DE2437090A1 - Reinigungsmittel - Google Patents
ReinigungsmittelInfo
- Publication number
- DE2437090A1 DE2437090A1 DE2437090A DE2437090A DE2437090A1 DE 2437090 A1 DE2437090 A1 DE 2437090A1 DE 2437090 A DE2437090 A DE 2437090A DE 2437090 A DE2437090 A DE 2437090A DE 2437090 A1 DE2437090 A1 DE 2437090A1
- Authority
- DE
- Germany
- Prior art keywords
- sodium
- cleaning agent
- liquid
- weight
- solubilizers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic System
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/54—Quaternary phosphonium compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/886—Ampholytes containing P
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/36—Organic compounds containing phosphorus
- C11D3/361—Phosphonates, phosphinates or phosphonites
Description
HOECHST AKTIENGESELLSCHAFT , . 243/090
Aktenzeichen: HOE 74/F 219
Datum: 29- Juli 197^ Dr. GR/stl
Datum: 29- Juli 197^ Dr. GR/stl
Reinigungsmittel
Die Erfindung betrifft pulverförmige oder flüssige wäßrige Reinigungsmittel-Konzentrate
für die Verwendung in Haushalt und Industrie.
Moderne Reinigungsmittel für die Reinigung von Oberflächen nicht
textiler Materialien, die sowohl zur Reinigung von Hand als auch
in modernen Reinigungsanlagen, wie z.B. Strahlreinigungsanlagen, ,
Heißwassergeräten, DampfStrahlgeräten und dergleichen, als flüssige
oder pulverförmige Industrie- und Haushaltsreiniger, flüssige Geschirreiniger und flüssige Schwerwaschmittel eingesetzt, bestehen
im wesentlichen aus. nichtionischen, anionischen und/oder amphoteren Tensiden, Gerüststoffen und Lösungsvermittlern.
Die Mitverwendung von LösungsVermittlern ist erforderlich, wenn
derartige Reinigungsmittel als konzentrierte flüssige Zubereitungen hergestellt werden. Ihre Mitverwendung ist auch bei solchen pulverförmigen
oder pastenförmigen Reinigungsmitteln erforderlich, die in Form von konzentrierten wäßrigen Stammlösungen eingesetzt
v/erden sollen, wie das z.B. bei modernen Strahlreinigungsgeräten oder Plüssig-Dosiergeräten der Fall ist.
6O9808/O97S
Die Verwendung von Lösungsvermittlern ist dort vor allem erforderlich,
weil die nichtionischen und anionischen Tenside in wäßrigen-,
Gerüststoffe enthaltenden Lösungen nicht ausreichend löslich sind. Bereits bei relativ niedrigem Gehalt der wäßrigen Lösungen an"
Gerüststoffen oder anderen Elektrolyten separieren die Tenside aus "der Lösung. Durch Zusatz geeigneter Lösungsvermittler gelingt es,
die Löslichkeit dieser Tenside in wäßrigen Lösungen von Gerüststoffen zu verbessern. Als Lösungsvermittler für anionische Tenside
sind bisher vor allem Alkalisalze von Paratoluolsulfonsäure,
Xylolsulfonsäure und Cumolsulfonsäure bekannt geworden. Bekannte Lösungsvermittler für nichtionische Tenside sind primäre und
sekundäre Phosphorsäureester von Fettalkoholpolyglykoläthern und Alkylphenolpolyglykoläthern (vgl. Soap and Chemical Specialities
Mai 1969, Seiten 86 bis 93). Die hydrotropen Eigenschaften der
bekannten LösungsVermittler sind jedoch nur schwach ausgeprägt und
ihre Wirkung reicht nicht aus, um die zur Herstellung von Reinigungsmitteln-Konzentraten
erforderlichen Mengen der Tenside in Gegenwart hoher Elektrolytkonzentrationen klar zu lösen bzw. zu dispergieren.
So werden z.B., um etwa 3 Gewichtsteile eines nichtionischen Tensids in 100 Teilen eines wäßrigen Reinigungsmittel-Konzentrats entsprechend
etwa der folgenden Zusammensetzung:
Laurylalkoholnonaglykolather 3 Teile
Natriumtripolyphosphat 10 Teile
Trinatriumphosphat 5 Teile
Natriummetasilikat 5 Teile
Kaliumhydroxid 2 Teile
Wasser ■ 75 Teile
etwa 5 Gewichtsteile eines Phosphorsäuremono-Zdiesters von Nonylphenoltetraglykoläther
oder eines Phosphorsäuremono-/diesters von Laurylalkoholtetraglykoläther benötigt. Zur Bereitung eines flüssigen
Reinigungskonzentrates auf Basis eines anionischen Tensides wie die folgenden typischen Formulierungen anionischer Reiniger-Konzentrate
zeigen, je nach Anteil des Pyrophosphat-Gerüststoffes 2 bzw.
