DE60023023T2 - Zirkoniumdioxidsol und verfahren zu seiner herstellung - Google Patents

Zirkoniumdioxidsol und verfahren zu seiner herstellung Download PDF

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Publication number
DE60023023T2
DE60023023T2 DE60023023T DE60023023T DE60023023T2 DE 60023023 T2 DE60023023 T2 DE 60023023T2 DE 60023023 T DE60023023 T DE 60023023T DE 60023023 T DE60023023 T DE 60023023T DE 60023023 T2 DE60023023 T2 DE 60023023T2
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DE
Germany
Prior art keywords
dioxideol
zirconium
production
zirconium dioxideol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60023023T
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English (en)
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DE60023023D1 (de
Inventor
U Kolb
T Chien
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3M Innovative Properties Co
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3M Innovative Properties Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Publication of DE60023023D1 publication Critical patent/DE60023023D1/de
Application granted granted Critical
Publication of DE60023023T2 publication Critical patent/DE60023023T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0004—Preparation of sols
    • B01J13/0008—Sols of inorganic materials in water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2244—Oxides; Hydroxides of metals of zirconium
DE60023023T 1999-10-28 2000-04-03 Zirkoniumdioxidsol und verfahren zu seiner herstellung Expired - Lifetime DE60023023T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/428,374 US6376590B2 (en) 1999-10-28 1999-10-28 Zirconia sol, process of making and composite material
PCT/US2000/008796 WO2001030702A1 (en) 1999-10-28 2000-04-03 Zirconia sol and process of making same

Publications (2)

Publication Number Publication Date
DE60023023D1 DE60023023D1 (de) 2006-02-16
DE60023023T2 true DE60023023T2 (de) 2006-06-14

Family

ID=23698626

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60023023T Expired - Lifetime DE60023023T2 (de) 1999-10-28 2000-04-03 Zirkoniumdioxidsol und verfahren zu seiner herstellung

Country Status (7)

Country Link
US (1) US6376590B2 (de)
EP (1) EP1232118B1 (de)
JP (1) JP4559004B2 (de)
AU (1) AU4065200A (de)
CA (1) CA2388876C (de)
DE (1) DE60023023T2 (de)
WO (1) WO2001030702A1 (de)

Families Citing this family (206)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7476889B2 (en) * 1998-12-07 2009-01-13 Meridian Research And Development Radiation detectable and protective articles
US20090000007A1 (en) * 1998-12-07 2009-01-01 Meridian Research And Development, Inc. Nonwoven radiopaque material for medical garments and method for making same
US6194481B1 (en) * 1999-05-19 2001-02-27 Board Of Regents Of The University Of Texas System Mechanically strong and transparent or translucent composites made using zirconium oxide nanoparticles
CA2387215C (en) * 1999-10-28 2010-02-09 3M Innovative Properties Company Dental materials with nano-sized silica particles
WO2002014433A1 (fr) * 2000-08-11 2002-02-21 Sun Medical Co., Ltd. Composition polymerisable, objet durci obtenu a partir de cette composition, et materiau composite
US6982073B2 (en) * 2001-11-02 2006-01-03 Altair Nanomaterials Inc. Process for making nano-sized stabilized zirconia
CA2473861C (en) * 2002-01-31 2012-03-13 3M Innovative Properties Company Dental pastes, dental articles, and methods
DE10219879A1 (de) * 2002-05-03 2003-11-20 Basf Ag Katalysatorträger und Verfahren zu seiner Herstellung
US7091259B2 (en) * 2002-07-03 2006-08-15 3M Innovative Properties Company Dental fillers, pastes, and compositions prepared therefrom
DE50212920D1 (de) * 2002-08-30 2008-11-27 Itn Nanovation Ag Pulverteilchen
US7288324B1 (en) 2002-09-05 2007-10-30 University Of Central Florida Research Foundation, Inc. Synthesis of tetragonal phase stabilized nano and submicron sized nanoparticles
US7297731B2 (en) * 2003-03-11 2007-11-20 3M Innovative Properties Company Coating dispersions for optical fibers
TWI252215B (en) * 2003-03-27 2006-04-01 Univ Nat Central Zirconia sol and method of preparing the same
US7289202B2 (en) 2004-09-10 2007-10-30 3M Innovative Properties Company Methods for testing durable optical elements
US7282272B2 (en) * 2003-09-12 2007-10-16 3M Innovative Properties Company Polymerizable compositions comprising nanoparticles
US7074463B2 (en) * 2003-09-12 2006-07-11 3M Innovative Properties Company Durable optical element
DE10359659A1 (de) * 2003-12-18 2005-07-21 Institut für Neue Materialien Gemeinnützige GmbH Verwendung von nanoskaligen ZrO2-Teilchen
