CN105017971A - Artificial quartz stone polishing agent and preparation method therefor - Google Patents
Artificial quartz stone polishing agent and preparation method therefor Download PDFInfo
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- CN105017971A CN105017971A CN201510410984.5A CN201510410984A CN105017971A CN 105017971 A CN105017971 A CN 105017971A CN 201510410984 A CN201510410984 A CN 201510410984A CN 105017971 A CN105017971 A CN 105017971A
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- artificial quartz
- polishing
- oxide
- oxalic acid
- sodium oxalate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
The invention discloses an artificial quartz stone polishing agent and a preparation method therefor. The artificial quartz stone polishing agent is prepared from the raw materails comprising silicon oxide, carborundum, tin oxide, iron oxide, calcium fluoride and a solution in a mass ratio of (15-25) to (15-25) to (5-10) to (5-10) to (25-35) to (25-35), wherein the solution is prepared from oxalic acid, sodium oxalate and water. The artificial quartz stone polishing agent disclosed by the invention is used for polishing artificial quartz stones, has the advantages such as high polishing efficiency, good glossiness after polishing, which is improved by more than 10% in comparison with that of a conventional marble polishing agent, and the like, and has a very good application value.
Description
Technical field
The present invention relates to grinding, polishing tool technical field, be specifically related to a kind of artificial quartz in lump rumbling compound and preparation method thereof.
Technical background
Stone material is a kind of finishing material very popular at present, due to the chemical and physical properties of material itself, thus it in use there will be the change of color and luster and gloss, simultaneously, also there will be wearing and tearing, the phenomenon such as damaged and contaminated, finally cause the decorative effect of stone material to decline.Stone material is remained, and desirable gloss and color are the important contents that people evaluate stone decoration effect maintenance degree.Grinding and polishing after stone material installation can remove the trickle cut of stone surface, the defects such as watermark, effectively improves the gloss of stone material, makes the limpid light of stone material.
For stone polishing mechanism, there is no final conclusion in the industry, but totally belong to the category of chemically machinery polished (CMP).Polishing powder is as glass, and the polishing material in jewel and marble industry belongs to traditional Application Areas.At present, study more polishing material mainly with the oxide cmp agent that cerium oxide, silicon oxide, zirconium white, diamond etc. are main raw material(s), and the composite modified rumbling compound of oxide compound.In addition, the chromic oxide for jewel and kaolinite great soil group rumbling compound is also had.But these rumbling compound materials all need to carry out modification to oxide surface, and need by high―temperature nuclei, preparation process is complicated, cost is high.In addition, domestic many experts had once done some useful work to the polishing problem of stone material, summed up and had four classes to marmorean finishing method: i.e. felt---aluminum oxide polishing processes; Felt---oxalic acid polishing processes; Abrading block polishing processes; Containing oxalic acid abrading block polishing processes.But substantially blank is in for the polishing research of the hard such as grouan, quartzite stone material.
At present, no matter be domestic or external for marmorean polishing, all done large quantity research, after polishing, the glossiness of stone material is high.But for this kind of hard stone material of artificial quartz in lump, use marble polishing agent, polishing efficiency and glossiness effect are all weak.
Summary of the invention
The object of the invention is to overcome the problem that existing marble polishing agent is not suitable for rotten-stone diamond stone, provide that a kind of polishing efficiency is high, glossiness is good after polishing artificial quartz in lump rumbling compound.
Another object of the present invention is the preparation method providing above-mentioned artificial quartz in lump rumbling compound.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
A kind of artificial quartz in lump rumbling compound, is raw material by silicon oxide, silicon carbide, stannic oxide, ferric oxide, Calcium Fluoride (Fluorspan) and oxalic acid-sodium oxalate solution, makes according to the mass ratio of 15 ~ 25:15 ~ 25:5 ~ 10:5 ~ 10:25 ~ 35:25 ~ 35; Described oxalic acid-sodium oxalate solution is dissolved in 100ml water formulated by 0.8g oxalic acid and 2.4g sodium oxalate
Wherein, during the present invention is raw materials used, silicon oxide, silicon carbide, stannic oxide, ferric oxide are technical pure, and Calcium Fluoride (Fluorspan), oxalic acid and sodium oxalate are analytical pure; The particle diameter of described stannic oxide is 2 ~ 10 microns; The pH of described oxalic acid-sodium oxalate solution is 4 ~ 5.
The preparation method of artificial quartz in lump rumbling compound of the present invention comprises the steps:
(1) proportionally, by even to silicon oxide, silicon carbide and Calcium Fluoride (Fluorspan) mixed grinding;
(2) proportionally, by stannic oxide and ferric oxide mixed grinding even;
(3) batch mixing of step (1) and (2) gained is mixed, add oxalic acid-sodium oxalate solution, stir, obtain artificial quartz in lump rumbling compound.
Compared with prior art, the present invention has following beneficial effect:
The present invention is using silicon oxide and silicon carbide as the main raw material of rumbling compound, add stannic oxide and change its hardness, add fluorochemical and organic acid again, obtained artificial quartz in lump rumbling compound is used for polishing artificial quartz in lump, can significantly improve polishing efficiency, the marble polishing agent that the glossiness after polishing is more traditional improves more than 10%.
Embodiment
Below in conjunction with embodiment, the present invention is further elaborated.But embodiment does not limit in any form the present invention.
