CN103284368A - Blended flame-retardant fabric and flame-retardant protecting clothes - Google Patents
Blended flame-retardant fabric and flame-retardant protecting clothes Download PDFInfo
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- CN103284368A CN103284368A CN2013101755786A CN201310175578A CN103284368A CN 103284368 A CN103284368 A CN 103284368A CN 2013101755786 A CN2013101755786 A CN 2013101755786A CN 201310175578 A CN201310175578 A CN 201310175578A CN 103284368 A CN103284368 A CN 103284368A
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Abstract
The invention discloses blended flame-retardant fabric and flame-retardant protecting clothes. The blended flame-retardant fabric comprises the following components, by weight, 10-40 parts of flame-retardant vinylon fibers, 10-40 parts of high-temperature resistant fibers, 10-20 parts of poly (aryl-oxadiazole) fibers and 20-40 parts of flame-retardant viscose. The blended flame-retardant fabric is weaved by a normal method after the components are blended. The flame-retardant fabric is high in flame retardant property, moisture penetrability, air permeability and abrasive resistance.
Description
Technical field
The present invention relates to a kind of fabric and protective garment, relate in particular to a kind of blending fire retardant fabric and fire retardant protective clothing.
Background technology
Fire fighter, emergency response personnel, racing car personnel, army personnel, industrial production personnel are exposed in flame or the high temperature through regular meeting; the protective garment that they need or protective article are except can be high temperature resistant; also needing can be more wear-resisting; simultaneously because violent motion and the high temperature occasion of human body makes the amount of sweat of human body discharge at double, so a kind of heat-resistant fireproof fabric with functions such as comfortableness, poisture-penetrability, gas permeability, elimination peculiar smell receives an acclaim especially.
Summary of the invention
At the deficiencies in the prior art, one of technical problem to be solved by this invention provides a kind of blending fire retardant fabric.
Two of technical problem to be solved by this invention provides a kind of fire retardant protective clothing.
Technical problem to be solved by this invention is achieved by the following technical solution:
A kind of blending fire retardant fabric forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part.
A kind of blending fire retardant fabric forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part;
Ju Fang oxadiazole fiber 10-20 part.
A kind of blending fire retardant fabric forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part;
Ju Fang oxadiazole fiber 10-20 part;
FRC 20-40 part.
Wherein,
Described high-temperature fibre is a kind of or its mixture in polysulphonamide fiber and the aramid fiber 1313 fiber.
Described FRC, adopt following method to be prepared from: fire retardant is mixed with viscose solution, and wet spinning spray silk technological forming can make described FRC routinely;
Described fire retardant accounts for the quality percentage composition 5-15% of described FRC;
Described fire retardant is made up of following components in mass portion: N, N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide 20-40 part; N-methylol-3-(dimethoxy phosphono) propionamide 20-40 part; Three (2,3-dibromopropyl) fulminuric acid ester 30-50 part.
Preferably, in the described viscose solution, the weight percent content of first fibre is 8-9%, and the weight percent content of NaOH is 4-6%, falling ball viscosity 45-65 second, degree of ripeness 8-16%.
The present invention also provides a kind of fire retardant protective clothing, and its material is above-mentioned blending fire retardant fabric.
Concrete, in the present invention:
Described flame vinylon fiber, it is the compound that contains anti-flaming function element (halogen, phosphorus, nitrogen etc.) by grafting on the big molecule of polyvinyl alcohol (PVA), or by after adding the fire retardant blend, carry out technical process such as solution spinning, stretching, heat treatment and formalizing and make fire-retardant polyvinyl.Main fire-retardant polyvinyl kind has at present: dimension polyvinyl chloride fibre, CY841 fiber (trade name of the fire-retardant polyvinyl of decabromodiphenyl oxide/antimony), high-strength fire-retarding polyvinyl (TDE fire-retardant high-strength polyvinyl), high-strength halogen-free flameproof polyvinyl (fire retardant: the DDPS fire resistance fibre).
Be example with the CY841 fiber, this fiber utilization decabromodiphenyl oxide and antimony oxide are made fire retardant, adopt common wet spinning to produce fire-retardant polyvinyl; The fire-retardant polyvinyl of deca-BDE is compared with common polyvinyl, and its core-skin layer architectural difference is less, and fire retardant is dispersed in the fiber with granular form, and its continuous phase is PVA, is the less fire resistance fibre of epidermal area fire retardant.