US7803347B2 (en) * 2005-07-01 2010-09-28 Tohoku Techno Arch Co., Ltd. Organically modified fine particles
DE102004008275A1 (de) * 2004-02-18 2005-09-15 Heraeus Kulzer Gmbh Dispersionen nanoskaliger, nicht-agglomerierte Metalloxid-Teilchen zum Einsatz in Dentalmaterialien
DE102004008772A1 (de) * 2004-02-23 2005-09-08 Institut für Neue Materialien Gemeinnützige GmbH Abriebbeständige und alkalibeständige Beschichtungen oder Formkörper mit Niedrigenergieoberfläche
DE102004009287A1 (de) * 2004-02-26 2005-09-15 Institut Für Neue Materialien Gem. Gmbh Amphiphile Nanopartikel
DE102004017124B4 (de) * 2004-04-07 2008-07-10 Ivoclar Vivadent Ag Härtbare Dentalmaterialien mit einer einstellbaren Transluzenz und hohen Opaleszenz
US7649029B2 (en) * 2004-05-17 2010-01-19 3M Innovative Properties Company Dental compositions containing nanozirconia fillers
US7090722B2 (en) * 2004-05-17 2006-08-15 3M Innovative Properties Company Acid-reactive dental fillers, compositions, and methods
US7090721B2 (en) * 2004-05-17 2006-08-15 3M Innovative Properties Company Use of nanoparticles to adjust refractive index of dental compositions
US7156911B2 (en) 2004-05-17 2007-01-02 3M Innovative Properties Company Dental compositions containing nanofillers and related methods
KR101245946B1 (ko) * 2004-06-17 2013-03-21 쓰리엠 이노베이티브 프로퍼티즈 컴파니 광학 필름, 어셈블리 및 디스플레이 장치
US20060009536A1 (en) * 2004-07-12 2006-01-12 Guang-Way Jang Functionalized sol-gel material, sol-gel film derived therefrom, and method for preparing the same
WO2006017336A2 (en) * 2004-07-13 2006-02-16 Altairnano, Inc. Ceramic structures for prevention of drug diversion
DE102004048230A1 (de) * 2004-10-04 2006-04-06 Institut für Neue Materialien Gemeinnützige GmbH Verfahren zur Herstellung von Nanopartikeln mit maßgeschneiderter Oberflächenchemie und entsprechenden Kolloiden
US7241437B2 (en) * 2004-12-30 2007-07-10 3M Innovative Properties Company Zirconia particles
US7297810B2 (en) * 2004-12-30 2007-11-20 3M Innovative Properties Company High refractive index monomers for optical applications
US7491441B2 (en) 2004-12-30 2009-02-17 3M Innovative Properties Company High refractive index, durable hard coats
US7264872B2 (en) * 2004-12-30 2007-09-04 3M Innovative Properties Company Durable high index nanocomposites for AR coatings
US7943206B2 (en) * 2005-02-17 2011-05-17 3M Innovative Properties Company Brightness enhancement film comprising polymerized organic phase having low glass transition temperature
US7326448B2 (en) 2005-02-17 2008-02-05 3M Innovative Properties Company Polymerizable oligomeric urethane compositions comprising nanoparticles
US20060204745A1 (en) * 2005-03-14 2006-09-14 Jones Clint L Light management films with zirconia particles
EP1869509A2 (de) * 2005-03-11 2007-12-26 3M Innovative Properties Company Lichtverwaltungsfilme mit zirconia-partikeln
WO2006099168A2 (en) * 2005-03-11 2006-09-21 3M Innovative Properties Company Polymerizable compositions comprising nanoparticles
US20060204676A1 (en) * 2005-03-11 2006-09-14 Jones Clinton L Polymerizable composition comprising low molecular weight organic component
KR101308118B1 (ko) 2005-04-18 2013-09-12 닛산 가가쿠 고교 가부시키 가이샤 산성 지르코니아 졸 및 그 제조방법
FR2885308B1 (fr) * 2005-05-04 2007-07-06 Eastman Kodak Co Procede pour maintenir l'etat de dispersion d'une solution colloidale de particules d'oxyde metallique
US7400445B2 (en) * 2005-05-31 2008-07-15 3M Innovative Properties Company Optical filters for accelerated weathering devices
GB0512666D0 (en) * 2005-06-22 2005-07-27 Univ Loughborough Method for concentrating nanosuspensions
JP4961829B2 (ja) * 2005-08-09 2012-06-27 ソニー株式会社 ナノ粒子−樹脂複合材料の製造方法
CA2620167A1 (en) * 2005-08-23 2007-03-01 Altairnano, Inc. Highly photocatalytic phosphorus-doped anatase-tio2 composition and related manufacturing methods
JP4963820B2 (ja) * 2005-09-02 2012-06-27 第一稀元素化学工業株式会社 Ｚｒ−Ｏ系粒子を分散質とするゾルの製造方法
WO2007033934A2 (de) * 2005-09-20 2007-03-29 Basf Se Verfahren zur ermittlung der tortuosität, katalysatorträger, katalysator und verfahren zur dehydrierung von kohlenwasserstoffen
JP2007103708A (ja) * 2005-10-05 2007-04-19 Sumitomo Osaka Cement Co Ltd 発光素子封止用組成物及び発光素子並びに光半導体装置
JP5011695B2 (ja) * 2005-10-05 2012-08-29 住友大阪セメント株式会社 ジルコニア透明分散液及び透明複合体並びに透明複合体の製造方法
WO2007049573A1 (ja) * 2005-10-28 2007-05-03 Sumitomo Osaka Cement Co., Ltd. 無機酸化物透明分散液と無機酸化物粒子含有樹脂組成物、発光素子封止用組成物及び発光素子、ハードコート膜と光学機能膜及び光学部品、並びに無機酸化物粒子含有樹脂組成物の製造方法
JP5540458B2 (ja) * 2006-02-17 2014-07-02 住友大阪セメント株式会社 無機酸化物透明分散液と樹脂組成物、透明複合体、発光素子封止用組成物及び発光素子並びに透明複合体の製造方法
JP2009515218A (ja) 2005-11-05 2009-04-09 スリーエム イノベイティブ プロパティズ カンパニー 高屈折率及び反射防止コーティングを備えている光学フィルム
US7547467B2 (en) 2005-11-15 2009-06-16 3M Innovative Properties Company Brightness enhancing film and methods of surface treating inorganic nanoparticles
