DE102005054034A1 - Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern - Google Patents

Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern Download PDF

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Publication number
DE102005054034A1
DE102005054034A1 DE102005054034A DE102005054034A DE102005054034A1 DE 102005054034 A1 DE102005054034 A1 DE 102005054034A1 DE 102005054034 A DE102005054034 A DE 102005054034A DE 102005054034 A DE102005054034 A DE 102005054034A DE 102005054034 A1 DE102005054034 A1 DE 102005054034A1
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Germany
Prior art keywords
production
release agent
aqueous release
polyurethane moldings
dollar
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
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DE102005054034A
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English (en)
Inventor
Ralf Althoff
Torsten Henning
Helmut Lammerting
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Evonik Operations GmbH
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Goldschmidt GmbH
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Priority to DE102005054034A priority Critical patent/DE102005054034A1/de
Priority to US11/586,267 priority patent/US8748514B2/en
Priority to EP06022561A priority patent/EP1785252B1/de
Priority to DE502006001485T priority patent/DE502006001485D1/de
Priority to ES06022561T priority patent/ES2313532T3/es
Publication of DE102005054034A1 publication Critical patent/DE102005054034A1/de
Withdrawn legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C33/00—Moulds or cores; Details thereof or accessories therefor
    • B29C33/56—Coatings, e.g. enameled or galvanised; Releasing, lubricating or separating agents
    • B29C33/60—Releasing, lubricating or separating agents
    • B29C33/62—Releasing, lubricating or separating agents based on polymers or oligomers
    • B29C33/64—Silicone
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C33/00—Moulds or cores; Details thereof or accessories therefor
    • B29C33/56—Coatings, e.g. enameled or galvanised; Releasing, lubricating or separating agents
    • B29C33/60—Releasing, lubricating or separating agents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C33/00—Moulds or cores; Details thereof or accessories therefor
    • B29C33/56—Coatings, e.g. enameled or galvanised; Releasing, lubricating or separating agents
    • B29C33/60—Releasing, lubricating or separating agents
    • B29C33/62—Releasing, lubricating or separating agents based on polymers or oligomers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/017—Mixtures of compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
    • C09K23/54—Silicon compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00—Lubricating compositions containing more than 10% water
    • C10M173/02—Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/06—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing conjugated dienes
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms
    • C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/283—Esters of polyhydroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/14—Containing carbon-to-nitrogen double bounds, e.g. guanidines, hydrazones, semicarbazones
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/04—Siloxanes with specific structure
    • C10M2229/047—Siloxanes with specific structure containing alkylene oxide groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/36—Release agents or mold release agents

Abstract

Gegenstand der Erfindung sind wässrige Dispersionen, enthaltend trennaktive Mittel, Emulgatoren und übliche Hilfs- und Zusatzmittel, welche dadurch gekennzeichnet sind, dass als trennaktive Mittel eine Kombination aus DOLLAR A A) mindestens einem trennaktiven Mittel, ausgesucht aus der Gruppe Seifen, Öle, Wachse und Siliconen, und DOLLAR A B) Polyester, DOLLAR A verwendet wird.
DE102005054034A 2005-11-12 2005-11-12 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern Withdrawn DE102005054034A1 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
DE102005054034A DE102005054034A1 (de) 2005-11-12 2005-11-12 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
US11/586,267 US8748514B2 (en) 2005-11-12 2006-10-25 Aqueous release agent and its use in the production of polyurethane moldings
EP06022561A EP1785252B1 (de) 2005-11-12 2006-10-28 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
DE502006001485T DE502006001485D1 (de) 2005-11-12 2006-10-28 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
ES06022561T ES2313532T3 (es) 2005-11-12 2006-10-28 Agente acuoso de separacion y su utilizacion en la produccion de cuerpos moldeados de poliuretanos.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102005054034A DE102005054034A1 (de) 2005-11-12 2005-11-12 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern

Publications (1)

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DE102005054034A1 true DE102005054034A1 (de) 2007-05-16

Family

ID=37698100

Family Applications (2)

Application Number Title Priority Date Filing Date
DE102005054034A Withdrawn DE102005054034A1 (de) 2005-11-12 2005-11-12 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
DE502006001485T Active DE502006001485D1 (de) 2005-11-12 2006-10-28 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE502006001485T Active DE502006001485D1 (de) 2005-11-12 2006-10-28 Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern

Country Status (4)

