CN1267373C - Face smearing mortar for self temperature regulation building wall and its preparing method - Google Patents

Face smearing mortar for self temperature regulation building wall and its preparing method Download PDF

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Publication number
CN1267373C
CN1267373C CN 200310112982 CN200310112982A CN1267373C CN 1267373 C CN1267373 C CN 1267373C CN 200310112982 CN200310112982 CN 200310112982 CN 200310112982 A CN200310112982 A CN 200310112982A CN 1267373 C CN1267373 C CN 1267373C
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China
Prior art keywords
mortar material
phase
weight
temperature
building wall
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Expired - Fee Related
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CN 200310112982
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Chinese (zh)
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CN1554613A (en
Inventor
梁金生
王静
金宗哲
吴子钊
陈志成
冀志江
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China Building Materials Academy CBMA
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China Building Materials Academy CBMA
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00482Coating or impregnation materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • C04B2111/29Frost-thaw resistance

Abstract

The present invention discloses a building wall decorative mortar material capable of automatically adjusting temperature and a preparation method thereof, which belongs to the field of a novel energy-saving building material. The purpose of the present invention is to provide a building wall decorative mortar material capable of automatically adjusting temperature and a preparation method thereof, wherein the building wall decorative mortar material has the advantages of no exudation, no frost formation and stable performance. The building wall decorative mortar material has the technical scheme that the decorative mortar material is characterized in that the mortar material comprises the following components in weight percentage: 5 to 15% of phase change composite material, 20 to 50% of construction sand, 30 to 50% of gelation material, 1 to 5% of antibiotic and rot resistance additive and water as the balance. The building wall decorative mortar material has the preparation method that the construction sand, the gelation material, the antibiotic and rot resistance additive and the water as the balance added with the phase change composite material after being firstly and thoroughly mixed, and the building wall decorative mortar material is directly used for wall surfaces of building operation after being uniformly mixed. The building wall decorative mortar material has the advantages of simplicity of the production method, labor saving, time saving, low cost and easy generalization and implementation; furthermore, the fluctuation spread of room temperature is reduced by 4 to 6 DEG C, and the service time of an air conditioner is reduced by more than 2 hours per day.