US20070190314A1 (en) * 2006-01-13 2007-08-16 Fujifilm Corporation Transparent article and method for producing it, and lens substrate
JP2007213022A (ja) * 2006-01-13 2007-08-23 Fujifilm Corp 透明成形体とその製造方法、およびレンズ基材
US20080020175A1 (en) * 2006-03-02 2008-01-24 Fred Ratel Nanostructured Indium-Doped Iron Oxide
WO2007103812A1 (en) * 2006-03-02 2007-09-13 Altairnano, Inc. Method for low temperature production of nano-structured iron oxide coatings
WO2007103829A1 (en) * 2006-03-02 2007-09-13 Altairnano, Inc. Method for production of metal oxide coatings
JP2007314773A (ja) * 2006-04-28 2007-12-06 Mitsubishi Chemicals Corp 高屈折率粒子含有樹脂組成物
US20100119697A1 (en) * 2006-05-10 2010-05-13 3M Innovative Properties Company Compositions and coatings containing fluorescent, inorganic nanoparticles
JP4961828B2 (ja) * 2006-05-12 2012-06-27 ソニー株式会社 ナノ粒子−樹脂複合材料の製造方法
US20070286994A1 (en) * 2006-06-13 2007-12-13 Walker Christopher B Durable antireflective film
US7897526B1 (en) 2006-07-13 2011-03-01 NEI, Corp Silicone nanocomposite coatings for fabrics
JP5177970B2 (ja) * 2006-07-18 2013-04-10 株式会社日本触媒 金属酸化物ナノ粒子の製造方法、金属ナノ粒子、処理金属ナノ粒子およびその用途
JP5030694B2 (ja) * 2006-07-18 2012-09-19 株式会社日本触媒 酸化ジルコニウムナノ粒子
WO2008010533A1 (en) * 2006-07-18 2008-01-24 Nippon Shokubai Co., Ltd. Metal oxide nanoparticle and method for producing the same
JP5019826B2 (ja) * 2006-07-28 2012-09-05 第一稀元素化学工業株式会社 ジルコニアゾル及びその製造方法
JP4952906B2 (ja) * 2006-11-15 2012-06-13 ソニーケミカル＆インフォメーションデバイス株式会社 封止樹脂組成物及び発光素子
JP2010510671A (ja) * 2006-11-17 2010-04-02 スリーエム イノベイティブ プロパティズ カンパニー Ｌｅｄ光源用の光学接着組成物
EP2087533A2 (de) * 2006-11-17 2009-08-12 3M Innovative Properties Company Planarisierte led mit optischem extraktor
JP2010510685A (ja) * 2006-11-20 2010-04-02 スリーエム イノベイティブ プロパティズ カンパニー Ｌｅｄ光源用の光学接着組成物
JP4561732B2 (ja) * 2006-11-20 2010-10-13 トヨタ自動車株式会社 移動体位置測位装置
US20080124555A1 (en) 2006-11-29 2008-05-29 3M Innovative Properties Company Polymerizable composition comprising perfluoropolyether urethane having ethylene oxide repeat units
JP4817254B2 (ja) * 2006-12-01 2011-11-16 大日本塗料株式会社 酸化ジルコニウム粒子分散液、酸化ジルコニウム粒子含有光硬化性組成物及び硬化膜
CN101573415B (zh) * 2006-12-21 2013-08-14 3M创新有限公司 制备纳米粒子的方法
JP4315195B2 (ja) * 2006-12-21 2009-08-19 ソニー株式会社 硬化性樹脂材料−微粒子複合材料及びその製造方法、光学材料、並びに発光装置
US8647426B2 (en) * 2006-12-28 2014-02-11 3M Innovative Properties Company Dental filler and methods
JP5331705B2 (ja) 2006-12-29 2013-10-30 スリーエム イノベイティブ プロパティズ カンパニー ジルコニア体及び方法
US7709092B2 (en) * 2007-01-19 2010-05-04 3M Innovative Properties Company Solar control multilayer film
JP2008201634A (ja) * 2007-02-21 2008-09-04 Fujifilm Corp ジルコニア微粒子分散液、該分散剤から製造される有機無機複合材料および光学部品
US7939578B2 (en) * 2007-02-23 2011-05-10 3M Innovative Properties Company Polymeric fibers and methods of making
JP2010519599A (ja) 2007-02-27 2010-06-03 スリーエム イノベイティブ プロパティズ カンパニー 耐亀裂性が改良されたナノコンポジット構造を備えた輝度向上フィルム
ATE510800T1 (de) * 2007-04-04 2011-06-15 Essilor Int Verfahren zur herstellung einer kolloidalen zirkoniumlösung
WO2008128000A1 (en) * 2007-04-12 2008-10-23 Altairnano, Inc. Teflon replacements and related production methods
US8513322B2 (en) * 2007-05-31 2013-08-20 3M Innovative Properties Company Polymeric beads and methods of making polymeric beads
DE102007036998A1 (de) 2007-08-06 2009-02-19 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren zur Herstellung von amorphen metallorganischen Makromolekülen, mit diesem Verfahren erhaltenes Material und seine Verwendung
JP2009137774A (ja) * 2007-12-03 2009-06-25 Sumitomo Osaka Cement Co Ltd ジルコニア粒子とその製造方法及びジルコニア透明分散液、並びに透明複合体及びその製造方法
US20100266794A1 (en) 2007-12-12 2010-10-21 Wright Robin E Hydrophilic gel materials and methods of making
EP2231733B1 (de) * 2007-12-12 2014-04-16 3M Innovative Properties Company Verfahren zur herstellung von geformten polymermaterialien
WO2009085721A1 (en) * 2007-12-21 2009-07-09 3M Innovative Properties Company Mixed ligand surface-modified nanoparticles
CN101945824B (zh) * 2007-12-28 2014-07-23 3M创新有限公司 制备含氧化锆的纳米粒子的方法
WO2009088043A1 (ja) * 2008-01-09 2009-07-16 Asahi Glass Company, Limited 表面修飾ジルコニア粒子、その製造方法及び樹脂組成物
FR2927005B1 (fr) * 2008-02-05 2011-12-23 Commissariat Energie Atomique Materiau hybride organique-inorganique, couche mince optique de ce materiau, materiau optique les comprenant, et leur procede de fabrication
JP5037393B2 (ja) * 2008-03-12 2012-09-26 富士フイルム株式会社 金属酸化物微粒子分散液及び成形体
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US20090275720A1 (en) * 2008-04-30 2009-11-05 3M Innovative Properties Company Ortho-benzylphenol mono(meth)acrylate monomers suitable for microstructured optical films
JP5701474B2 (ja) * 2008-06-13 2015-04-15 富士フイルム株式会社 無機微粒子分散液、有機無機複合組成物、成形体および光学部品