Described high-temperature fibre mainly comprises polysulphonamide fiber and aramid fiber 1313 fiber.
Described polysulphonamide fiber claims polysulfonamides fibre again, is called for short the PSA fiber, commodity special peace synthetic fibre (TANLON) by name.Virtue sulfone synthetic fibre is a kind of aromatic polyamide fibre with special construction, and formal name used at school is PPSU terephthalamide fiber, and this fiber is by 4,4'-DADPS, and the condensation polymer of 3,3'-DADPS and paraphthaloyl chloride is made.Polysulphonamide fiber has been introduced benzene structure and sulfuryl when producing, and makes amide groups and sulfuryl interconnect contraposition phenyl and a position phenyl formation linear macromolecule.Since exist on the macromolecular main chain strong electrophilic sulfuryl group-(SO2)-, two keys by phenyl ring are gripped effect altogether, by the system of gripping altogether of phenyl ring, make that the cloud density of nitrogen-atoms significantly reduces on the amide groups, so have outstanding heat-resisting, firing resistance, its long-term serviceability temperature is 250 ℃.The experiment proved that the hear resistance of polysulphonamide fiber, high temperature dimensional stability, chemical resistance, hygroscopicity and dyeability are all comparatively good.The polysulphonamide fiber material is applied to fields such as protective article, high-temperature-resistant filtering material, friction sealed material, electrically insulating material more.
Described aramid fiber 1313 fiber claims again: Fanglun 1313; Polyisophthaloyl metaphenylene diamine fibre; Fanglun1313 is formed by the solution spinning by m-phenylene diamine (MPD) and m-phthaloyl chloride polycondensation, and its characteristics gas permeability, poisture-penetrability are good, heat-resisting quantity, anti-flammability, anti-most corrosion.
Described Ju Fang oxadiazole fiber is called for short POD, English name: Poly-1, and 3,4-oxadiazole is a kind of high temperature resistant aromatic heterocycle polymer material that possesses good thermal stability, chemical stability, electrical insulating property etc.Have low flame shrinkage, can provide extra heat endurance for spun yarn, Ju Fang oxadiazole fiber refers to the fiber that the polymer by Bao Han oxadiazole unit constitutes.The method of the poly-fragrant oxadiazole fiber of preparation can be referring to U.S.'s granted patent 4202962, and commodity are called the Powerleader synthetic fibre.
Described FRC has good flame retardant effect, has the characteristics that are similar to natural cotton fiber simultaneously, and this material has gone out to have outside the enhancing dress ornament comfort property, also has good natural antistatic effect.Present Austrian Lenzin company and Chinese Jilin chemical fibre, Tangshan three friendly chemical industry, Shandong sea otter etc. have this fiber production.
Described FRC, adopt following method to be prepared from: fire retardant is mixed with viscose solution, and wet spinning spray silk technological forming can make described FRC routinely;
Described fire retardant accounts for the quality percentage composition 5-15% of described FRC;
Described fire retardant is made up of following components in mass portion: N, N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide 20-40 part; N-methylol-3-(dimethoxy phosphono) propionamide 20-40 part; Three (2,3-dibromopropyl) fulminuric acid ester 30-50 part.
Described viscose solution refers to the sodium hydrate aqueous solution of cellulose sulfonate, and it is the general intermediate raw material of the industry.
Preferably, in the described viscose solution, the weight percent content of first fibre is 8-9%, and the weight percent content of NaOH is 4-6%, falling ball viscosity 45-65 second, degree of ripeness 8-16%.
Blending fire retardant fabric of the present invention can mix each component earlier originally, adopted industry universal method to make blended yarns, adopted conventional method to weave blended yarns again and formed.
Described blending fire retardant fabric includes but not limited to Woven fabric or knit goods.General Fabric Design and structure are well known to those skilled in the art.
Wherein, described Woven fabric refers to, usually passing through radially or the broadwise interwoven yarns that loom forms, and make yarn fill each other or interweave to form any fabric tissue (as plain weave, the crowfoot knit, square plain weave, satin face are knitted, twill weave etc.) fabric.Wherein plain weave and twill weave are the tissues of normal use in the commerce, and preferred in many embodiments.