Description

A kind of from temperature adjustment construction wall plastering mortar material and preparation method thereof
Technical field
The present invention relates to a kind of construction wall plastering mortar material, specifically relate to a kind ofly, belong to novel energy-saving construction meterial additive technical field from temperature adjustment construction wall plastering mortar material and preparation method thereof.
Background technology
The construction wall plastering mortar material that has from temperature adjustment function is a kind of New Building Materials.It is as follows from the temperature adjustment principle of work: when envrionment temperature is higher than the transformation temperature of material, adds phase change material in the building materials to and absorb heat undergo phase transition from environment, room temp is reduced; When envrionment temperature is lower than the transformation temperature of material, add phase change material in the building materials to and undergo phase transition and emit heat, room temp is raise.This material has the advantages that to regulate architecture indoor temperature, raising indoor comfort degree automatically according to variation of ambient temperature.Therefore, from the temperature adjustment building materials in use, can reduce air-conditioning, heating installation duration of service, less air-conditioning is opened number of times, also helps them to avoid peak of power consumption work and the translation electricity consumption time, thereby reaches energy saving purposes.
At present existing from the temperature adjustment material of construction mainly contain self-regulated fire stons cream sheet material, from temperature adjustment top ceiling, self-regulated warm water mud sheet material and from the temperature adjustment concrete plate etc., the manufacture method of these sheet materials is mainly used the method for directly mixing or infiltration method processing, promptly in the mortar preparation process, a kind of phase-change working substance material is directly mixed wherein; Or the sheet material after the moulding directly immersed in the phase-change working substance material, make material of construction with phase-transition self-temperature-regulating function.The material of construction of method for preparing in use, its phase-change working substance material property instability, be easy to generate ooze out, phenomenon such as frosting, have a strong impact on the realization of its temperature adjustment function, also hinder its normal use, and do not have antibacterial and antimildew function.
Summary of the invention
Existing in order to solve from temperature adjustment material of construction defective in use, the purpose of this invention is to provide a kind of can be directly in the building surface construction, have antibacterial and mouldproof and energy-saving and cost-reducing function from temperature adjustment construction wall plastering mortar material.
To achieve these goals, the present invention by the following technical solutions: a kind of from temperature adjustment construction wall plastering mortar material, it is made up of following batching basically: phase change composite material 5~15 weight %; Building sand 20~50 weight %, inorganic coagulation material 30~50 weight %, anti-bacterium mildewproof additive 1~5 weight %, surplus is a water.
Described phase change composite material is to contain the phase-transition self-temperature-regulating unit grain that 40~70 weight % organic phase-change working materials and 30~60 weight % mineral materials are composited, its particulate median size is 1~50 micron, and wherein the organic phase-change working material is selected for use in lauryl alcohol or the tetradecyl alcohol at least a; Mineral material is selected for use in sepiolite, polygorskite or the attapulgite at least a.
Described phase change composite material can also be selected the microcapsule that are composited by the capsule heart that accounts for 40~70 weight % and the cyst wall that accounts for 30~60 weight % for use, the median size of microcapsule is 0.1~20 micron, and the described capsule heart is selected for use in n-hexadecane, Octadecane or the NSC 62789 alkane at least a; Described cyst wall is the aminoresin material, and aminoresin is selected melamine formaldehyde resin for use.
The median size of described building sand is less than 1.5mm; Described inorganic coagulation material is any one or two kinds of mixing in Portland cement, the calcium lime powder; Described anti-bacterium mildewproof additive be in silver zeolite antiseptic-germicide, copper zeolite antibacterial agent, zinc zeolite antibacterial agent and the rare earth activated inorganic antiseptic agent any; Wherein be preferably the rare earth activated inorganic antiseptic agent.
To achieve these goals, the present invention also provides a kind of preparation method from temperature adjustment construction wall plastering mortar material, the steps include: the building sand of elder generation with 20~50 weight %, the inorganic coagulation material of 30~50 weight %, the anti-bacterium mildewproof additive of 1~5 weight %, after surplus was the water thorough mixing, the phase change composite material that adds 5~15 weight % more fully stirred, and mixed the back and directly used.
Phase change composite material of the present invention, phase-transition self-temperature-regulating unit combination thing wherein, microcapsule coated phase-change material, phase-changing and temperature-regulating matrix material Detection of Stability method and METHOD FOR CONTINUOUS DETERMINATION phase change material method of life and device are all open in the inventor applies for a patent, and its patent name and number of patent application are respectively: phase-transition self-temperature-regulating unit combination thing and its production and use 03129763.3; A kind of microcapsule coated phase-change material and preparation method thereof 03130587.3; Phase-changing and temperature-regulating matrix material Detection of Stability method 03129762.5; METHOD FOR CONTINUOUS DETERMINATION phase change material method of life and install 03129761.7; Phase-transition self-temperature-regulating unit grain wherein, microcapsule and preparation method thereof describe in detail, do not repeat them here.