10 Gewichtsprozent Natrium-paratoluolsulfonat eingesetzt werden.
609808/0975 BAD ORIGINAL
sek. Alkansulfonat-Natrium (C1, - C-g) . 10 % 10 %
Nonylphenoldekaglykoläther ~b % _ 3 %
Kokosfettsäuremonoäthanolamidpentaglykoläthör 2 % 2 %
Tetrakaliumpyrophosphat ' 10 $ 20 %
p.-Toluolsulfonat-Natrium 2 %■' 10 %
Ammoniak - 1 % 1 %
Wasser 72 % 5^ %
Die zur Stabilisierung der nichtiortisch'en und anionischen Waschrohstoffe
in hohen Elektrolyt-Konzentrationen aufweisenden wäßrigen Lösungen erforderlichen Mengen dieser Lösungsvermittler sind, wie
die vorstehenden Beispiele zeigen, beachtlich und führen zu einer negativen Beeinflussung der Eigenschaften der Reinigungsmittel,
wie z.B. des Schaumverhaltens; sie stellen darüberhinaus eine zusätzliche Abwasserbelastung dar und verursachen außerdem erhebliche
Kosten. . .
Es wurde nun gefunden, daß Verbindungen der'allgemeinen Formel I
R-P-OY
OX (I)
in der R einen geradkettigen oder verzweigten Alkyl- oder Alkenylresfc
mit 6 bis 1*1, vorzugsweise 8 bis 10 Kohlenstoffatomen, X und
Y Wasserstoff, Alkali, den Ammoniumrest oder einen Äthanolaminrest "
bedeuten, ausgezeichnete, den bekannten LösungsVermittlern überlegene
hydrotrope Eigenschaften gegenüber nichtionischen und anionischen oberflächenaktiven Verbindungen besitzen und deshalb
mit besonderem Vorteil als Lösungsvermittler zur Herstellung pulverförmiger oder flüssiger Reinigungsmittel-Konzentraten auf
Basis nich'tionischer und/oder anionischer oberflächenaktiver Verbindungen geeignet sind..
Die Erfindung betrifft weiterhin pulverförmige oder flüssige Reinigungsmittel-Konzentrate auf Basis anionischer, nichtionischer
und/oder amphoterer oberflächenaktiver Verbindungen, die gekennzeichnet
sind durch einen Gehalt an Phosphonsäurederivaten der allgemeinen Formel I
98Ö8/Q97
.jf. 7437090
ο Η
Il
R-P-OY (I)
R-P-OY (I)
OX
in der R, X und Y die vorstehend genannten Bedeutungen besitzen.
Die Zusammensetzung der pulverförmigen oder flüssigen Reinigungsmittel-Konzentrate
gemäß der Erfindung kann jedoch-nach dem Verwendungszweck in weiten Grenzen variieren. Der Gehalt der Reinigungsmittel-Konzentrate
an Waschaktivsubstansen (WAS) d.h. der Gehalt an nichtionischen, anionischen und amphoteren Tensiden
zusammengenommen, beträgt im allgemeinen etwa 1 bis 20, vorzugsweise
2 bis 12 Gewichtsprozent und ihr Gehalt an Phosphonsäurederivaten der Formel I etwa 0,5 bis 5>
vorzugsweise 1,0 bis 3,0 Gewichtsprozent.
Handelt es sich bei den Reinigungsmittel-Konzentraten der Erfindung
um flüssige Einstellungen, so beträgt der Wassergehalt im allgemeinen etwa 65 bis 85 Gewichtsprozent. Diese flüssigen Konzentrate
werden durchweg alkalisch, vorzugsweise auf pH-Werte im Bereich von etwa 8 bis 1Ü eingestellt.
Neben den nichtionischen, anionischen und/oder amphoteren Tensiden
und den Phosphonsäurederivaten der Formel T enthalten die Reinigungsmittel-Konzentrate
gemäß der Erfindung üblicherweise als Gerüstsubstanzen und Additive bezeichnete Produkte, wie sie z.B. in dem
Standardwerk Schwartz. Perry, Berch, "Surface Active Agents and Detergents", Vol. 2, (1958), Seiten 288 bis 317 beschrieben sind.