US8343622B2 (en) * 2008-07-01 2013-01-01 3M Innovative Properties Company Flexible high refractive index hardcoat
US8611010B2 (en) * 2008-09-30 2013-12-17 3M Innovative Properties Company Substrate comprising unmatched refractive index primer at optically significant thickness
WO2010045105A1 (en) 2008-10-15 2010-04-22 3M Innovative Properties Company Fillers and composite materials with zirconia and silica nanoparticles
JP5397829B2 (ja) * 2008-12-04 2014-01-22 堺化学工業株式会社 酸化ジルコニウム分散液の製造方法
WO2010074862A1 (en) * 2008-12-15 2010-07-01 3M Innovative Properties Company High refractive index inorganic oxide nanoparticles comprising surface treatment, polymerizable resin, and articles
KR20110110240A (ko) 2008-12-30 2011-10-06 쓰리엠 이노베이티브 프로퍼티즈 컴파니 반사방지 용품 및 이의 제조 방법
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JP2012524381A (ja) 2009-04-15 2012-10-11 スリーエム イノベイティブ プロパティズ カンパニー ボイドを含有する光学フィルムを備える光ガイド及びディスプレイシステム用ブラックライト
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KR101954456B1 (ko) 2010-04-15 2019-03-05 쓰리엠 이노베이티브 프로퍼티즈 캄파니 광학적 활성 영역 및 광학적 불활성 영역을 포함하는 재귀반사성 물품
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KR101894056B1 (ko) 2010-04-23 2018-10-04 픽셀리전트 테크놀로지스 엘엘씨 나노결정의 합성, 캐핑 및 분산
US8298329B2 (en) 2010-04-29 2012-10-30 James R. Glidewell Dental Ceramics, Inc. Nano-crystalline dental ceramics
WO2011140018A1 (en) 2010-05-07 2011-11-10 3M Innovative Properties Company Antireflective films comprising microstructured surface
KR101639082B1 (ko) * 2010-10-20 2016-07-13 코오롱인더스트리 주식회사 광중합성 조성물 및 이로부터 형성된 수지 경화층을 포함하는 광학시트
EP2632849A4 (de) 2010-10-27 2014-12-31 Pixelligent Technologies Llc Synthese, abdeckung und dispergierung von nanokristallen
US8742022B2 (en) 2010-12-20 2014-06-03 3M Innovative Properties Company Coating compositions comprising non-ionic surfactant exhibiting reduced fingerprint visibility
US9296904B2 (en) 2010-12-20 2016-03-29 3M Innovative Properties Company Coating compositions comprising non-ionic surfactant exhibiting reduced fingerprint visibility
CN103261098B (zh) 2010-12-22 2015-05-20 3M创新有限公司 表面改性的氧化锆纳米粒子
KR101862899B1 (ko) 2011-02-04 2018-05-30 쓰리엠 이노베이티브 프로퍼티즈 컴파니 산화지르코늄 나노입자를 포함하는 비결정성 퍼플루오로중합체
WO2012121858A1 (en) 2011-03-09 2012-09-13 3M Innovative Properties Company Antireflective film comprising large particle size fumed silica
BR112013023128A2 (pt) 2011-03-14 2019-09-24 3M Innovative Properties Co artigos nanoestruturados
US20140004304A1 (en) 2011-03-14 2014-01-02 3M Innovative Properties Company Multilayer nanostructured articles
WO2012162057A2 (en) 2011-05-20 2012-11-29 3M Innovative Properties Company Laser-personalizable security articles
US9289962B2 (en) 2011-05-20 2016-03-22 3M Innovative Properties Company Laser-personalizable security articles
CN103732629B (zh) 2011-08-23 2015-10-21 3M创新有限公司 加成-断裂剂
RU2586743C2 (ru) 2011-08-23 2016-06-10 Зм Инновейтив Пропертиз Компани Стоматологические композиции, содержащие агенты присоединения-фрагментации
US9359689B2 (en) * 2011-10-26 2016-06-07 Pixelligent Technologies, Llc Synthesis, capping and dispersion of nanocrystals
EP2610318A1 (de) 2011-12-30 2013-07-03 Essilor International (Compagnie Générale D'Optique) Beschichtungszusammensetzung für einen optischen Artikel mit einer kolloidalen Suspension von Zirkoniumpartikeln
WO2013130247A1 (en) 2012-02-28 2013-09-06 3M Innovative Properties Company Composition comprising surface modified high index nanoparticles suitable for optical coupling layer
US11133118B2 (en) 2012-05-22 2021-09-28 University Of Massachusetts Patterned nanoparticle structures
JP6363072B2 (ja) 2012-06-19 2018-07-25 スリーエム イノベイティブ プロパティズ カンパニー 低表面エネルギー基及びヒドロキシル基を含む添加剤、並びにコーティング組成物
EP2861678B1 (de) 2012-06-19 2017-10-11 3M Innovative Properties Company Beschichtungszusammensetzungen mit nichtionischem tensid mit reduzierter sichtbarkeit von fingerabdrücken
EP2872537A1 (de) 2012-07-13 2015-05-20 3M Innovative Properties Company Hartbeschichtungen mit alkoxylierten multi(meth)acrylatmonomeren
WO2014074427A1 (en) 2012-11-12 2014-05-15 3M Innovative Properties Company Addition-fragmentation agents
CN104768519B (zh) 2012-11-12 2018-11-23 3M创新有限公司 包含加成-断裂剂的牙科组合物
US9477354B2 (en) 2012-11-16 2016-10-25 3M Innovative Properties Company Conductive trace hiding materials, articles, and methods
US9829604B2 (en) 2012-12-20 2017-11-28 3M Innovative Properties Company Method of making multilayer optical film comprising layer-by-layer self-assembled layers and articles
JP2013075824A (ja) * 2012-12-25 2013-04-25 Sumitomo Osaka Cement Co Ltd 透明複合体及びその製造方法
US9802174B2 (en) 2012-12-26 2017-10-31 Essilor International (Compagnie Generale D'optique) Method for producing zirconia colloids