Country Link
US (1) US8748514B2 (de)
EP (1) EP1785252B1 (de)
DE (2) DE102005054034A1 (de)
ES (1) ES2313532T3 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2987598A1 (de) 2014-08-19 2016-02-24 Evonik Degussa GmbH Hybride Dispersion und ihre Verwendung

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102005054033A1 (de) * 2005-11-12 2007-05-16 Goldschmidt Gmbh Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
DE102007024493A1 (de) * 2007-05-25 2008-11-27 Evonik Goldschmidt Gmbh Wässrige Trennmittel und ihre Verwendung bei der Herstellung von Polyurethan-Formkörpern
PL2017053T3 (pl) * 2007-07-19 2015-11-30 Evonik Degussa Gmbh Bezrozpuszczalnikowy środek antyadhezyjny i jego zastosowanie przy wytwarzaniu elementów formowanych z poliuretanu
DE102007037571A1 (de) * 2007-08-09 2009-02-12 Evonik Goldschmidt Gmbh Wässriges Trennmittel und seine Verwendung bei der Herstellung von Polyurethan-Formkörpern
DE102007040567B4 (de) * 2007-08-28 2010-10-14 Ems-Patent Ag Wässrige Polyesterdispersion, deren Verwendungen und kontinuierliches Beschichtungsverfahren
ES2842501T5 (es) 2015-09-21 2023-04-13 Modern Meadow Inc Materiales compuestos de tejido reforzados con fibras
DE102017102080A1 (de) 2017-02-02 2018-08-02 Mathias Dränkow Trennschichtgewebe, Verfahren zur Herstellung von Trennschichtgewebe und dessen Verwendung
CN108381827A (zh) * 2018-03-26 2018-08-10 佛山市顺德区佳力精细化工有限公司 一种非硅油脱模剂及其制备方法
EP4215333A1 (de) 2022-01-24 2023-07-26 Productos Concentrol, S.A. Verfahren zur herstellung eines wässrigen formtrennmittels

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DE2702930A1 (de) * 1977-01-25 1978-07-27 Alois Stankiewicz Chemische Er Trennmittel fuer formen
US4491607A (en) * 1981-11-23 1985-01-01 Park Chemical Company Mold release agents and means of application
US4473403A (en) * 1984-02-15 1984-09-25 Park Chemical Company Mold release agents for open-cell molded foamed articles and means of application
USH444H (en) * 1985-05-20 1988-03-01 A. E. Staley Manufacturing Company Process for making molded articles with mold release agents
DE3742370A1 (de) 1987-12-14 1989-06-22 Codal Chemie Gmbh Waessriges trennmittel zur herstellung von polyurethan-formkoerpern
US4936917A (en) * 1988-01-12 1990-06-26 Air Products And Chemicals, Inc. Water based mold release compositions containing poly(siloxane-glycol) surfactants for making polyurethane foam article in a mold
DK653488D0 (da) * 1988-11-23 1988-11-23 Esti Kemi Aps Smoeremiddel
DE4020036A1 (de) 1990-06-23 1992-01-02 Klueber Chemie Kg Waessriges trennmittel zur herstellung von polyurethan-formkoerpern enthaltend ethoxylierten alkohol
US5137966A (en) * 1991-02-25 1992-08-11 Miles Inc. Internal release agents, active hydrogen containing mixtures which contain such agents and the use thereof in a process for the production of molded products
DE10158154A1 (de) * 2001-11-28 2003-06-18 Bayer Ag Trennmittel und Verfahren zur Herstellung von Kunststoffformteilen
DE10259184B3 (de) * 2002-12-18 2004-09-09 Bayer Ag Stabile Polyoldispersionen und daraus hergestellte Polyurethanformkörper und ihre Verwendung

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2987598A1 (de) 2014-08-19 2016-02-24 Evonik Degussa GmbH Hybride Dispersion und ihre Verwendung
WO2016026639A1 (de) 2014-08-19 2016-02-25 Evonik Degussa Gmbh Hybride dispersion und ihre verwendung
US10421051B2 (en) 2014-08-19 2019-09-24 Evonik Degussa Gmbh Hybrid dispersion and use thereof

Also Published As

Publication number Publication date
EP1785252B1 (de) 2008-09-03
ES2313532T3 (es) 2009-03-01
EP1785252A1 (de) 2007-05-16
US20070112083A1 (en) 2007-05-17
US8748514B2 (en) 2014-06-10
DE502006001485D1 (de) 2008-10-16

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