sneak into easily impurity, affect fiber quality, but also there are Dualayer solution system operation inconvenience, the problems such as fibre diameter lack of homogeneity.In addition, the ELMARCO company of Czech designs a kind of commercial electrostatic spinning machine Nanospider, this device adopts metal roller to replace traditional needle point shower nozzle, during electrospinning metallic cylinder is immersed in the polymer solution, rotation under the driving of motor causes disturbance to the Free Surface of solution, produces jet, the final nanofiber that obtains, but there is the not shortcoming such as easy to clean of residue in it.
Summary of the invention
The purpose of this invention is to provide a kind ofly overcome that feed flow is discontinuous, the jet size difference is large and surface solution such as solidifies at the shortcoming, can guarantee the continuous fiber manufacturing installation of fibre diameter uniformity and continuous electro-spinning nanofiber.
The present invention is provided with motor, connector, turning cylinder, induces roller, pinpoint array, annular reservoir, DC high-voltage power supply, collecting board and liquid feed device;
Motor output shaft is connected with turning cylinder through connector, induce roller and turning cylinder to be rotationally connected, induce roller surface to be provided with gear ring, pinpoint array is installed on induces roller surface, is provided with annular rack in the annular reservoir, annular rack and described gear ring engagement of inducing roller, DC high-voltage power supply is anodal to be connected with annular solution tank, and the DC high-voltage power supply negative pole is connected with collecting board, and collecting board is located at annular solution tank top, collecting board ground connection, liquid feed device is communicated with annular reservoir by woven hose.
Described motor preferably adopts stepper motor.
Described motor output shaft preferably is positioned on the center line of annular reservoir centre bore, and described turning cylinder preferably is horizontal and is vertical with motor output shaft.
The described roller of inducing preferably is rotationally connected by bearing and turning cylinder, and described gear ring preferably is located at and is induced the roller middle part.
Described pinpoint array is installed on induces roller surface, and preferably each needle point of pinpoint array induces the screwed hole of roller surface to be spirally connected with being located at.
Described pinpoint array can be provided with 4 row's needle points, and all along inducing roller shaft to setting, the interval angle of adjacent 2 row's needle points on same circumference is 90 degree to 4 row's needle points.
Operation principle of the present invention and beneficial effect are as follows:
When device is started working, opening high pressure power supply and adjust to certain voltage (such as 50kV) at first, then starter motor, turning cylinder begins to rotate, and turning cylinder drives induces roller to do circumferential movement; Since induce roller cog with annular reservoir in annular rack engagement, make and induce roller to carry out rotation around the axis of turning cylinder, induce the array needle point on the roller to provoke the polymer solution liquid level this moment, assisted solution overcomes the capillary constraint of free surface, produce taylor cone and under electric field action, form a large amount of jets, moving and the solvent evaporates through the unstability whip is finally at collecting board deposition solid nano fiber.After jet sustained firing a period of time of solution surface, will disappear, for this reason before it disappears, the array needle point will again move to this place or near bring out and produce next jet, so go round and begin again, but the continuous electro-spinning nanofiber.Because described roller and the needle point of inducing is small-sized, the distance of needle point and collecting board is little with liquid level and collecting board spacing difference, and a small amount of formed fiber of jet is basic identical with the fibre diameter of liquid level generation on the array needle point so; Induce simultaneously roller inducing the formation jet process less to the electric field interference, guaranteed the uniformity of fibre diameter.In addition, liquid feed device for annular solution tank provides solution, remains unchanged the liquid level of solution in the annular solution tank by woven hose, has realized the continous-stable manufacturing of fiber.
Description of drawings
Fig. 1 is the structural representation of the embodiment of the invention.
Fig. 2 is the turning cylinder in the embodiment of the invention and induces the roller structure schematic diagram.
Fig. 3 is the use view of the embodiment of the invention.
The specific embodiment
Referring to Fig. 1 and 2, the embodiment of the invention is provided with stepper motor 1, connector 2, turning cylinder 3, induces roller 4, pinpoint array 5, annular reservoir 6, annular rack 7, DC high-voltage power supply 8, collecting board 9 and liquid feed device 10.
Stepper motor 1 output shaft is connected with turning cylinder 3 through connector 2, induces roller 4 and turning cylinder 3 to be rotationally connected.Pinpoint array 5 is installed on induces roller 4 surfaces, each needle point of pinpoint array 5 be located at the screwed hole (not drawing among Fig. 1 and 2) of inducing roller 4 surfaces and be spirally connected.Induce roller 4 to be made of inducer 41,2 ball bearings 42, sleeve 43 and snap rings 44, inducer 41 middle parts are provided with gear ring 45.Ball bearing 42 inner rings and turning cylinder 3 interference fit, induce roller 4 left and right sides axially fixing by the shaft shoulder, sleeve 43 and the snap ring 44 of turning cylinder 3, inducer 41 and ball bearing 42 outer ring interference fit, ball bearing 42 is by snap ring 44 restrictions, and sleeve 43 is rotatably assorted with turning cylinder 3.Take gear ring 45 as benchmark, described pinpoint array 5 is along inducing roller 4 axially to be symmetrically arranged with 4 row's needle points, and the interval angle of adjacent 2 row's needle points on same circumference is 90 degree (namely 4 row's needle points are the cross setting).
Be provided with annular rack 7 in the annular reservoir 6, annular rack 7 is connected with annular reservoir 6 with gear ring 42 engagements, DC high-voltage power supply 8 positive poles, and DC high-voltage power supply 8 negative poles are connected with collecting board 9, and collecting board 9 is located at annular reservoir 6 tops, collecting board 9 ground connection.Liquid feed device 10 is communicated with annular reservoir 6 by woven hose 101.
Described stepper motor 1 output shaft is positioned on the center line of annular reservoir 6 centre bores, and described turning cylinder 3 is horizontal and is vertical with stepper motor 1 output shaft.
Referring to Fig. 1 and Fig. 3, when electronic 1 machine of stepping rotated, the connection by connector 2 drove turning cylinder 3 and moves in a circle around annular reservoir 6 centers of circle, drives simultaneously and induces roller 4 to move in a circle.Owing to induce gear ring 45 and 7 engagements of the annular rack in the annular reservoir 6 of roller 4, therefore induce roller 4 in moving axis 3 revolution that rotate, also to carry out rotation.Be installed in the needle point battle array 5 of inducing on the roller 4 and continuously carry out inducing solution Surface Creation jet according to path and the motion mode of inducer.Polymer solution in the annular reservoir 7 forms nanofiber in collecting board 9 under the effect of pinpoint array 5 electric fields.Arrow among Fig. 3 represents the direction that rotating shaft 3 moves in a circle around annular reservoir 6 centers of circle.Sweep among Fig. 3 represents the nanofiber jet.
During practical application, needle point quantity and the arrangement mode of pinpoint array 5 can arrange as required, preferably are single arrangement, and the spacing of each needle point is suitable, can reduce the phase mutual interference between the initial jet.