Embodiment 1
Prepare the rumbling compound of artificial quartz in lump:
(1) take 6g silicon oxide, 6g silicon carbide, 9g Calcium Fluoride (Fluorspan) is poured in mortar, and grinding evenly;
(2) take 1.65g stannic oxide, 1.8g ferric oxide is poured in mortar, and grinding evenly;
(3) jointly poured in beaker by the batch mixing in step (1) and (2), the adjusted good pH value of 10g is that the oxalic acid-sodium oxalate solution of 4-5 is poured in beaker, stirs, obtains light yellow mortar and be rumbling compound of the present invention.
(4) choosing artificial quartz in lump is test piece, by sub-for Austria MR5 marble crystallizing agent and 3) gained rumbling compound, with 9518E type portable grinding, polishing machine, polishing is carried out to model, and by vancometer experiment with measuring model glossiness, final gained rumbling compound of the present invention is compared sub-MR5 marble crystallizing agent difficult to understand and is improved 12.6%.
Embodiment 2
Prepare the rumbling compound of artificial quartz in lump:
(1) take 8g silicon oxide, 8g silicon carbide, 9g Calcium Fluoride (Fluorspan) is poured in mortar, and grinding evenly;
(2) take 2g stannic oxide, 2g ferric oxide is poured in mortar, and grinding evenly;
(3) by step 1) and 2) in batch mixing jointly pour in beaker, the adjusted good pH value of 15g is that the oxalic acid-sodium oxalate solution of 4-5 is poured in beaker, stirs, obtains light yellow mortar and be rumbling compound of the present invention.
(4) choosing artificial quartz in lump is test piece, by sub-for Austria MR5 marble crystallizing agent and 3) gained rumbling compound, with 9518E type portable grinding, polishing machine, polishing is carried out to model, and by vancometer experiment with measuring model glossiness, final gained rumbling compound of the present invention is compared sub-MR5 marble crystallizing agent difficult to understand and is improved 13.1%.
Claims (2)
1. an artificial quartz in lump rumbling compound, is characterized in that by silicon oxide, silicon carbide, stannic oxide, ferric oxide, Calcium Fluoride (Fluorspan) and oxalic acid-sodium oxalate solution be raw material, makes according to the mass ratio of 15 ~ 25:15 ~ 25:5 ~ 10:5 ~ 10:25 ~ 35:25 ~ 35;
Wherein, the particle diameter of described stannic oxide is 2 ~ 10 microns; The pH of described oxalic acid-sodium oxalate solution is 4 ~ 5, and described oxalic acid-sodium oxalate solution is dissolved in 100ml water formulated by 0.8g oxalic acid and 2.4g sodium oxalate.
2. the preparation method of artificial quartz in lump rumbling compound described in claim 1, is characterized in that comprising the steps:
(1) proportionally, by even to silicon oxide, silicon carbide and Calcium Fluoride (Fluorspan) mixed grinding;
(2) proportionally, by stannic oxide and ferric oxide mixed grinding even;
(3) batch mixing of step (1) and (2) gained is mixed, add oxalic acid-sodium oxalate solution, stir, obtain artificial quartz in lump rumbling compound.
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CN201510410984.5A CN105017971A (en) | 2015-07-14 | 2015-07-14 | Artificial quartz stone polishing agent and preparation method therefor |
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CN201510410984.5A CN105017971A (en) | 2015-07-14 | 2015-07-14 | Artificial quartz stone polishing agent and preparation method therefor |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105647391A (en) * | 2016-01-13 | 2016-06-08 | 上海欧柏森环境工程管理有限公司 | Stone polishing powder |
CN106118490A (en) * | 2016-06-30 | 2016-11-16 | 禹州市远大塑料电器有限责任公司 | A kind of quartz polishing agent and preparation technology thereof |
Citations (4)
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US5084071A (en) * | 1989-03-07 | 1992-01-28 | International Business Machines Corporation | Method of chemical-mechanical polishing an electronic component substrate and polishing slurry therefor |
CN1452535A (en) * | 2000-04-28 | 2003-10-29 | 3M创新有限公司 | Abrasive article and methods for grinding glass |
CN1637101A (en) * | 2003-11-26 | 2005-07-13 | 福吉米株式会社 | Polishing composition and polishing method |
JP2008000847A (en) * | 2006-06-22 | 2008-01-10 | Admatechs Co Ltd | Polishing material |
-
2015
- 2015-07-14 CN CN201510410984.5A patent/CN105017971A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5084071A (en) * | 1989-03-07 | 1992-01-28 | International Business Machines Corporation | Method of chemical-mechanical polishing an electronic component substrate and polishing slurry therefor |
CN1452535A (en) * | 2000-04-28 | 2003-10-29 | 3M创新有限公司 | Abrasive article and methods for grinding glass |
CN1637101A (en) * | 2003-11-26 | 2005-07-13 | 福吉米株式会社 | Polishing composition and polishing method |
JP2008000847A (en) * | 2006-06-22 | 2008-01-10 | Admatechs Co Ltd | Polishing material |
Non-Patent Citations (1)
Title |
---|
张秉坚: "装饰石材表面增光技术研究", 《新型建筑材料技术与发展—中国硅酸盐学会2003年学术年会新型建筑材料论文集》 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105647391A (en) * | 2016-01-13 | 2016-06-08 | 上海欧柏森环境工程管理有限公司 | Stone polishing powder |
CN105647391B (en) * | 2016-01-13 | 2017-12-15 | 上海欧柏森环境工程管理有限公司 | A kind of stone polishing powder |
CN106118490A (en) * | 2016-06-30 | 2016-11-16 | 禹州市远大塑料电器有限责任公司 | A kind of quartz polishing agent and preparation technology thereof |
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Application publication date: 20151104 |