Der Anteil dieser Gerüstsubstanzen und Additive in den Reinigungsmittel-Konzentraten
beträgt im allgemeinen bis zu 35 Gewichtsprozent, insbesondere 5 bis 30 Gewichtsprozent. Als solche Gerüstsubstanzen
kommen vor allem Alkaliortho- und-polyphosphate wie z.B. Natriumtripolyphosphat, Natriumpyrophosphat, Natriummetaphosphat
und die entsprechenden Kaliumsalze in Mengen bis zu etwa 25 Gew.-JS,
vornehmlich 8 bis l8 Gew.-%, zur Anwendung. Weitere Zusatzstoffe
dieser Art sind organische Komplexbildner, wie z.B. Alkalisalze von Ethylendiamintetraessigsäure, Trinatriumcitrat oder Alkalisalze
der Nitrilotriessigsäure, die in Mengen bis zu etwa 20 Gew.-/?,
8/0975
insbesondere bis zu etwa 12 Gew.-5S3 in den Reinigungsmitteln enthalten
sein können. Als solche Zusatzstoffe kommen ferner Alkalisilikate wie z.B. Natriummetalsilikat oder Natriumdi- oder trisilikat
in Mengen bis zu etwa 10 Gew.-%s insbesondere bis zu etwa
8 Gew.-? in Betracht.
Niehtionogene, oberflächenaktive Produkte,· wie sie in den Reinigungsmittel-Konzentraten'
gemäß der Erfindung enthalten sein können, werden z.B. beschrieben in dem Standardwerk Schwartz, Perry,
Berch "Surface Active Agents and. Detergents", Vol. II, (1958),
Seiten 120 bis 138. Bevorzugt verwendete niehtionogene Waschrohstoffe
sind z.N.
a. Alkylphenolpolyglykolätherj besonders solche mit 8 bis 12 Kohlenstoffatomen
im Alkylrest und einem Gehalt an etwa 4 bis 15 Oxyäthyleneinheitenj
b. geradkettige oder verzweigte, primäre oder' sekundäre Alkyl-
. polyglykoläther, besonders solche, deren Alkylreste etwa 8 bis
20 Kohlenstoffatome umfassen und die etwa 4 bis 20 Oxäthyleneinheiten
im Molekül enthalten, " .
c. Propylenoxid-Ä'thylenoxid-Blockpolymerisate, besonders die Anlagerungsverbindungen
von etwa 5 bis 20 Molen Äthylenoxid an 1 Mol
Propylenglykol vom Molgewicht von etwa 1800 bis 3000,
d. Alkylamin-Oxyäthylate, besonders, solche mit Alkylresten von etwa
10 bis 20 Kohlenstoffatomen und etwa 4 bis 15 A'thylenglykoläthergruppen
im Molekül sowie
■ . ι
e. Fettsäureoxäthylate, besonders solche mit Alkylresten von etwa 8 bis 20 Kohlenstoffatomen und etwa 4 bis 15 Oxyäthylenglykol-
Xäthergruppen im Molekül. ■
Als anionische oberflächenaktive Produkte kommen in den Reinigungsmittel-Konzentraten
vor allem solche vom Sulfonat- oder Sulfattyp in Betracht. In erster Linie handelt es sich hierbei um Alkansulf
onate, wie aus n-Alkanen durch Sulfogilorierung oder SuIfoxida-
tion und anschließende Hydrolyse bzw. Neutralisation oder durch : Bisulfataddition an Olefine erhältlich sind, um Olefinsulfonate j
wie sie beispielsweise durch Sulfonierung primärer oder sekundärer !
aliphatischer Monoolefine mit gasförmigem Schwefeltrioxid und anschließende alkalische oder saure Hydrolyse erhalten werden,
sowie Alkylbenzolsulfonate, beispielsweise n-Dodecylbenzolsulfonat.