Described knit goods refers to, passes through the fabric that uses pin that the yarn coil interconnection is formed usually.In many cases, for making knit goods, short fiber is fed into yarn is transformed in the knitting machine of fabric.If desired, can provide plying or not many warps or the yarn of plying in the knitting machine; Routine techniques is, is encased in a branch of yarn or a branch of doubled yarn in the knitting machine simultaneously and is knitted into fabric, or directly be knitted into the clothing goods.
Blending fire retardant fabric of the present invention has higher fire resistance, and poisture-penetrability height, gas permeability height and wearability are strong.
Surprisingly, in the present invention, further blending adds poly-fragrant oxadiazole fiber on the basis of flame vinylon fiber and high-temperature fibre, and Synergistic has further improved fire resistance and the anti-wear performance of product.
Can also add FRC in the blending fire retardant fabric of the present invention, can effectively improve the wearability of fabric, fabric is soft, and wearability is good.Especially, adopt the FRC of the special preparation of the present invention, with respect to the FRC of prior art, the flame retardant effect of blending fire retardant fabric is more excellent.
Blending fire retardant fabric of the present invention can use conventional dyestuff to dye.
Blending fire retardant fabric of the present invention can be applied in protective garment or other protective articles, especially personnel's such as fire fighter, emergency response personnel, racing car personnel, army personnel, industrial production protective garment or other protective articles, when high temperature resistant, anti-wear performance is outstanding, can prolong the service life of protective garment or other protective articles, the cost performance height.
The specific embodiment
Be further described below in conjunction with the present invention of embodiment.
Among the following embodiment, each raw material basic condition is introduced, and sees the following form 1.
Table 1: stock chart
| Material name | Concrete commodity | Oxygen index (OI), the LOI value |
| Flame vinylon fiber | CY841 fiber (SINOPEC Sichuan Vinylon Factory provides) | 31.4 |
| High-temperature fibre | (Shanghai Tanlon Fibre Co., Ltd. provides the PSA fiber, trade name: TANLON) | 33 |
| High-temperature fibre | (du pont company provides the aramid fiber 1313 fiber, trade name: Nomex) | 29.3 |
| Ju Fang oxadiazole fiber | (Jiangsu Powerleader new material Co., Ltd provides trade name to the POD fiber: the Powerleader synthetic fibre) | 30.5 |
Embodiment 1
Take by weighing each raw material by corresponding embodiment 1 data of table 2, mix, the shredding preliminary treatment is carded to the carded sliver at carding machine; Again on drawing frame and close and make ripe; Carry out drawing-off and twisting at fly frame, mixed yarn is made in further draw twisting on spinning frame at last, and yarn linear density is 39tex.Again mixed yarn is adopted large circle machine weft knitting method for weaving to weave, weft-knitted rib construction, gross density is (100 stringer * 60 lines)/5cm, finally makes the blending fire retardant fabric.
Table 2: textile component list weight: kilogram
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 |
| The CY841 fiber | 25 | 25 | 25 | 25 | 25 | 25 |
| The PSA fiber | 25 | 25 | 25 | / | / | / |
| The aramid fiber 1313 fiber | / | / | / | 25 | 25 | 25 |
| The POD fiber | / | 15 | 15 | 15 | 15 | / |
| FRC | / | / | 30 | / | 30 | / |
Embodiment 2
Take by weighing each raw material according to corresponding embodiment 2 data in the table 2, adopt embodiment 1 described method to prepare the blending fire retardant fabric.
Embodiment 3
Take by weighing each raw material according to corresponding embodiment 3 data in the table 2, adopt embodiment 1 described method to prepare the blending fire retardant fabric.Wherein, described raw material FRC is selected from the An Fusai fire resistance fibre that Shandong Hailong Co., Ltd. provides, trade name: Anti-fcell, oxygen index (OI), LOI value 31.2.
Embodiment 4
Take by weighing each raw material according to corresponding embodiment 4 data in the table 2, adopt embodiment 1 described method to prepare the blending fire retardant fabric.
Embodiment 5
Take by weighing each component according to embodiment 5 data corresponding in the table 2, adopt embodiment 1 described method to prepare the blending fire retardant fabric.Wherein, described raw material FRC is selected from the An Fusai fire resistance fibre that Shandong Hailong Co., Ltd. provides, trade name: Anti-fcell, oxygen index (OI), LOI value 31.2.
