CN1720288A - 制造阻燃聚碳酸酯的方法和相关组合物 - Google Patents
制造阻燃聚碳酸酯的方法和相关组合物 Download PDFInfo
- Publication number
- CN1720288A CN1720288A CN03825739.4A CN03825739A CN1720288A CN 1720288 A CN1720288 A CN 1720288A CN 03825739 A CN03825739 A CN 03825739A CN 1720288 A CN1720288 A CN 1720288A
- Authority
- CN
- China
- Prior art keywords
- salt
- sulfonate
- postassium
- sodium salt
- perfluoroalkane sulfonate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 56
- 239000004417 polycarbonate Substances 0.000 title claims abstract description 50
- 229920000515 polycarbonate Polymers 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims description 51
- 150000003839 salts Chemical class 0.000 claims abstract description 80
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 claims abstract description 65
- 239000000654 additive Substances 0.000 claims abstract description 47
- 239000004431 polycarbonate resin Substances 0.000 claims abstract description 44
- 229920005668 polycarbonate resin Polymers 0.000 claims abstract description 44
- 159000000000 sodium salts Chemical class 0.000 claims abstract description 44
- 230000000996 additive effect Effects 0.000 claims abstract description 36
- 239000003063 flame retardant Substances 0.000 claims abstract description 35
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000002253 acid Substances 0.000 claims description 42
- 150000007513 acids Chemical class 0.000 claims description 42
- LVTHXRLARFLXNR-UHFFFAOYSA-M potassium;1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate Chemical compound [K+].[O-]S(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F LVTHXRLARFLXNR-UHFFFAOYSA-M 0.000 claims description 24
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 22
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 22
- 229910052700 potassium Inorganic materials 0.000 claims description 22
- 239000011591 potassium Substances 0.000 claims description 22
- 239000003112 inhibitor Substances 0.000 claims description 19
- KVCGISUBCHHTDD-UHFFFAOYSA-M sodium;4-methylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1 KVCGISUBCHHTDD-UHFFFAOYSA-M 0.000 claims description 18
- 229910052799 carbon Inorganic materials 0.000 claims description 12
- 125000004432 carbon atom Chemical group C* 0.000 claims description 12
- 230000002195 synergetic effect Effects 0.000 claims description 8
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 239000008365 aqueous carrier Substances 0.000 claims description 4
- 125000005010 perfluoroalkyl group Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims 11
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims 1
- 235000011164 potassium chloride Nutrition 0.000 claims 1
- 239000001103 potassium chloride Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 14
- LBLYYCQCTBFVLH-UHFFFAOYSA-N 2-Methylbenzenesulfonic acid Chemical compound CC1=CC=CC=C1S(O)(=O)=O LBLYYCQCTBFVLH-UHFFFAOYSA-N 0.000 abstract description 3
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000009472 formulation Methods 0.000 description 9
- 239000012760 heat stabilizer Substances 0.000 description 9
- 239000000463 material Substances 0.000 description 9
- 229920005989 resin Polymers 0.000 description 7
- 239000011347 resin Substances 0.000 description 7
- 239000008367 deionised water Substances 0.000 description 5
- 229910021641 deionized water Inorganic materials 0.000 description 5
- 239000000843 powder Substances 0.000 description 5
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 4