US20140242343A1 (en) 2013-02-27 2014-08-28 3M Innovative Properties Company Lamination transfer films for forming embedded nanostructures
CN105229090A (zh) 2013-05-31 2016-01-06 3M创新有限公司 逐层自组装包含光吸收或光稳定化合物的高分子电解质的方法和制品
JP6416247B2 (ja) 2013-06-27 2018-10-31 イフォクレール ビバデント， インコーポレイテッド ナノ結晶ジルコニアおよびその加工方法
WO2015002685A1 (en) 2013-07-01 2015-01-08 3M Innovative Properties Company Protection film suitable for illuminated display devices
CN105593323B (zh) 2013-10-02 2018-11-09 3M创新有限公司 包含聚丙烯酸酯压敏底漆以及含聚丙烯酸酯组分的粘合剂的制品
JP6441912B2 (ja) 2013-10-02 2018-12-19 スリーエム イノベイティブ プロパティズ カンパニー 窒素含有ポリマーを含むポリアクリレートプライマーを含む物品及び方法
JP6643226B2 (ja) 2013-10-02 2020-02-12 スリーエム イノベイティブ プロパティズ カンパニー 第１の微細構造層及びコーティングを含む微細構造化拡散体、光学積層体、並びに方法
BR112016007358A2 (pt) 2013-10-04 2017-08-01 3M Innovative Properties Co bloco bruto para usinagem de próteses dentárias
US10213993B2 (en) 2013-12-19 2019-02-26 3M Innovative Properties Company Multilayer composite article
CN105829921B (zh) 2013-12-19 2018-11-09 3M创新有限公司 包括包含带有磷表面处理剂的纳米粒子的自组装层的制品
JP6189547B2 (ja) 2014-01-15 2017-08-30 スリーエム イノベイティブ プロパティズ カンパニー アルコキシ化マルチ（メタ）アクリレートモノマーを含むハードコート及び表面処理されたナノ粒子
US20150202834A1 (en) 2014-01-20 2015-07-23 3M Innovative Properties Company Lamination transfer films for forming antireflective structures
US9246134B2 (en) 2014-01-20 2016-01-26 3M Innovative Properties Company Lamination transfer films for forming articles with engineered voids
EP3096945B1 (de) 2014-01-20 2019-08-14 3M Innovative Properties Company Laminierungstransferfolien zur formung von strukturen mit hinterschnitt
KR102456918B1 (ko) 2014-01-22 2022-10-19 쓰리엠 이노베이티브 프로퍼티즈 컴파니 글레이징을 위한 미세광학체
EP3140355B1 (de) 2014-05-09 2018-07-11 3M Innovative Properties Company Artikel mit hartbeschichtung und herstellungsverfahren dafür
TWI543938B (zh) 2014-05-13 2016-08-01 國立中央大學 金屬氧化物奈米顆粒材料
US11247501B2 (en) 2014-08-27 2022-02-15 3M Innovative Properties Company Layer-by-layer assembled multilayer lamination transfer films
US9586385B2 (en) 2014-08-27 2017-03-07 3M Innovative Properties Company Inorganic multilayer lamination transfer films
EP3186082B1 (de) 2014-08-27 2021-01-27 3M Innovative Properties Company Mehrschichtige elektrische laminierungstransferfolien
WO2016032795A1 (en) 2014-08-29 2016-03-03 3M Innovative Properties Company Inductively curable composition
WO2016039820A1 (en) 2014-09-10 2016-03-17 3M Innovative Properties Company Exposed lens retroreflective articles comprising a self-assembled dielectric mirror
CN107003462A (zh) 2014-12-15 2017-08-01 3M创新有限公司 具有硬涂层的制品及其制造方法
WO2016140950A1 (en) 2015-03-05 2016-09-09 3M Innovative Properties Company Composite material having ceramic fibers
EP3277741A4 (de) 2015-03-30 2018-11-14 Pixelligent Technologies, LLC Lösemittelfreie silikonnanokomposite mit hohem brechungsindex
EP3313617B1 (de) 2015-06-25 2023-06-14 3M Innovative Properties Company Verfahren zur herstellung metallgebundener schleifartikel und metallgebundene schleifartikel
GB201518996D0 (en) * 2015-10-27 2015-12-09 Magnesium Elektron Ltd Zirconia-based compositions for use as three-way catalysts
WO2017142744A1 (en) 2016-02-18 2017-08-24 3M Innovative Properties Company 3-d printing surface
WO2017163610A1 (ja) * 2016-03-25 2017-09-28 株式会社日本触媒 酸化ジルコニウムナノ粒子
JP6851740B2 (ja) * 2016-03-25 2021-03-31 株式会社日本触媒 酸化ジルコニウムナノ粒子
WO2018005088A1 (en) 2016-06-27 2018-01-04 3M Innovative Properties Company Compositions comprising nanoparticles functionalized with an alpha-hydroxy acid or salt, articles, and methods
EP3478501A4 (de) 2016-07-01 2020-03-04 3M Innovative Properties Company Schutzfolie für displays aus polyurethan mit niedrigem tg
CN109642143B (zh) 2016-07-22 2021-09-24 3M创新有限公司 作为陶瓷前体的硅氧烷基粘合剂层
US11292940B2 (en) 2016-07-22 2022-04-05 3M Innovative Properties Company Polymeric adhesive layers as ceramic precursors
US9822039B1 (en) * 2016-08-18 2017-11-21 Ivoclar Vivadent Ag Metal oxide ceramic nanomaterials and methods of making and using same
EP3515703A1 (de) 2016-09-21 2019-07-31 3M Innovative Properties Company Schutzfolie mit glas für eine anzeige
CN109890568B (zh) 2016-10-25 2022-07-29 3M创新有限公司 包括取向磨料颗粒的粘结磨料制品及其制备方法
CN109983092A (zh) 2016-11-21 2019-07-05 3M创新有限公司 包含氢键键合至丙烯酸类聚合物的氨基甲酸酯低聚物的柔性硬质涂层
KR102503640B1 (ko) 2016-12-01 2023-02-23 쓰리엠 이노베이티브 프로퍼티즈 컴파니 이중 경화 보호 디스플레이 필름
TW201830102A (zh) 2016-12-14 2018-08-16 美商3M新設資產公司 分段保護顯示膜
EP3558589B1 (de) 2016-12-23 2024-01-24 3M Innovative Properties Company Verfahren zur herstellung von polymergebundene schleifartikel
US20200096683A1 (en) 2017-05-25 2020-03-26 3M Innovative Properties Company Cube corner retroreflective articleswith tailored retroreflectivity and methods of making