Embodiment 6
Take by weighing each raw material according to corresponding embodiment 6 data in the table 2, adopt embodiment 1 described method to prepare the blending fire retardant fabric.
Embodiment 7
Take by weighing N, 30 kilograms of N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide; N-methylol-3-(dimethoxy phosphono) propionamide is 30 kilograms; 40 kilograms of three (2,3-dibromopropyl) fulminuric acid esters mix and make composite flame-retardant agent.
Above-mentioned composite flame-retardant agent is mixed with viscose solution, and wet spinning spray silk technological forming can make described FRC routinely, and the length of FRC is 38mm.Wherein, the content of fire retardant is 10wt% in the control finished product FRC.
Viscose solution in the described raw material, the weight percent content of first fibre are 8.5%, and the weight percent content of NaOH is 5%, falling ball viscosity 50 seconds, degree of ripeness 12%.
The oxygen index (OI) LOI value that records this FRC is 32.4%.
Take by weighing CY841 fiber 25 weight portions, PSA fiber 25 weight portions, POD fiber 15 weight portions, the above-mentioned FRC that makes 30 weight portions mix, and the shredding preliminary treatment is carded to the carded sliver at carding machine; Again on drawing frame and close and make ripe; Carry out drawing-off and twisting at fly frame, mixed yarn is made in further draw twisting on spinning frame at last, and yarn linear density is 39tex.Again mixed yarn is adopted large circle machine weft knitting method for weaving to weave, weft-knitted rib construction, gross density is (100 stringer * 60 lines)/5cm, finally makes the blending fire retardant fabric.
Embodiment 8
With N, N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide mixes with viscose solution, and wet spinning spray silk technological forming can make described FRC routinely, and the length of FRC is 38mm.Wherein, the content of fire retardant is 10wt% in the control finished product FRC.
Viscose solution in the described raw material, the weight percent content of first fibre are 8.5%, and the weight percent content of NaOH is 5%, falling ball viscosity 50 seconds, degree of ripeness 12%.
The oxygen index (OI) LOI value that records this FRC is 31.4%.
Take by weighing CY841 fiber 25 weight portions, PSA fiber 25 weight portions, POD fiber 15 weight portions, the above-mentioned FRC that makes 30 weight portions mix, and the shredding preliminary treatment is carded to the carded sliver at carding machine; Again on drawing frame and close and make ripe; Carry out drawing-off and twisting at fly frame, mixed yarn is made in further draw twisting on spinning frame at last, and yarn linear density is 39tex.Again mixed yarn is adopted large circle machine weft knitting method for weaving to weave, weft-knitted rib construction, gross density is (100 stringer * 60 lines)/5cm, finally makes the blending fire retardant fabric.
Embodiment 9
With N-methylol-3-(dimethoxy phosphono) propionamide mixes with viscose solution, and a wet spinning spray silk technological forming can make described FRC routinely, and the length of FRC is 38mm.Wherein, the content of fire retardant is 10wt% in the control finished product FRC.
Viscose solution in the described raw material, the weight percent content of first fibre are 8.5%, and the weight percent content of NaOH is 5%, falling ball viscosity 50 seconds, degree of ripeness 12%.
The oxygen index (OI) LOI value that records this FRC is 31.2%.
Take by weighing CY841 fiber 25 weight portions, PSA fiber 25 weight portions, POD fiber 15 weight portions, the above-mentioned FRC that makes 30 weight portions mix, and the shredding preliminary treatment is carded to the carded sliver at carding machine; Again on drawing frame and close and make ripe; Carry out drawing-off and twisting at fly frame, mixed yarn is made in further draw twisting on spinning frame at last, and yarn linear density is 39tex.Again mixed yarn is adopted large circle machine weft knitting method for weaving to weave, weft-knitted rib construction, gross density is (100 stringer * 60 lines)/5cm, finally makes the blending fire retardant fabric.
Embodiment 10
Three (2,3-dibromopropyl) fulminuric acid ester is mixed with viscose solution, and wet spinning spray silk technological forming can make described FRC routinely, and the length of FRC is 38mm.Wherein, the content of fire retardant is 10wt% in the control finished product FRC.