Claims (6)

1. continuous fiber manufacturing installation is characterized in that being provided with motor, connector, turning cylinder, induces roller, pinpoint array, annular reservoir, DC high-voltage power supply, collecting board and liquid feed device;
Motor output shaft is connected with turning cylinder through connector, induce roller and turning cylinder to be rotationally connected, induce roller surface to be provided with gear ring, pinpoint array is installed on induces roller surface, is provided with annular rack in the annular reservoir, annular rack and described gear ring engagement of inducing roller, DC high-voltage power supply is anodal to be connected with annular solution tank, and the DC high-voltage power supply negative pole is connected with collecting board, and collecting board is located at annular solution tank top, collecting board ground connection, liquid feed device is communicated with annular reservoir by woven hose.
2. continuous fiber manufacturing installation as claimed in claim 1 is characterized in that described motor adopts stepper motor.
3. continuous fiber manufacturing installation as claimed in claim 1 is characterized in that described motor output shaft is positioned on the center line of annular reservoir centre bore, and described turning cylinder is horizontal and is vertical with motor output shaft.
4. continuous fiber manufacturing installation as claimed in claim 1 is characterized in that the described roller of inducing is rotationally connected by bearing and turning cylinder, and described gear ring is located at and is induced the roller middle part.
5. continuous fiber manufacturing installation as claimed in claim 1 is characterized in that described pinpoint array is installed on to induce roller surface, is that each needle point of pinpoint array induces the screwed hole of roller surface to be spirally connected with being located at.
6. continuous fiber manufacturing installation as claimed in claim 5 is characterized in that pinpoint array is provided with 4 row's needle points, and 4 row's needle points are all along inducing roller shaft to setting, and adjacent 2 to arrange the interval angle of needle points on same circumference be 90 to spend.
CN201310074095.7A 2013-03-08 2013-03-08 Continuous fiber-manufacturing device Expired - Fee Related CN103114347B (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103757719A (en) * 2014-02-12 2014-04-30 厦门大学 Fiber felt manufacturing device
CN104313705A (en) * 2014-09-29 2015-01-28 中鸿纳米纤维技术丹阳有限公司 Novel nanofiber electrostatic spinning machine
CN104887282A (en) * 2015-05-25 2015-09-09 东华大学 Vascular repair device
CN104911721A (en) * 2015-07-06 2015-09-16 苏州大学 Electrostatic spinning device for producing nanofiber in batches
CN106119994A (en) * 2016-09-02 2016-11-16 天津工业大学 A kind of nonmetal rotating shaft being easy to power up
CN108642577A (en) * 2018-05-29 2018-10-12 巢湖学院 A kind of liquid level induction electrostatic spinning apparatus
WO2022126818A1 (en) * 2020-12-15 2022-06-23 苏州大学 Rolling-type electrostatic spinning device with sawtooth grooves and gear
CN115386971A (en) * 2022-09-05 2022-11-25 广东石油化工学院 Stepping ratchet electrostatic spinning device and using method thereof