KR20200096528A (ko) 2017-12-08 2020-08-12 쓰리엠 이노베이티브 프로퍼티즈 컴파니 가요성 하드코트
US20200347236A1 (en) 2018-01-24 2020-11-05 3M Innovative Properties Company Flexible hardcoat comprising urethane oligomer hydrogen bonded to an acrylic polymer suitable for stretchable films
CN112585200B (zh) 2018-08-14 2023-06-27 3M创新有限公司 设置在有机基体构件和硅质层之间的柔性硬质涂层以及可清洁制品
FR3089136B1 (fr) * 2018-11-30 2024-03-22 Mathym Procede de preparation de nanoparticules de dioxyde de zirconium en presence d’acide amine
EP3941970A1 (de) 2019-03-18 2022-01-26 Basf Se Uv-härtbare zusammensetzungen für schmutzaufnahmebeständigkeit
KR20210153734A (ko) 2019-05-09 2021-12-17 쓰리엠 이노베이티브 프로퍼티즈 컴파니 가요성 하드코트
US11827811B2 (en) 2019-05-09 2023-11-28 3M Innovative Properties Company Flexible hardcoat
CN114072468A (zh) 2019-05-09 2022-02-18 3M创新有限公司 柔性硬质涂层
CN113874208B (zh) 2019-05-31 2023-10-10 3M创新有限公司 复合冷却膜和包括该复合冷却膜的制品
US20220266421A1 (en) 2019-07-15 2022-08-25 3M Innovative Properties Company Abrasive articles having internal coolant features and methods of manufacturing the same
EP4237194A1 (de) 2020-10-28 2023-09-06 3M Innovative Properties Company Systeme und verfahren zur bereitstellung von kühlmittel für einen aktiven schleifbereich
US20230323151A1 (en) 2020-11-05 2023-10-12 3M Innovative Properties Company Imide addition-fragmentation agents
KR20220078242A (ko) * 2020-12-03 2022-06-10 주식회사 케이씨텍 금속 산화물 분산액
WO2023105327A1 (en) 2021-12-06 2023-06-15 3M Innovative Properties Company Adhesives comprising cyclic imide addition-fragmentation and adhesion agents
CN115124074B (zh) * 2022-07-26 2024-02-06 宣城市晶纳环保科技有限公司 一种高分散复合纳米二氧化锆的制备方法
CN116102060A (zh) * 2023-02-10 2023-05-12 广州市汉宵科研技术有限公司 一种纳米级氧化锆颗粒材料及其制备方法

Family Cites Families (100)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2984628A (en) 1956-11-29 1961-05-16 Du Pont Concentrated zirconia and hafnia aquasols and their preparation
US3018262A (en) 1957-05-01 1962-01-23 Shell Oil Co Curing polyepoxides with certain metal salts of inorganic acids
US3066112A (en) 1959-01-30 1962-11-27 Rafael L Bowen Dental filling material comprising vinyl silane treated fused silica and a binder consisting of the reaction product of bis phenol and glycidyl acrylate
NL128404C (de) 1959-12-24
US3442817A (en) 1966-04-15 1969-05-06 Du Pont Preparation of zirconia and hafnia sols
US3514252A (en) 1967-07-07 1970-05-26 Grace W R & Co Process for the preparation of stabilized zirconia powders
US3860556A (en) 1968-03-15 1975-01-14 Minnesota Mining & Mfg Low water absorption dental restorative
US3539533A (en) 1968-06-14 1970-11-10 Johnson & Johnson Dental filling material
US3708296A (en) 1968-08-20 1973-01-02 American Can Co Photopolymerization of epoxy monomers
US3709706A (en) 1969-05-16 1973-01-09 Minnesota Mining & Mfg Refractory fibers and other articles of zirconia and silica mixtures
US3629187A (en) 1969-06-25 1971-12-21 Dentsply Int Inc Dental compositions containing adduct of 2 2' - propane bis 3-(4-phenoxy)-1 2-hydroxy propane - 1 - methacrylate and isocyanate
US3709866A (en) 1970-06-01 1973-01-09 Dentsply Int Inc Photopolymerizable dental products
US3766132A (en) 1971-02-12 1973-10-16 Lee Pharmaceuticals Diacrylate esters of low viscosity and the use thereof as binders in dental restorative compositions
US3751399A (en) 1971-05-24 1973-08-07 Lee Pharmaceuticals Polyacrylate resin compositions
US3729113A (en) 1971-07-08 1973-04-24 Reflector Hardware Corp Modular cabinet assembly, and components and subassemblies therefor
GB1408265A (en) 1971-10-18 1975-10-01 Ici Ltd Photopolymerisable composition
US3808006A (en) 1971-12-06 1974-04-30 Minnesota Mining & Mfg Photosensitive material containing a diaryliodium compound, a sensitizer and a color former
US3741769A (en) 1972-10-24 1973-06-26 Minnesota Mining & Mfg Novel photosensitive polymerizable systems and their use
DE2406557C3 (de) 1974-02-12 1981-02-19 Kulzer & Co Gmbh, 6380 Bad Homburg Hydroxyl-Gruppen enthaltende Diester von Acrylsäuren und diese enthaltendes Zahnfüllungsmaterial
US4115346A (en) 1974-02-12 1978-09-19 Kulzer & Co. Gmbh Hydroxy group containing diesters of acrylic acids and their use in dental material
AU497960B2 (en) 1974-04-11 1979-01-25 Minnesota Mining And Manufacturing Company Photopolymerizable compositions
US4250311A (en) 1974-05-02 1981-02-10 General Electric Company P, As, and Sb hexafluoride onium salts as photoinitiators
GB1512981A (en) 1974-05-02 1978-06-01 Gen Electric Curable epoxide compositions
GB1569021A (en) 1976-03-17 1980-06-11 Kuraray Co Adhesive cementing agents containing partial phosphonic orphosphonic acid esters
JPS5940953B2 (ja) * 1977-11-30 1984-10-03 東邦化学工業株式会社 ポリエステル系合成繊維の染色法