Viscose solution in the described raw material, the weight percent content of first fibre are 8.5%, and the weight percent content of NaOH is 5%, falling ball viscosity 50 seconds, degree of ripeness 12%.
The oxygen index (OI) LOI value that records this FRC is 30.8%.
Take by weighing CY841 fiber 25 weight portions, PSA fiber 25 weight portions, POD fiber 15 weight portions, the above-mentioned FRC that makes 30 weight portions mix, and the shredding preliminary treatment is carded to the carded sliver at carding machine; Again on drawing frame and close and make ripe; Carry out drawing-off and twisting at fly frame, mixed yarn is made in further draw twisting on spinning frame at last, and yarn linear density is 39tex.Again mixed yarn is adopted large circle machine weft knitting method for weaving to weave, weft-knitted rib construction, gross density is (100 stringer * 60 lines)/5cm, finally makes the blending fire retardant fabric.
Test case
The fabric that embodiment 1-10 is obtained carries out performance test respectively.
Table 3: fabric performance test table
The embodiment of the invention 1 adopts flame vinylon fiber and high-temperature fibre PSA fiber to carry out blend, and obtained fabric has higher fire resistance, oxygen index (OI) LOI value 32.2%.In the embodiment of the invention 2, further blending adds poly-fragrant oxadiazole fiber (oxygen index (OI) LOI value 30.5%) on the basis of embodiment 1, the fabric oxygen index (OI) LOI value 32.6% that makes, the oxygen index (OI) LOI value and the Ju Fang oxadiazole fiber that are higher than embodiment 1, as seen three kinds of fiber Synergistics have further improved fire resistance, anti-wear performance, gas permeability and the poisture-penetrability of product.
Need to prove in addition, the raw material of embodiment 7-10 and embodiment 3 form and the preparation method identical, unique difference is the FRC difference that adopts.
And the unique difference between embodiment 7-10 is used fire retardant difference in the FRC preparation process.Embodiment 8-10 adopts single fire retardant, and embodiment 7 adopts the composite of the used fire retardant of embodiment 8-10.
The present invention is by carrying out the blending method flame-proof treatment to viscose rayon; make the FRC of preparation have fire resistance preferably; again with other fiber blends after; the fabrics flame resistance effect that makes is better; especially, with N, N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide, N_ methylol-3-(dimethoxy phosphono) propionamide and three (2; the 3-dibromopropyl) these three kinds of composite uses of fire retardant of fulminuric acid ester, the flame retardant effect Synergistic.
The above; it only is the specific embodiment of the present invention; but protection scope of the present invention is not limited thereto; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; variation or the replacement that can expect without creative work all should be encompassed within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (7)
1. a blending fire retardant fabric is characterized in that, forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part.
2. a blending fire retardant fabric is characterized in that, forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part;
Ju Fang oxadiazole fiber 10-20 part.
3. a blending fire retardant fabric is characterized in that, forms by adopting conventional method to weave after the following components by part by weight blend:
Flame vinylon fiber 10-40 part;
High-temperature fibre 10-40 part;
Ju Fang oxadiazole fiber 10-20 part;
FRC 20-40 part.
4. as each described blending fire retardant fabric among the claim 1-3, it is characterized in that: described high-temperature fibre is a kind of or its mixture in polysulphonamide fiber and the aramid fiber 1313 fiber.
5. blending fire retardant fabric as claimed in claim 3 is characterized in that, described FRC adopts following method to be prepared from: fire retardant is mixed with viscose solution, routinely wet spinning spray silk technological forming;
Described fire retardant accounts for the quality percentage composition 5-15% of described FRC;
Described fire retardant is made up of following components in mass portion: N, N '-two (two phenoxy group thiophosphoryl bases) dithiothyldimaide 20-40 part; N-methylol-3-(dimethoxy phosphono) propionamide 20-40 part; Three (2,3-dibromopropyl) fulminuric acid ester 30-50 part.
6. blending fire retardant fabric as claimed in claim 5 is characterized in that, in the described viscose solution, the weight percent content of first fibre is 8-9%, and the weight percent content of NaOH is 4-6%, falling ball viscosity 45-65 second, degree of ripeness 8-16%.
7. fire retardant protective clothing, it is characterized in that: the material of described fire retardant protective clothing is each described blending fire retardant fabric among the claim 1-6.
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Application publication date: 20130911 |