The present invention has adopted above technical scheme, and it is as follows that it has beneficial effect:
1. with the phase change composite material storage, the release essentially consist thing of energy, and be equipped with building sand, gelling material, anti-bacterium mildewproof additive, water, after mixing stirring, make from temperature adjustment function construction wall plastering mortar material, this mortar can directly be constructed at building surface, and is strong to the adaptive faculty of environment.With from temperature adjustment function construction wall plastering mortar material after traditional architecture body of wall internal surface construction, the phase-change working substance material does not have the frosting of oozing out phenomenon and occurs, and the fluctuations in indoor temperature amplitude reduces, the metope that comparable employing current material applies, the fluctuations in indoor temperature amplitude reduces 2~6 ℃, and when especially summer or winter, indoor/outdoor temperature-difference was very big, the fluctuations in indoor temperature amplitude reduced, can reduce the open hour of air-conditioning, realize the purpose of building energy conservation, and comfortable for living.
2. added in the composition of raw materials of the present invention that any uses as anti-bacterium mildewproof additive in silver zeolite antiseptic-germicide, copper zeolite antibacterial agent, zinc zeolite antibacterial agent or the rare earth activated inorganic antiseptic agent, wherein preferred rare earth activated inorganic antiseptic agent, it is added among the present invention, after the construction of traditional architecture body of wall internal surface, surface of wall has increased the function of antibacterial and mouldproof, inorganic antiseptic can will be adsorbed onto the killing bacteria of wall, has mildew-proof function simultaneously, the cross infection of bacteriological protection in advance improves the wholesomeness of building.
3. production technique of the present invention is simple, and cost is low, consumption is big, be convenient to popularization, meets the requirement of environment-friendly material of construction, has tangible exploitation advantage in temperature adjustment construction wall plastering mortar material.
Description of drawings
Fig. 1 is applied to the cross-sectional view of surface of wall back wall for the present invention
Fig. 2 is the electron scanning micrograph of the used phase change composite material microcapsule of the present invention
Fig. 3 is the electron scanning micrograph of the used phase-transition self-temperature-regulating unit grain of the present invention
Embodiment
Below in conjunction with drawings and Examples technical scheme of the present invention is described in detail:
As shown in Figure 1, it has shown and of the present inventionly has been applied to the cross-section structure of surface of wall back wall material from temperature adjustment construction wall plastering mortar material, comprises functional construction coating for internal wall 1; Has interior wall plastering mortar material 2 from temperature adjustment function; Wall main body 3; Exterior wall coating material 4; Outer wall building coating 5; The interior wall plastering mortar material 2 that has from temperature adjustment function is generally used for interior metope, and its skin also is coated with the functional interior wall coating 1 of one deck.
Have from the interior wall plastering mortar material 2 of temperature adjustment function and form by the batching of following weight per-cent basically: phase change composite material 5~15%; Building sand 20~50%, inorganic coagulation material 30~50%, anti-bacterium mildewproof additive 1~5%, surplus is a water.
Above-mentioned phase change composite material is the phase-transition self-temperature-regulating unit grain that contains organic phase-change working material and mineral material composition, and its particulate median size is 1~50 micron; Wherein the weight percent of organic phase-change working material and mineral material is 40~50: 50~60; The organic phase-change working material is at least a in lauryl alcohol or the tetradecyl alcohol; Mineral material is at least a in sepiolite, polygorskite or the attapulgite.
Above-mentioned organic phase-change matrix material can also be selected the microcapsule of being made up of the capsule heart that accounts for weight percent 40~50% and the cyst wall that accounts for weight percent 50~60% for use, and the median size of microcapsule is 0.1~20 micron; Wherein capsule heartwood material is the organic phase-change working material; Cyst material is an aminoresin; The organic phase-change working material adopts in n-hexadecane, Octadecane or the NSC 62789 alkane at least a; Aminoresin adopts melamine formaldehyde resin.
The transformation temperature of above-mentioned organic phase-change working material requires to satisfy between 16~28 ℃.
In addition, of the present invention in temperature adjustment construction wall plastering mortar material, the median size that also requires building sand is less than 1.5mm; Inorganic coagulation material is selected any one or two kinds of mixing in Portland cement, the calcium lime powder for use; Anti-bacterium mildewproof additive can be selected any in silver zeolite antiseptic-germicide, copper zeolite antibacterial agent, zinc zeolite antibacterial agent and the rare earth activated inorganic antiseptic agent for use, best preferred rare earth activated inorganic antiseptic agent.
Above-mentioned preparation method from temperature adjustment construction wall plastering mortar material, its step is: will build sand 20~50% earlier, inorganic coagulation material 30~50%, anti-bacterium mildewproof additive 1~5%, after surplus is the water thorough mixing, add phase change composite material 5~15% again and fully stir, can directly be coated on metope after mixing.
As shown in Figure 2, by the microcapsule electron scanning micrograph that the melamine formaldehyde resin cyst wall of the octadecane capsule heart that contains weight ratio 50% and 50% is formed, the transformation temperature of its phase-change working substance material is 23.15 ℃.