Geeignet sind ferner ^- -SuIfofettsäureester, primäre und sekundäre
Alkylsulfate sowie die Sulfate von äthoxylierten oder propoxylierten
höhermolekularen Alkoholen. Ferner kommen Sulfate von äthoxylierten
oder propoxylierten Fettsäureamiden und Alkylphenolen sowie Fettsäuretauride
und Fettsäureesäthionate in Frage. Geeignete anionische Tenside sind weiterhin Alkaliseifen von Fettsäuren natürlichen oder
synthetischen Ursprungs, z.B. die Natriumseifen von Kokos-, Palmkernoder Talgfettsäuren. Einen Überblick über die in Betracht kommenden
anionischen Tensiden gibt beispielsweise das Standard, Schwartz, Perry, Berch "Surfa.ce Active Agents and Detergents" Vol. II, 1958
Seiten 25 bis 102. Die anionsichen Tenside können in Form der Natrium-, Kalium- oder Ammoniumsalze oder auch als Salze organischer
Basen, wie Mono-, Di- oder Triäthanolamin, vorliegen.
Die als Bestandteile der Reinigungsmittel-Konzentrate in Betracht kommenden amphoteren Tenside werden z.B. in Surface Active Agents
and Detergents in "Vol. II (1958), Seiten 138 bis 1^3 beschrieben.
Solche Tenside sind beispielsweise Alkylbetaine und insbesondere Alky!sulfobetaine, z.B. das 3-(N,N-dimethyl-N-alkyla.mmonium)-propan-1-sulfonat.
Die Reinigungsmittel-Konzentrate gemäß der Erfindung können ferner
auch Alkalilaugen in Mengen bis zu etwa 15 Gew.-^, vornehmlich bis
zu 8 Gew.-%s sowie erforderlichenfalls weitere übliche Hilfsstoffe
enthalten.
Die als Lösungsvermittler in den Reinigungsmittel-Konzentraten gemäß der Erfindung verwendeten Phosphonsäurederivate der Formel I
weisen neben den hervorragenden hydrotropen Eigenschaften überraschenderweise auch eine gute Beständigkeit gegenüber Alkalilaugen
auf; sie sind im allgemeinen in einer Konzentration von z.B. 10 g/l
8/0975
in einer 25 #igen Natronlauge bie Raumtemperatur noch klar löslich.
Von besonderem technischen Interesse ist jedoch vor allem das
Vermögen der genannten Phosphonsäurederivate, nichtionischen und anionischen oberflächenaktiven Produkten eine ausreichende Beständigkeit
in salzhaltigen Lösungen und insbesondere auch in Lösungen . mit hohem Anteil an Natriumsalzen kondensierte Phosphorsäuren
zu verleihen. Der Anteil des als Lcsungsvermittler verwendeten Verbindungen der Formel I in den Reinigungsmittel-Konzentraten
gemäß der Erfindung wird insbesondere aus wirtschaftlichen Gründen
so niedrig wie möglich gehalten. Durch eine ausreichende hydrotrope Wirkung der Verbindungen der Formel I erforderliche Menge ist in
erster Linie von der Zusammensetzung der Konzentrate, besonders vom Ionengehalt an WAS und Elektrolyten abhängig. Im allgemeinen
kann davon ausgegangen werden, daß bezogen auf die Gewichtsmenge an WAS, in Abhängigkeit von dem Elektrolytgehalt, etwa 1 bis 50 %
der Phosphonsäurederivate der Formel I anzuwenden sind. Gegenüber den bisher bekannten Lösungsvermittlern besitzen die Phosphonsäurederivate
der Formel I den Vorteil, daß sie sowohl für Reiniger auf Basis von nichtionischen Tensiden als auch für Reiniger auf
Basis von anionsichen Tensiden geeignet sind. Mit den neuen Lösungsvermittlern gemäß der Erfindung lassen sich in vielen Fällen,
z.B. bei Reinigern mit sehr hohen Elektrolytgehalten, auch dann noch beständige wäßrige Lösungen einstellen, wenn die bekannten
Lösungsvermittler versagen. Die bessere Wirksamkeit der erfindungsgemäß verwendten Phosphonsäurederivate der Formel I zeigt sich auch
darin, daß von ihnen im Vergleich zu den bekannten Lösungsvermittlern eine deutlich geringere Menge ausreicht, um vergleichbare
Effekte zu erzielen.
So werden z.B. bei der weiter oben genannten typischen Formulierung
eines flüssigen Reinigungsmittel-Konzentrates auf Basis eines nichtionischen Tensids, bestehend aus
3 Gewichtsteilen . Laurylalkoholnonaglykoäther j '
10 Gewichtsteilen Pentanatriumphosphat 5 Gewichtsteilen' Trinatriumphosphat
5 Gewichtsteilen Natriummetasilikat 2 Gewichtsteilen Hydroxid
609-8 08/0975
und
75 Gewichtsteilen Wasser anstelle von 5 Gewichtsteilen eines üblichen Lösungsvermittlers nur I1I Gewichtsteile n-Octanphosphonsäure
benötigt um eine klare, stabile Lösung herzustellen.