US4292029A (en) 1978-05-15 1981-09-29 University Of Michigan Hydrophobic composite restorative materials and their use in tooth treatment
US4387240A (en) 1978-06-02 1983-06-07 Minnesota Mining And Manufacturing Company Oligomeric methacryl substituted alkylsiloxanes
US4216288A (en) 1978-09-08 1980-08-05 General Electric Company Heat curable cationically polymerizable compositions and method of curing same with onium salts and reducing agents
DE2850917A1 (de) 1978-11-24 1980-06-04 Bayer Ag Dentalwerkstoffe auf basis von organischen kunststoffen in pastoeser form
US4327014A (en) 1979-04-11 1982-04-27 Kanebo Ltd. Resin-forming material, implant material and compositions for restorative material suitable for medical or dental use
US4250053A (en) 1979-05-21 1981-02-10 Minnesota Mining And Manufacturing Company Sensitized aromatic iodonium or aromatic sulfonium salt photoinitiator systems
US4379695A (en) 1980-06-02 1983-04-12 Scientific Pharmaceuticals, Inc. Dental material comprising dimethyacrylate adducts of glycidyl methacrylate with diesters of bis(hydroxymethyl) tricyclo[5.2.1.02,6 ]decane and dicarboxylic acids
JPS5828878B2 (ja) 1980-08-20 1983-06-18 三金工業株式会社 環状ピロ燐酸エステル誘導体
DE3170993D1 (en) 1981-03-24 1985-07-25 Blendax Werke Schneider Co Dental filling material
EP0094915B1 (de) 1982-05-19 1987-01-21 Ciba-Geigy Ag Härtbare, Metallocenkomplexe enthaltende Zusammensetzungen, daraus erhältliche aktivierte Vorstufen und deren Verwendung
US5089536A (en) 1982-11-22 1992-02-18 Minnesota Mining And Manufacturing Company Energy polmerizable compositions containing organometallic initiators
US5073476A (en) 1983-05-18 1991-12-17 Ciba-Geigy Corporation Curable composition and the use thereof
US4545924A (en) 1983-06-13 1985-10-08 Owens-Corning Fiberglas Corporation Production of a magnesium chloride gel system useful in ceramics and fiber production
US4612138A (en) * 1983-08-04 1986-09-16 Nalco Chemical Company Stable acidic and alkaline metal oxide sols
DE3341888A1 (de) 1983-11-19 1985-05-30 Bayer Ag, 5090 Leverkusen Anorganisch-organische fuellstoffe, verfahren zu deren herstellung sowie deren verwendung in polymerisierbaren massen
DE3342601C1 (de) 1983-11-25 1985-03-14 Blendax-Werke R. Schneider Gmbh & Co, 6500 Mainz Verwendung von bromierten aromatischen Diacrylsaeure- bzw. Dimethacrylsaeureestern in dentalen Fuellungsmaterialien
US4544359A (en) 1984-01-13 1985-10-01 Pentron Corporation Dental restorative material
DE3403040A1 (de) 1984-01-30 1985-08-08 Blendax-Werke R. Schneider Gmbh & Co, 6500 Mainz Dentales fuellungsmaterial
US4503169A (en) 1984-04-19 1985-03-05 Minnesota Mining And Manufacturing Company Radiopaque, low visual opacity dental composites containing non-vitreous microparticles
US4746685A (en) 1984-08-31 1988-05-24 Nippon Oil And Fats Co., Ltd. Light curable dental composition
DE3443221A1 (de) 1984-11-27 1986-06-05 ESPE Fabrik pharmazeutischer Präparate GmbH, 8031 Seefeld Bisacylphosphinoxide, ihre herstellung und verwendung
US4661540A (en) 1984-12-06 1987-04-28 Berger, Jenson & Nicholson Limited Water reducible coating compositions
EP0184467A3 (de) 1984-12-06 1988-06-08 Berger, Jenson and Nicholson Limited Wasserverdünnbare Beschichtungszusammensetzungen
US4642126A (en) 1985-02-11 1987-02-10 Norton Company Coated abrasives with rapidly curable adhesives and controllable curvature
US4619817A (en) 1985-03-27 1986-10-28 Battelle Memorial Institute Hydrothermal method for producing stabilized zirconia
US4652274A (en) 1985-08-07 1987-03-24 Minnesota Mining And Manufacturing Company Coated abrasive product having radiation curable binder
US4772530A (en) 1986-05-06 1988-09-20 The Mead Corporation Photosensitive materials containing ionic dye compounds as initiators
US4772511A (en) 1985-11-22 1988-09-20 Minnesota Mining And Manufacturing Company Transparent non-vitreous zirconia microspheres
JPH0729771B2 (ja) 1986-01-14 1995-04-05 悦朗 加藤 単斜ジルコニア超微結晶の高分散ゾルまたはゲルおよび製造方法
JPS62260718A (ja) 1986-05-06 1987-11-13 Shigeyuki Somiya 水熱法による高純度ジルコニア−アルミナ系超微粉末の製造方法
US4719091A (en) 1986-07-01 1988-01-12 Corning Glass Works Preparation of mono-sized zirconia powders by forced hydrolysis
US4778671A (en) 1986-07-14 1988-10-18 Corning Glass Works Preparation of unagglomerated metal oxide particles with uniform particle size
DE3777940D1 (de) 1986-09-27 1992-05-07 Nissan Chemical Ind Ltd Verfahren zur herstellung von feinem zirkonoxydpulver.
US4874450A (en) 1987-01-29 1989-10-17 The Mead Corporation Laminating transparent or translucent materials using ionic dye-counter ion complexes
DE3863940D1 (de) 1987-02-25 1991-09-05 Nippon Catalytic Chem Ind Verfahren zur erzeugung sehr kleiner, anorganischer, kugelfoermiger teilchen.