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 3
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 3
- 229910052794 bromium Inorganic materials 0.000 description 3
- 125000001309 chloro group Chemical group Cl* 0.000 description 3
- 150000003871 sulfonates Chemical class 0.000 description 3
- OCKWAZCWKSMKNC-UHFFFAOYSA-N [3-octadecanoyloxy-2,2-bis(octadecanoyloxymethyl)propyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(COC(=O)CCCCCCCCCCCCCCCCC)(COC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC OCKWAZCWKSMKNC-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- VSIKJPJINIDELZ-UHFFFAOYSA-N 2,2,4,4,6,6,8,8-octakis-phenyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical compound O1[Si](C=2C=CC=CC=2)(C=2C=CC=CC=2)O[Si](C=2C=CC=CC=2)(C=2C=CC=CC=2)O[Si](C=2C=CC=CC=2)(C=2C=CC=CC=2)O[Si]1(C=1C=CC=CC=1)C1=CC=CC=C1 VSIKJPJINIDELZ-UHFFFAOYSA-N 0.000 description 1
- CMQUQOHNANGDOR-UHFFFAOYSA-N 2,3-dibromo-4-(2,4-dibromo-5-hydroxyphenyl)phenol Chemical compound BrC1=C(Br)C(O)=CC=C1C1=CC(O)=C(Br)C=C1Br CMQUQOHNANGDOR-UHFFFAOYSA-N 0.000 description 1
- IISBACLAFKSPIT-UHFFFAOYSA-N Bisphenol A Natural products C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 1
- 101100518972 Caenorhabditis elegans pat-6 gene Proteins 0.000 description 1
- 229920004142 LEXAN™ Polymers 0.000 description 1
- 239000004418 Lexan Substances 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000008052 alkyl sulfonates Chemical class 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- 229940106691 bisphenol a Drugs 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000000536 complexating effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 239000003365 glass fiber Substances 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- USVKKJUSLJKPHV-UHFFFAOYSA-N phenylmethanesulfonic acid;sodium Chemical compound [Na].OS(=O)(=O)CC1=CC=CC=C1 USVKKJUSLJKPHV-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- GGRIQDPLLHVRDU-UHFFFAOYSA-M potassium;2-(benzenesulfonyl)benzenesulfonate Chemical compound [K+].[O-]S(=O)(=O)C1=CC=CC=C1S(=O)(=O)C1=CC=CC=C1 GGRIQDPLLHVRDU-UHFFFAOYSA-M 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 235000015598 salt intake Nutrition 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- ITMCEJHCFYSIIV-UHFFFAOYSA-M triflate Chemical class [O-]S(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0066—Flame-proofing or flame-retarding additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/36—Sulfur-, selenium-, or tellurium-containing compounds
- C08K5/41—Compounds containing sulfur bound to oxygen
- C08K5/42—Sulfonic acids; Derivatives thereof
Abstract
Description
组1-1 | 组1-2 | 组1-3 | 组1-4 | 组1-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTSp(FTP)@62密耳 | 60400.350.030.320.0050.10.68 | 60400.350.030.320.0050.10.96 | 60400.350.030.320.00750.150.8 | 60400.350.030.320.010.20.3 | 60400.350.030.320.010.20.31 |
组2-1 | 组2-2 | 组2-3 | 组2-4 | 组2-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTS去离子水p(FTP)@62密耳 | 60400.350.030.320.0030.050.250.87 | 60400.350.030.320.0090.050.250.93 | 60400.350.030.320.0060.080.250.13 | 60400.350.030.320.0030.110.250.48 | 60400.350.030.320.0090.110.250.13 |
组3-1 | 组3-2 | 组3-3 | 组3-4 | 组3-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTS去离子水p(FTP)@62密耳 | 60400.350.030.320.0060.0250.40.99 | 60400.350.030.320.010.0250.41 | 60400.350.030.320.0080.0350.40.55 | 60400.350.030.320.0060.0450.40.67 | 60400.350.030.320.010.0450.40.23 |