In gleicher Weise werden für die vorstehend ebenfalls bereits erwähnten typischen Formulierungen von flüssigen Reinigungsmittel-Konzentraten
auf Basis anionischer Tenside, wie die nachstehenden Zusammensetzungen zeigen, bei Verwendung von z.B. n-Octanphosphonsäuren
gegenüber p-Toluolsulfonat-natrium auf nur die Hälfte oder
weniger als die Hälfte an Lösungsvermittler benötigt:
Gewichtsteile | 10,0 | |
sec. Alkansulfonat-Natriμm (^^ύ'^λά) | 10,0 | 3,0 |
Nonylphenoldekaglykoläther | 3,0 | 2,0 |
Kokosfettfäuremonoäthanolamidpenta- | 2,0 | |
glykoiäther | 20,0 | |
Tetrakaliumpyrophosphat | 10,0 | 1,0 |
Ammoniak | 1,0 | 3,5 |
n"Oktanphosphonsäure | 0,5 | 60,5 |
Wasser | 73,5 |
In der nachfolgenden Gegenüberstellung wird für einige Reinigungsmittel-Systeme
die jeweils zur Bereitung klarer, stabiler Lösungen erforderliche Menge an Lösungsvermittlern nach dem Stand der Technik
und gemäß der Erfindung aufgeführt. Bei den folgenden Reinigern handelt es sich um flüssige Einstellungen deren Zusammensetzungen
zunächst ohne Berücksichtigung der Lösungsvermittler in Gewichtsprzenten angegeben sind. Die bei den Lösungsvermittlern aufgeführten
Zahlen geben an, wieviel Prozent, bezogen auf das Gewicht der Lösungen des jeweiligen LösungsVermittlers erforderlich sind, um
klare stabile Lösungen zu erzielen. Dabei bedeutet das Zeichen daß mit der angegebenen Menge des betreffenden Lösungsvermittlers
klare Lösungen noch nicht erreicht werden konnten.
Beispiel 2, flüssige Reiniger Nonylphenolmonoglykoläther K11P2O7
a. | b. |
5 | 10 |
10 | 10 |
€09808/0975
243709Q
Lösungsvermittler:
Mono-/Diphosphorsäureester von Nonylphenol- 5,6 10,0
monoglykoläther . ·
Natrium-Xylolsulfonat Kalium-Xylolsulfonat
Natrium-Dodecyldiphenyläthersulfonat"
Natrium-p-Toluolsulfonat Kalium-p-Toluolsulfonat
n-Octanphosphorsäure
n-Decanphosphorsäure n-Tetradecanphosphorsäure
C8H17PO3HNa
C8H17PO3Na2.
C8H17PO3KH ·
C8H17PO3HN(C2H4OH)3
CgH17PO HNH(C2H4OH)2
CgH17PO3HNH2C2H4OH
Beispiel 3, flüssige Reiniger Cq-C11-Alkohol-heptaglykoläther
Na5P3°10
Na3PO4
Na3PO4
Lösungsvermittler: Natrium-p-Toluolsulfonat Natrium-Xylolsulfonat Mono-/Diphosphorsäureester eines
C10-C 4 Alkohol-hexaglykoläthers
n-Oktanphosphorsäure
n-Dekanphosphorsäure n-Tetradekanphosphorsäure
Beispiel 4, flüssiges Waschmittel C12-C1J- Alkohol-monoglykoläther
Kokosfettsäuremonoäthanolamidpentaglykoläther Natriumeitrat . 2 H3O
Na3SiO-,
KOH
KOH
6(19808/0975
6 | ,3 | |
4,7 | 10 | ,2 |
4,0 | 10 | ,0 |
5,4 | 10 | ,0 |
5,6 | 10 | ,2 |
1,2 | 1 | ,8 |
0,8 | 1 | ,0 |
1,2 | . 1. | ,3 |
1,3 | 1 | ,7 |
1,0 | 1 | ,5, |
1,5 | 2 | ,2 |
2,0· | 3 | ,5 |
2,0 | 3 | ,5 |
2,0 | 3 | ,5 |
2,0 | 3 | ,0 |
5 | • | |
14 | ||
6 | ||
20 | ||
!5 | ||
15 | ||
2,1 | ||
2,3 | ||
3,0 | ||
10,0 | ||
2,0 | ||
20,0 | ||
5,0 | ||
1,0 |
Lösungsvermittler:
Natrium-p-Toluolsulfonat Natrium-Xylolsulfonat n-Oktanphosphorsäure
Natrium-p-Toluolsulfonat Natrium-Xylolsulfonat n-Oktanphosphorsäure
243709Π
20,0 20,0
4,5
Beispiel 5, Druckstrahlreiniger Cq-C11-Alkohol-heptaglykoläther
Na PO11
Na2SiO,
Na2CO
Atfiylendiamintetraessigsaure
5,0
10,0 5,0 5,0 3,0 1,0
Lösungsvermittler:
Natrium-p-Toluolsulfonat Natrium-Xylolsulfonat n-Oktanphosphorsäure
Natrium-p-Toluolsulfonat Natrium-Xylolsulfonat n-Oktanphosphorsäure
17,0 20,0
3,5
Zur weiteren Erläuterung der Erfindung werden nachfolgend noch
Beispiele für flüssige und pulverförmige Reinigungsmittel-Konzentrate gegeben. Die Konzentrate werden durch einfaches Mischen mit der Komponenten hergestellt. Die Prozentangaben bedeuten in allen Fällen Gewichtsprozente.