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005024101A1 (en) * 2003-09-08 2005-03-17 Technicka Univerzita V Liberci A method of nanofibres production from a polymer solution using electrostatic spinning and a device for carrying out the method
CN1888154A (en) * 2006-07-24 2007-01-03 厦门大学 Polymer nano fiber batch spurting device
CN101189368A (en) * 2005-06-07 2008-05-28 埃尔马科有限公司 A method and device for production of nanofibres from the polymeric solution through electrostatic spinning
WO2009156822A1 (en) * 2008-06-24 2009-12-30 Stellenbosch University Method and apparatus for the production of fine fibres
TWM393520U (en) * 2010-01-25 2010-12-01 Yi-An Teng The screw spinning device for the electrostatic spinning apparatus
CN203080121U (en) * 2013-03-08 2013-07-24 厦门大学 Continuous fibre manufacturing device

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2005024101A1 (en) * 2003-09-08 2005-03-17 Technicka Univerzita V Liberci A method of nanofibres production from a polymer solution using electrostatic spinning and a device for carrying out the method
CN101189368A (en) * 2005-06-07 2008-05-28 埃尔马科有限公司 A method and device for production of nanofibres from the polymeric solution through electrostatic spinning
CN1888154A (en) * 2006-07-24 2007-01-03 厦门大学 Polymer nano fiber batch spurting device
WO2009156822A1 (en) * 2008-06-24 2009-12-30 Stellenbosch University Method and apparatus for the production of fine fibres
TWM393520U (en) * 2010-01-25 2010-12-01 Yi-An Teng The screw spinning device for the electrostatic spinning apparatus
CN203080121U (en) * 2013-03-08 2013-07-24 厦门大学 Continuous fibre manufacturing device

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103757719A (en) * 2014-02-12 2014-04-30 厦门大学 Fiber felt manufacturing device
CN103757719B (en) * 2014-02-12 2015-11-11 厦门大学 A kind of fibrofelt preparation facilities
CN104313705A (en) * 2014-09-29 2015-01-28 中鸿纳米纤维技术丹阳有限公司 Novel nanofiber electrostatic spinning machine
CN104313705B (en) * 2014-09-29 2017-05-24 中鸿纳米纤维技术丹阳有限公司 Nanofiber electrostatic spinning machine
CN104887282A (en) * 2015-05-25 2015-09-09 东华大学 Vascular repair device
CN104911721A (en) * 2015-07-06 2015-09-16 苏州大学 Electrostatic spinning device for producing nanofiber in batches
CN106119994A (en) * 2016-09-02 2016-11-16 天津工业大学 A kind of nonmetal rotating shaft being easy to power up
CN106119994B (en) * 2016-09-02 2018-05-01 天津工业大学 A kind of nonmetallic shaft easy to power-up
CN108642577A (en) * 2018-05-29 2018-10-12 巢湖学院 A kind of liquid level induction electrostatic spinning apparatus
WO2022126818A1 (en) * 2020-12-15 2022-06-23 苏州大学 Rolling-type electrostatic spinning device with sawtooth grooves and gear
CN115386971A (en) * 2022-09-05 2022-11-25 广东石油化工学院 Stepping ratchet electrostatic spinning device and using method thereof

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Inventor after: Huang Shaohua

Inventor after: Sun Daoheng

Inventor after: Wu Dezhi

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