组4-1 | 组4-2 | 组4-3 | 组4-4 | 组4-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTSp(FTP)@62密耳 | 60400.350.050.350.00900.1067 | 60400.350.050.350.0090.0050.913 | 60400.350.050.350.0090.010.947 | 60400.350.050.350.0090.020.963 | 60400.350.050.350.0090.030.86 |
组5-1 | 组5-2 | 组5-3 | 组5-4 | 组5-5 | 组5-6 | 组5-7 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTSp(FTP)@62密耳 | 60400.350.050.3500.0150.071 | 60400.350.050.350.0030.0150.4355 | 60400.350.050.350.0060.0150.908 | 60400.350.050.350.0090.0150.999 | 60400.350.050.350.0150.0150.999 | 60400.350.050.350.0260.0150.999 | 60400.350.050.350.0450.0151 |
组6-1 | 组6-2 | 组6-3 | 组6-4 | 组6-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂RimarNaTS | 65350.350.050.35 | 65350.350.050.350.020.015 | 65350.350.050.350.030.015 | 65350.350.050.350.040.015 | 65350.350.050.350.050.015 |
组7-1 | 组7-2 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂Rimar盐NaTS去离子水p(FTP)@45密耳5V@125密耳 | 40600.350.050.450.0120.0150.30.97通过 | 60400.350.050.450.0120.0150.30.96通过 |
组8-1 | 组8-2 | 组8-3 | 组8-4 | 组8-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂Triflate-Cl盐NaTS去离子水p(FTP)@45密耳 | 40600.350.050.450.00900.20.003 | 40600.350.050.450.0090.0040.20.057 | 40600.350.050.450.0090.0080.20.172 | 40600.350.050.450.0090.0120.20.715 | 40600.350.050.450.0090.0160.20.765 |
组9-1 | 组9-2 | 组9-3 | 组9-4 | 组9-5 | |
高流动性PC100等级PC脱模剂热稳定剂防滴剂Triflate-Cl盐NaTS去离子水p(FTP)@45密耳 | 40600.350.050.4500.0120.20.007 | 40600.350.050.450.0060.0120.20.568 | 40600.350.050.450.0090.0120.20.913 | 40600.350.050.450.0120.0120.20.936 | 40600.350.050.450.0150.0120.20.953 |
Claims (75)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/065,545 | 2002-10-29 | ||
US10/065,545 US6790899B2 (en) | 2002-10-29 | 2002-10-29 | Method for making fire-retarded polycarbonate and related compositions |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1720288A true CN1720288A (zh) | 2006-01-11 |
CN1312205C CN1312205C (zh) | 2007-04-25 |
Family
ID=32106069
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB038257394A Expired - Fee Related CN1312205C (zh) | 2002-10-29 | 2003-08-27 | 制造阻燃聚碳酸酯的方法和相关组合物 |
Country Status (7)
Country | Link |
---|---|
US (1) | US6790899B2 (zh) |
EP (1) | EP1558676A1 (zh) |
JP (1) | JP2006504823A (zh) |
CN (1) | CN1312205C (zh) |
AU (1) | AU2003272245A1 (zh) |
TW (1) | TW200420644A (zh) |
WO (1) | WO2004039879A1 (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101472995B (zh) * | 2006-06-22 | 2011-12-28 | 沙伯基础创新塑料知识产权有限公司 | 聚碳酸酯组合物及由其形成的制品 |
CN101384684B (zh) * | 2006-02-14 | 2012-01-04 | 沙伯基础创新塑料知识产权有限公司 | 聚碳酸酯组合物和由其形成的制品 |
CN101400763B (zh) * | 2006-02-14 | 2012-06-27 | 沙伯基础创新塑料知识产权有限公司 | 不含卤素的聚碳酸酯组合物和由其形成的制品 |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080015292A1 (en) * | 2006-07-12 | 2008-01-17 | General Electric Company | Flame retardant and scratch resistant thermoplastic polycarbonate compositions |
US20090062439A1 (en) * | 2007-08-30 | 2009-03-05 | Van De Grampel Robert Dirk | Polyestercarbonate compositions |
US7732516B2 (en) * | 2008-01-31 | 2010-06-08 | Sabic Innovative Plastics Ip B.V. | Flame retardant polyimide/polyester-polycarbonate compositions, methods of manufacture, and articles formed therefrom |
US20090227707A1 (en) * | 2008-03-07 | 2009-09-10 | Domenico La Camera | Flame retardant polycarbonate based composition including carbon |
JP5364653B2 (ja) * | 2010-06-14 | 2013-12-11 | 三菱エンジニアリングプラスチックス株式会社 | 難燃性ポリカーボネート樹脂組成物及びそれからなる成形品 |
CN103333478A (zh) * | 2013-06-26 | 2013-10-02 | 江苏启蓝新材料有限公司 | 无卤阻燃聚碳酸酯及其制备方法 |