Beispiele für flüssige und pulverförmige Reinigungsmittel-Konzentrate gegeben. Die Konzentrate werden durch einfaches Mischen mit der Komponenten hergestellt. Die Prozentangaben bedeuten in allen Fällen Gewichtsprozente.
Beispiel 6, flüssige Reiniger %
Nonylphenol + 9 Mol AeO | 2,0 | .1,0 | 6,0 |
Na5P3O10 | 12,5 | 12,5 | 12,5 |
Na3SiO3 | 10,0 | 10,0 | 10,0 |
KOH | 2,5 . | 2,5 | 2,5 |
n-Oktanphosphonsäure | 1,0 | 1,3 | 1,6 |
Wasser | 71,0 | 69,7 | 67,4 |
/0975
?43709Γ)
Beispiel 7, flüssige Reiniger
C -C ^-Alkohol + 9 Mol AeO
Na5P3O10
Na3SiO3
n-Oktanphosphonsäure
Wasser
2,0 | 4,0 | 6 | ,0 |
10,0 | 10,0 | 10 | ,0 |
8,0 | 8,0 | 8 | ,0 |
2,0 | 2,0 | 2 | ,0 |
0,8 | 1,2 | 1 | ,8 |
77,2 | 7^,8 | 72 | ,2 |
Beispiel 8, pulverförmiger Dampfstrahl- und Hochdruckreiniger
-Alkohol-pentaglykoläther 18,5 %
24,7 % 24,7 %
Cq-C .
Na5P3O10
Na3PO4 Natriumwasserglas (Verhältnis
Na2O
SiO2 = 1:3,3)
n-Oktanphosphonsäure
24,7 % 7,4 %
27 g dieses pulverförmigen Reinigers lösen sich in 73 g Wasser
zu einer klaren stabilen Lösung.
Beispiel 9, Autoreiniger in Pulverform
-Alkohol-heptaglykoläther 15,0 %
-Alkohol-pentaglykoläther
9 Il
C9"Cii
Na3PO4 !
Natriumsalz der Nitrilotriessigsäure KOH
n-Oktanphosphonsäure
n-Oktanphosphonsäure
5,0 % 23,0 % 50,0 %
2,0 % 5,0 %
20 g dieses Reinigers lösen in 80 g Wasser zu einer klaren stabilen
Lösung.
Beispiel 10, Druckstrahlreiniger in Pulverform Cq-C11-Alkohol-heptaglykoläther 12,0 %
CQ-C11-Alkohol-pentaglykoläther
Na5P3O10
Na3PO4 sekundäres C^-C^-Alkansulfonatnatrium
KOH
6,0 % 50,0 % 20,0 %
5,0 % 2,0 %
β 0 9808/097 S-
n-Oktanphosphonsäure 5,0 %
10 g dieses Reinigers lösen sich in 90 g Wasser zu einer klaren stabilen Lösung.