As shown in Figure 3, the electron scanning micrograph of the phase-transition self-temperature-regulating unit grain of forming for the sepiolite of the lauryl alcohol that contains weight ratio 60% and 40%, the transformation temperature of its phase-change working substance material is 24.0 ℃.
According to the proportioning and the method for above-mentioned accompanying drawing and material, its specific embodiment is as follows:
Embodiment 1
To build sand 40Kg, Portland cement 40Kg, rare earth activated inorganic antiseptic agent 5Kg, water 18Kg directly drop into thorough mixing in the concrete mixer, add phase change composite material 15Kg then; Fully stirred 2 minutes, mix the back and directly use.
Wherein phase change composite material is made up of the microcapsule that contain the phase-change working substance material, and wherein the phase-change working substance material adopts and to contain 50% the octadecane capsule heart and 50% melamine formaldehyde resin cyst wall is formed microcapsule; Wherein the pattern of phase change composite material is shown in the electron scanning micrograph of Fig. 2.
This mortar is used for building operation, itself has well in temperature adjustment function, after testing, adds metope sand finish material that the phase-change working substance material is arranged and can not produce macroscopic view in 30 years and ooze out phenomenon, do not tie bloom using; The fluctuating range of room temp can reduce by 4~6 ℃, when indoor/outdoor temperature-difference is big, still can keep room temp that the variation of great fluctuation process does not take place, and the start of air-conditioning can reduce more than 2 hours every day duration of service approximately; Surface of wall has applied sand finish material of the present invention, and inorganic antiseptic wherein has the long acting antibiotic mildew-proof function, can have mildew-proof function with being adsorbed onto the killing bacteria of wall, avoids bacterial cross-infection; In the weather of humidity in rainy season, this wall coating mortar material can not produce mould or mildew in 20 years, after 3 years mould can be taken place with prior art sand finish material or the mildew phenomenon is compared, effectively improved the wholesomeness of building, meet the requirement of green building material product, realize and comfortable for living and building energy conservation target.
Embodiment 2
Cement 50Kg, building sand 35Kg, silver zeolite inorganic antiseptic 5Kg, water 25Kg are dropped into thorough mixing in the concrete mixer, add phase-transition self-temperature-regulating matrix material 10Kg then, stirred 2 minutes, promptly can be made into self-regulated temperature function construction cement mortar.Wherein used phase change composite material is for adding the microcapsule of the weight percent 50% octadecane capsule heart and 50% melamine formaldehyde resin cyst wall, and the pattern of its microcapsule is shown in the electron scanning micrograph of Fig. 2.
Its technique effect is with embodiment one.
Embodiment 3
After 40Kg calcium lime powder, 54Kg building sand, the agent of 1Kg rare earth activated inorganic antiseptic, the mixing of 20Kg water, directly drop into thorough mixing in the concrete mixer, add phase-transition self-temperature-regulating unit grain 5Kg then, stir after 2 minutes, promptly can be made into self-regulated temperature function building mortar.Wherein the phase-transition self-temperature-regulating unit grain contains lauryl alcohol that accounts for weight percent 60% and the sepiolite that accounts for weight percent 40%, the pattern of described phase-transition self-temperature-regulating unit grain is shown in Fig. 3 electron scanning micrograph, and wherein the transformation temperature of phase-change working substance material is 24.0 ℃.
Its technique effect is with embodiment one.
Embodiment 4
After 20Kg calcium lime powder, 20Kg cement, 46Kg building sand, the agent of 4Kg rare earth activated inorganic antiseptic, the mixing of 20Kg water, directly drop into thorough mixing in the concrete mixer, add 10Kg phase-transition self-temperature-regulating unit grain then, stirred 2 minutes, promptly can be made into self-regulated temperature function building mortar.Wherein, the phase-transition self-temperature-regulating unit grain is formed for accounting for weight percent 60% lauryl alcohol and accounting for 40% sepiolite; Wherein the transformation temperature of phase-change working substance material is 24.0 ℃; The pattern of phase-transition self-temperature-regulating unit grain is shown in the electron scanning micrograph of Fig. 3.
Its technique effect is with embodiment one.
Embodiment 5
After 30Kg calcium lime powder, 54Kg building sand, the agent of 3Kg rare earth activated inorganic antiseptic, the mixing of 17Kg water, directly drop into thorough mixing in the concrete mixer, add 13Kg phase-transition self-temperature-regulating matrix material then, stir after 2 minutes, promptly can be made into the building mortar that has from temperature adjustment function.Wherein, the phase-transition self-temperature-regulating matrix material is formed for accounting for weight percent 60% lauryl alcohol and accounting for weight percent 40% sepiolite; Wherein, the transformation temperature of phase-change working substance material is 24.0 ℃.The pattern of phase-transition self-temperature-regulating unit grain is shown in the electron scanning micrograph of Fig. 3.
Its technique effect is with embodiment one.
Embodiment 6
After 32Kg calcium lime powder, 58Kg building sand, the agent of 3Kg rare earth activated inorganic antiseptic, the mixing of 17Kg water, directly drop into thorough mixing in the concrete mixer, add 7Kg phase-transition self-temperature-regulating matrix material then, stir after 2 minutes, promptly can be made into self-regulated temperature function construction cement mortar.Described phase-transition self-temperature-regulating matrix material is formed by accounting for weight percent 60% lauryl alcohol and 40% sepiolite, and wherein the transformation temperature of phase-change working substance material is 24.0 ℃.The pattern of phase-transition self-temperature-regulating unit grain is shown in the electron scanning micrograph of Fig. 3.
Its technique effect is with embodiment one.