EP3068817A1 (en) * | 2013-11-15 | 2016-09-21 | SABIC Global Technologies B.V. | Methods for measuring properties in crosslinked polycarbonate |
CN109810404B (zh) * | 2018-12-24 | 2021-11-23 | 浙江大学宁波理工学院 | 一种聚丙烯/金属氢氧化物/稀土化合物阻燃材料 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT297333B (de) * | 1969-06-13 | 1972-03-27 | Bayer Ag | Verfahren zur Herstellung von Polycarbonaten mit verminderter Brennbarkeit |
US3933734A (en) * | 1973-12-28 | 1976-01-20 | General Electric Company | Flame retardant polycarbonate composition |
US3971756A (en) * | 1974-08-09 | 1976-07-27 | General Electric Company | Flame retardant polycarbonate composition |
US4028297A (en) * | 1975-07-18 | 1977-06-07 | General Electric Company | Novel flame retardant polycarbonate compositions |
US4110299A (en) * | 1976-10-15 | 1978-08-29 | General Electric Company | Flame-retardant polycarbonate composition |
US4104253A (en) * | 1976-10-15 | 1978-08-01 | General Electric Company | Flame retardant polycarbonate composition |
US4130299A (en) * | 1977-09-12 | 1978-12-19 | Monsanto Company | Low-odor dye solvents for pressure-sensitive copying systems |
US4201832A (en) * | 1978-06-23 | 1980-05-06 | General Electric Company | Non melt-drip flame retardant polycarbonate composition |
US4303575A (en) * | 1980-02-07 | 1981-12-01 | Mobay Chemical Corporation | Flame retardant polycarbonate compositions |
US4335038A (en) * | 1980-09-26 | 1982-06-15 | The Dow Chemical Company | Polycarbonate containing a metal perfluoroborate and an organosilane as ignition depressants |
DE3203905A1 (de) * | 1982-02-05 | 1983-08-11 | Bayer Ag, 5090 Leverkusen | Polycarbonat-formmassen mit verbesserter flammwidrigkeit |
GB8806497D0 (en) * | 1988-03-18 | 1988-04-20 | Mortile Acoustic Ind Ltd | Non-toxic fire retardant thermoplastic material |
US4916194A (en) * | 1989-03-06 | 1990-04-10 | General Electric Company | Flame retardant aromatic polycarbonate blends |
US5508323A (en) * | 1992-06-29 | 1996-04-16 | Dow Corning Corporation | Method for imparting fire retardancy to organic resins |
US6353046B1 (en) * | 2000-04-28 | 2002-03-05 | General Electric Company | Fire-retarded polycarbonate resin composition |
US6462111B1 (en) * | 2001-12-10 | 2002-10-08 | General Electric Company | Translucent flame retardant polycarbonate compositions |
-
2002
- 2002-10-29 US US10/065,545 patent/US6790899B2/en not_active Expired - Lifetime
-
2003
- 2003-08-27 WO PCT/US2003/027048 patent/WO2004039879A1/en not_active Application Discontinuation
- 2003-08-27 JP JP2004548303A patent/JP2006504823A/ja active Pending
- 2003-08-27 CN CNB038257394A patent/CN1312205C/zh not_active Expired - Fee Related
- 2003-08-27 AU AU2003272245A patent/AU2003272245A1/en not_active Abandoned
- 2003-08-27 EP EP03754419A patent/EP1558676A1/en not_active Ceased
- 2003-10-14 TW TW092128452A patent/TW200420644A/zh unknown
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101384684B (zh) * | 2006-02-14 | 2012-01-04 | 沙伯基础创新塑料知识产权有限公司 | 聚碳酸酯组合物和由其形成的制品 |
CN101400763B (zh) * | 2006-02-14 | 2012-06-27 | 沙伯基础创新塑料知识产权有限公司 | 不含卤素的聚碳酸酯组合物和由其形成的制品 |
CN101472995B (zh) * | 2006-06-22 | 2011-12-28 | 沙伯基础创新塑料知识产权有限公司 | 聚碳酸酯组合物及由其形成的制品 |
Also Published As
Publication number | Publication date |
---|---|
EP1558676A1 (en) | 2005-08-03 |
US20040082691A1 (en) | 2004-04-29 |
TW200420644A (en) | 2004-10-16 |
JP2006504823A (ja) | 2006-02-09 |
WO2004039879A1 (en) | 2004-05-13 |
CN1312205C (zh) | 2007-04-25 |
AU2003272245A1 (en) | 2004-05-25 |
US6790899B2 (en) | 2004-09-14 |
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