Beispiel 11, pulverförmiger Geschirreiniger für Spulautomaten
(Angaben in Gew.-%)
Na5P3O10 38,1 38,1 38,1 38,1
Na3PO4 15,9 15,9
Na3PO4 . 10 H2O - -' 15,9 15,9
Na2SiO3 24,3 24,3
Na2SiO3 . 5 H2O - - 25,3 25,3
KOH 6,4 6,4 6,4 6,4
Tensid 1 3,2 - 3,2
Tensid 2 - 3,2 - 3,2
Kalium-Dichloriso-
cyanurat 1,0 1,0
n-Oktanphosphonsäure 11,1 11,1 11,1 11,1
klare, stabile wäßrige Lösungen dieser Reiniger lassen sich herstellen bis
zu folgenden Maximalkonzentrationen
zu folgenden Maximalkonzentrationen
20 % 25 % 30 % 30 %
Tensid 1 = Anlagerungsverbindung von 4 Molen Äthylenoxid an 1 Mol eines Polypropylenglykols vom Molgewicht I8OO
Tensid 2 = Umsetzungsprodukt von 1 Mol eines C10-C14-Fettalkohols
mit 15 Molen Propylenoxid und 12 Molen Äthylenoxid.
(609808/0975
Claims (1)
- Patentansprüche(l\ Pulverförmige oder flüssige Reinigungsmittel-Konzentrate auf Basis nichtionischer, anionischer und/oder amphoterer Tenside, gekennzeichnet durch einen Gehalt an Verbindungen der allgemeinen Formel I ■O
R-P-OY (I)in der R einen geradkettigen oder verzweigten Alkyl- oder Alkenylrest mit 6 bis lH Kohlenstoffatomen, X und Y Wasserstoff-, Alkali, das Ammoniumion oder ein Kthanolaminion bedeuten, als Lösungsvermittler.2,. Pulverförmige oder flüssige, Reinigungs.mittel-Konzentr,ate nach Anspruch 1, dadurch gekennzeichne,t, da.ß sie 0,5 b,isu § Ggy.-%: einer.. Verbindung der Formel I enthalten.]5. Pulverförmige od. er. flüssise, le^n.igupg^mitt.ei-Konzen.tij.ate, nach Anspruch, 2, dadurch geke^rize.ic,h.n,et:, df|f3> s,i§ §4η—£ Gehalt y;pn et^a 1 bis 20 Gevi.-JS an nicht ionischen, anipnis.c,h,en, und/>pde:£ amp^oteren Tens.idetn, s.ovi,ie außerden bis z.u 35: Sew..-| (Se^usit^ubstanZ.^ un^. gegebenenfalls organlsc.^en Kpinp.le^xbilde^r.fl, Alkalilauge ag$i«| ieiter-,§ üb.Uc,he Iiilfs,s;tpffe e^tb,%lt§^.\. Verwendung von. Verbindungen der; a.llgemqinep, ^pr.m§l I· gemM Anspruch 1, als hydrat.r,o,p,e Substanz in pMlyesr^riniigea pcjer, flüssigen Reinigun.gsmittel-Kpflzentr.aten auf la,sis aniqnisc^ii, iiic.htip.iais.cher., pder, spph;p.tf.r,er: ^Pen.sigle.INSPECTED
Priority Applications (19)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2437090A DE2437090A1 (de) | 1974-08-01 | 1974-08-01 | Reinigungsmittel |
US493953A US3929678A (en) | 1974-08-01 | 1974-08-01 | Detergent composition having enhanced particulate soil removal performance |
NL7508895A NL7508895A (nl) | 1974-08-01 | 1975-07-25 | Reinigingsmiddelen. |
AT581175A AT344301B (de) | 1974-08-01 | 1975-07-28 | Reinigungsmittel |
DE2533758A DE2533758C2 (de) | 1974-08-01 | 1975-07-29 | Waschmittel |
CH988275A CH614462A5 (en) | 1974-08-01 | 1975-07-29 | Cleaner concentrate |
NL7509077A NL7509077A (nl) | 1974-08-01 | 1975-07-30 | Werkwijze voor het bereiden van een wasmiddel met sterke, fijnverdeeld vuilverwijderende werking. |
GB31887/75A GB1522981A (en) | 1974-08-01 | 1975-07-30 | Detergent compositions |
LU73103A LU73103A1 (de) | 1974-08-01 | 1975-07-30 | |
IT25934/75A IT1040248B (it) | 1974-08-01 | 1975-07-30 | Mezzi di pulitura |
BE158838A BE831995A (fr) | 1974-08-01 | 1975-07-31 | Composition detergente ayant des performances ameliorees d'enlevement de salissures particulaires |
FR7523931A FR2280706A1 (fr) | 1974-08-01 | 1975-07-31 | Concentres d'agents de nettoyage |
JP50092622A JPS5137902A (de) | 1974-08-01 | 1975-07-31 | |
GB32084/75A GB1507083A (en) | 1974-08-01 | 1975-07-31 | Detergent composition having enhanced particulate soil removal performance |