Claims (7)

1. one kind from temperature adjustment construction wall plastering mortar material, and it is made up of following batching: phase change composite material 5~15 weight %; Building sand 20~50 weight %, inorganic coagulation material 30~50 weight %, anti-bacterium mildewproof additive 1~5 weight %, surplus is a water; Described phase change composite material is to contain the mineral material compound phase-transition self-temperature-regulating unit grain of the organic phase-change working material of 40~70 weight % and 30~60 weight % or by the cyst wall compound microcapsule of the capsule heart that contains 40~70 weight % and 30~60 weight %; Wherein, the organic phase-change working material is at least a in lauryl alcohol or the tetradecyl alcohol, and described mineral material is at least a in sepiolite, polygorskite or the attapulgite; The described capsule heart is at least a in n-hexadecane, Octadecane or the NSC 62789 alkane, and described cyst wall is an aminoresin.
2. according to claim 1 from temperature adjustment construction wall plastering mortar material, it is characterized in that: the median size of described phase-transition self-temperature-regulating unit grain is 1~50 micron; The median size of described microcapsule is 0.1~20 micron.
3. according to claim 1 from temperature adjustment construction wall plastering mortar material, it is characterized in that: described aminoresin is melamine formaldehyde resin.
4. according to claim 1 from temperature adjustment construction wall plastering mortar material, the median size of described building sand is less than 1.5mm; Described inorganic coagulation material is any one or two kinds of mixing in Portland cement, the calcium lime powder;
As described in claim 1 or 2 or 3 or 4 from temperature adjustment construction wall plastering mortar material, it is characterized in that: described anti-bacterium mildewproof additive be in silver zeolite antiseptic-germicide, copper zeolite antibacterial agent, zinc zeolite antibacterial agent and the rare earth activated inorganic antiseptic agent any.
As described in claim 1 or 2 or 3 or 4 from temperature adjustment construction wall plastering mortar material, it is characterized in that: described anti-bacterium mildewproof additive is the rare earth activated inorganic antiseptic agent.
7. each described preparation method of claim 1-6 from temperature adjustment construction wall plastering mortar material, it is characterized by: earlier with 20~50% building sand, 30~50% inorganic coagulation material, 1~5% anti-bacterium mildewproof additive, after surplus is the water thorough mixing, add 5~15% phase change composite material again and fully stir, mix the back and directly use.
CN 200310112982 2003-12-29 2003-12-29 Face smearing mortar for self temperature regulation building wall and its preparing method Expired - Fee Related CN1267373C (en)

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US8044793B2 (en) 2001-03-01 2011-10-25 Fisher-Rosemount Systems, Inc. Integrated device alerts in a process control system
US8055479B2 (en) 2007-10-10 2011-11-08 Fisher-Rosemount Systems, Inc. Simplified algorithm for abnormal situation prevention in load following applications including plugged line diagnostics in a dynamic process
US8073967B2 (en) 2002-04-15 2011-12-06 Fisher-Rosemount Systems, Inc. Web services-based communications for use with process control systems
US8301676B2 (en) 2007-08-23 2012-10-30 Fisher-Rosemount Systems, Inc. Field device with capability of calculating digital filter coefficients
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US8417595B2 (en) 2001-03-01 2013-04-09 Fisher-Rosemount Systems, Inc. Economic calculations in a process control system
US8620779B2 (en) 2001-03-01 2013-12-31 Fisher-Rosemount Systems, Inc. Economic calculations in a process control system
US8073967B2 (en) 2002-04-15 2011-12-06 Fisher-Rosemount Systems, Inc. Web services-based communications for use with process control systems
US8301676B2 (en) 2007-08-23 2012-10-30 Fisher-Rosemount Systems, Inc. Field device with capability of calculating digital filter coefficients
US7702401B2 (en) 2007-09-05 2010-04-20 Fisher-Rosemount Systems, Inc. System for preserving and displaying process control data associated with an abnormal situation
US8055479B2 (en) 2007-10-10 2011-11-08 Fisher-Rosemount Systems, Inc. Simplified algorithm for abnormal situation prevention in load following applications including plugged line diagnostics in a dynamic process

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