CA1323949C (en) 1987-04-02 1993-11-02 Michael C. Palazzotto Ternary photoinitiator system for addition polymerization
US4886624A (en) 1987-08-19 1989-12-12 Rhone-Poulenc, Inc. Colloidal alcohol-dispersible association complexes of ceric dioxide and a hydroxyphenyl carboxylic acid
FR2629071B1 (fr) * 1988-03-22 1991-03-15 Produits Refractaires Oxyde de zirconium reactif et sa preparation
US4985340A (en) 1988-06-01 1991-01-15 Minnesota Mining And Manufacturing Company Energy curable compositions: two component curing agents
US5234870A (en) 1988-07-21 1993-08-10 Nippon Shokubai Kagaku Kogyo Co., Ltd. Zirconia sol and method for production thereof
US4954414A (en) 1988-11-08 1990-09-04 The Mead Corporation Photosensitive composition containing a transition metal coordination complex cation and a borate anion and photosensitive materials employing the same
US5275759A (en) 1989-02-10 1994-01-04 Nippon Shokubai Kagaku Kogyo Co., Ltd. Zirconia sol, method for production thereof, porous ceramic-producing slurry, and porous ceramic product obtained by use thereof
US5057393A (en) 1989-07-10 1991-10-15 The Mead Corporation Dye branched-alkyl borate photoinitiators
JPH077895B2 (ja) 1989-07-14 1995-01-30 日本電気株式会社 可変利得増幅器
US5190583A (en) * 1989-12-04 1993-03-02 Transfer-Electric Gesellschaft Fur Aqueous coating composition and the use thereof for coating to be protected from light, especially ultraviolet radiation
US5084586A (en) 1990-02-12 1992-01-28 Minnesota Mining And Manufacturing Company Novel initiators for cationic polymerization
US5037579A (en) 1990-02-12 1991-08-06 Nalco Chemical Company Hydrothermal process for producing zirconia sol
US5124417A (en) 1990-02-12 1992-06-23 Minnesota Mining And Manufacturing Company Initiators for cationic polymerization
US5055372A (en) 1990-04-23 1991-10-08 The Mead Corporation Photohardenable composition containing borate salts and ketone initiators
JPH0472768A (ja) 1990-07-13 1992-03-06 Meidensha Corp 自己消弧型半導体装置
JPH0764564B2 (ja) * 1991-02-20 1995-07-12 株式会社槌屋 酸化ジルコニウム系前駆体ゲル状物及びその製造方法
US5332429A (en) 1991-05-31 1994-07-26 Minnesota Mining And Manufacturing Company Method for treating fluoroaluminosilicate glass
FR2681534B1 (fr) 1991-09-20 1995-01-27 Rhone Poulenc Chimie Solutions collouidales concentrees de particules monocristallines non agregees d'oxydes de metaux, leur procede de preparation et leur application a l'obtention de films.
DE4133621A1 (de) 1991-10-10 1993-04-22 Inst Neue Mat Gemein Gmbh Nanoskalige teilchen enthaltende kompositmaterialien, verfahren zu deren herstellung und deren verwendung fuer optische elemente
DE4212633A1 (de) 1992-04-15 1993-10-21 Inst Neue Mat Gemein Gmbh Verfahren zur Herstellung oberflächenmodifizierter nanoskaliger keramischer Pulver
WO1993023333A1 (en) * 1992-05-20 1993-11-25 E.I. Du Pont De Nemours And Company Process for making inorganic gels
US5460701A (en) 1993-07-27 1995-10-24 Nanophase Technologies Corporation Method of making nanostructured materials
TW343961B (en) 1994-06-17 1998-11-01 Nissan Chemical Ind Ltd Aqueous zirconia sol and method of preparing same
JP3214982B2 (ja) 1994-07-04 2001-10-02 株式会社トクヤマ 無機組成物
US5856373A (en) 1994-10-31 1999-01-05 Minnesota Mining And Manufacturing Company Dental visible light curable epoxy system with enhanced depth of cure
JP3542425B2 (ja) 1994-11-17 2004-07-14 キヤノン株式会社 インクジェット記録用水系分散インク、これを用いるインクジェット記録方法、インクカートリッジ、記録ユニットおよび記録装置
US5830242A (en) 1995-03-15 1998-11-03 Takeshi Yao Process for producing metal oxide precipitates
US5698483A (en) 1995-03-17 1997-12-16 Institute Of Gas Technology Process for preparing nanosized powder
DE19515820A1 (de) 1995-04-29 1996-10-31 Inst Neue Mat Gemein Gmbh Verfahren zur Herstellung schwach agglomerierter nanoskaliger Teilchen
US5648407A (en) 1995-05-16 1997-07-15 Minnesota Mining And Manufacturing Company Curable resin sols and fiber-reinforced composites derived therefrom
WO1997015526A1 (en) 1995-10-27 1997-05-01 E.I. Du Pont De Nemours And Company Hydrothermal process for making ultrafine metal oxide powders
DE19540623A1 (de) 1995-10-31 1997-05-07 Inst Neue Mat Gemein Gmbh Verfahren zur Herstellung von Kompositmaterialien mit hohem Grenzflächenanteil und dadurch erhältliche Kompositmaterialien
US5886069A (en) 1995-11-13 1999-03-23 E. I. Du Pont De Nemours And Company Titanium dioxide particles having substantially discrete inorganic particles dispersed on their surfaces
DE19617931C5 (de) 1996-04-26 2010-07-22 Ivoclar Vivadent Ag Verwendung eines gefüllten und polymerisierbaren Materials als Dentalmaterial
US5942559A (en) 1996-08-26 1999-08-24 Ivoclar Ag Dental light-curing opaquer
US6030914A (en) 1996-11-12 2000-02-29 Tosoh Corporation Zirconia fine powder and method for its production
JP4086338B2 (ja) 1996-12-06 2008-05-14 株式会社松風 歯科用弾性修復材料並びにそれを用いた歯科補綴材料の作製方法
US5760126A (en) 1996-12-20 1998-06-02 Minnesota Mining And Manufacturing Company Aqueous fluorochemical compositions and abrasion-resistant coatings therefrom
US6025406A (en) 1997-04-11 2000-02-15 3M Innovative Properties Company Ternary photoinitiator system for curing of epoxy resins
US5879715A (en) 1997-09-02 1999-03-09 Ceramem Corporation Process and system for production of inorganic nanoparticles

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DE60023023D1 (de) 2006-02-16
EP1232118A1 (de) 2002-08-21
CA2388876A1 (en) 2001-05-03
AU4065200A (en) 2001-05-08
EP1232118B1 (de) 2005-10-05
US20020004544A1 (en) 2002-01-10
JP2003512287A (ja) 2003-04-02
JP4559004B2 (ja) 2010-10-06
CA2388876C (en) 2009-10-27
US6376590B2 (en) 2002-04-23

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