FR7524026A FR2280705A1 (fr) | 1974-08-01 | 1975-07-31 | Composition detergente ayant des performances ameliorees d'enlevement de salissures particulaires |
IE1713/75A IE41438B1 (en) | 1974-08-01 | 1975-07-31 | Detergent compositions |
DK348875A DK348875A (da) | 1974-08-01 | 1975-07-31 | Pulverformige eller flydende, alkalisk indstillede rensemiddelkoncentrater samt fremgangsmade til fremstilling deraf |
SE7508754A SE7508754L (sv) | 1974-08-01 | 1975-08-01 | Rengoringsmedel |
BE158875A BE832048A (fr) | 1974-08-01 | 1975-08-01 | Concentres d'agents de nettoyage |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2437090A DE2437090A1 (de) | 1974-08-01 | 1974-08-01 | Reinigungsmittel |
US493953A US3929678A (en) | 1974-08-01 | 1974-08-01 | Detergent composition having enhanced particulate soil removal performance |
Publications (1)
Publication Number | Publication Date |
---|---|
DE2437090A1 true DE2437090A1 (de) | 1976-02-19 |
Family
ID=25767502
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE2437090A Pending DE2437090A1 (de) | 1974-08-01 | 1974-08-01 | Reinigungsmittel |
DE2533758A Expired DE2533758C2 (de) | 1974-08-01 | 1975-07-29 | Waschmittel |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE2533758A Expired DE2533758C2 (de) | 1974-08-01 | 1975-07-29 | Waschmittel |
Country Status (7)
Country | Link |
---|---|
US (1) | US3929678A (de) |
BE (2) | BE831995A (de) |
DE (2) | DE2437090A1 (de) |
FR (2) | FR2280705A1 (de) |
GB (1) | GB1507083A (de) |
LU (1) | LU73103A1 (de) |
NL (2) | NL7508895A (de) |
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Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1119884A (en) * | 1966-06-13 | 1968-07-17 | Unilever Ltd | Controlled sudsing compositions |
CA813301A (en) * | 1966-09-06 | 1969-05-20 | E. Zimmerer Roger | Detergent composition |
BE754502A (fr) * | 1969-08-07 | 1971-01-18 | Bayer Ag | Procede de teinture de matieres fibreuses azotees |
GB1315363A (en) * | 1970-05-29 | 1973-05-02 | Unilever Ltd | Liquid detergents |
GB1441588A (en) * | 1972-10-04 | 1976-07-07 | Unilever Ltd | Rinse composition |
-
1974
- 1974-08-01 US US493953A patent/US3929678A/en not_active Expired - Lifetime
- 1974-08-01 DE DE2437090A patent/DE2437090A1/de active Pending
-
1975
- 1975-07-25 NL NL7508895A patent/NL7508895A/xx not_active Application Discontinuation
- 1975-07-29 DE DE2533758A patent/DE2533758C2/de not_active Expired
- 1975-07-30 NL NL7509077A patent/NL7509077A/xx not_active Application Discontinuation
- 1975-07-30 LU LU73103A patent/LU73103A1/xx unknown
- 1975-07-31 FR FR7524026A patent/FR2280705A1/fr active Granted
- 1975-07-31 BE BE158838A patent/BE831995A/xx not_active IP Right Cessation
- 1975-07-31 FR FR7523931A patent/FR2280706A1/fr active Granted
- 1975-07-31 GB GB32084/75A patent/GB1507083A/en not_active Expired
- 1975-08-01 BE BE158875A patent/BE832048A/xx unknown
Also Published As
Publication number | Publication date |
---|---|
FR2280705B1 (de) | 1978-10-13 |
FR2280706A1 (fr) | 1976-02-27 |
LU73103A1 (de) | 1977-03-24 |
NL7509077A (nl) | 1976-02-03 |
GB1507083A (en) | 1978-04-12 |
FR2280706B1 (de) | 1978-12-08 |
DE2533758A1 (de) | 1976-02-12 |
BE831995A (fr) | 1976-02-02 |
BE832048A (fr) | 1976-02-02 |
DE2533758C2 (de) | 1984-03-01 |
NL7508895A (nl) | 1976-02-03 |
US3929678A (en) | 1975-12-30 |
FR2280705A1 (fr) | 1976-02-27 |
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