DE60028958D1 - Verfahren zur herstellung organischer säuren und ihrer ester - Google Patents

Verfahren zur herstellung organischer säuren und ihrer ester

Info

Publication number
DE60028958D1
DE60028958D1 DE60028958T DE60028958T DE60028958D1 DE 60028958 D1 DE60028958 D1 DE 60028958D1 DE 60028958 T DE60028958 T DE 60028958T DE 60028958 T DE60028958 T DE 60028958T DE 60028958 D1 DE60028958 D1 DE 60028958D1
Authority
DE
Germany
Prior art keywords
organic acid
alcohol
product stream
ester
optionally
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE60028958T
Other languages
English (en)
Other versions
DE60028958T2 (de
Inventor
Charles Cockrem
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Primary Products Ingredients Americas LLC
Original Assignee
Tate and Lyle Ingredients Americas LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate and Lyle Ingredients Americas LLC filed Critical Tate and Lyle Ingredients Americas LLC
Publication of DE60028958D1 publication Critical patent/DE60028958D1/de
Application granted granted Critical
Publication of DE60028958T2 publication Critical patent/DE60028958T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41Preparation of salts of carboxylic acids
    • C07C51/412Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
DE60028958T 1999-04-28 2000-04-19 Verfahren zur herstellung organischer säuren und ihrer ester Expired - Fee Related DE60028958T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US301466 1994-09-07
US09/301,466 US6291708B1 (en) 1999-04-28 1999-04-28 Process for production of organic acids and esters thereof
PCT/US2000/010588 WO2000064850A1 (en) 1999-04-28 2000-04-19 Process for production of organic acids and esters thereof

Publications (2)

Publication Number Publication Date
DE60028958D1 true DE60028958D1 (de) 2006-08-03
DE60028958T2 DE60028958T2 (de) 2007-02-08

Family

ID=23163501

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60028958T Expired - Fee Related DE60028958T2 (de) 1999-04-28 2000-04-19 Verfahren zur herstellung organischer säuren und ihrer ester

Country Status (11)

Country Link
US (1) US6291708B1 (de)
EP (1) EP1173402B1 (de)
CN (1) CN1315772C (de)
AT (1) ATE330929T1 (de)
AU (1) AU4473200A (de)
BR (1) BR0011220A (de)
DE (1) DE60028958T2 (de)
DK (1) DK1173402T3 (de)
ES (1) ES2267528T3 (de)
PT (1) PT1173402E (de)
WO (1) WO2000064850A1 (de)

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JP2002161071A (ja) * 2000-11-28 2002-06-04 Nippon Shokubai Co Ltd 脱水反応生成物の製造方法及びそれに用いられる脱水反応装置
US6984293B2 (en) 2001-03-15 2006-01-10 Tate & Lyle Ingredients Azeotropic distillation of cyclic esters of hydroxy organic acids
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US6926810B2 (en) 2001-03-15 2005-08-09 A. E. Staley Manufacturing Co. Process for obtaining an organic acid from an organic acid ammonium salt, an organic acid amide, or an alkylamine organic acid complex
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AU2003255244A1 (en) * 2002-08-07 2004-02-25 Deka Products Limited Partnership Method and apparatus for phase change enhancement
US7785448B2 (en) * 2002-08-07 2010-08-31 Deka Products Limited Partnership Method and apparatus for phase change enhancement
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US8069676B2 (en) 2002-11-13 2011-12-06 Deka Products Limited Partnership Water vapor distillation apparatus, method and system
US8511105B2 (en) 2002-11-13 2013-08-20 Deka Products Limited Partnership Water vending apparatus
US7445917B2 (en) * 2004-12-22 2008-11-04 E.I. Du Pont De Nemours And Company Process for producing glycolic acid from formaldehyde and hydrogen cyanide
CN102899362B (zh) 2004-12-22 2014-06-04 纳幕尔杜邦公司 乙醇酸的酶促生产
WO2006069113A2 (en) * 2004-12-22 2006-06-29 E.I. Dupont De Nemours And Company Method to produce a carboxylic acid ester from a carboxylic acid ammonium salt by alcoholysis
US7198927B2 (en) * 2004-12-22 2007-04-03 E. I. Du Pont De Nemours And Company Enzymatic production of glycolic acid
US20060160198A1 (en) * 2004-12-22 2006-07-20 Xu Li Method for the production of glycolic acid from ammonium glycolate by direct deammoniation
EP1842843A1 (de) * 2006-04-04 2007-10-10 Basf Aktiengesellschaft Verfahren zur Herstellung eines Carbonsäurealkylesters
US11826681B2 (en) 2006-06-30 2023-11-28 Deka Products Limited Partneship Water vapor distillation apparatus, method and system
US11884555B2 (en) 2007-06-07 2024-01-30 Deka Products Limited Partnership Water vapor distillation apparatus, method and system
CN101765563B (zh) 2007-06-07 2012-10-24 德卡产品有限公司 水蒸汽蒸馏设备、方法和系统
US7741088B2 (en) * 2007-10-31 2010-06-22 E.I. Dupont De Nemours And Company Immobilized microbial nitrilase for production of glycolic acid
US7871802B2 (en) * 2007-10-31 2011-01-18 E.I. Du Pont De Nemours And Company Process for enzymatically converting glycolonitrile to glycolic acid
DE102008040415A1 (de) * 2008-07-15 2010-01-21 Evonik Röhm Gmbh Thermisches Salzspalten von Ammoniumcarboxylaten
MX2011001778A (es) 2008-08-15 2011-05-10 Deka Products Lp Aparato expendedor de agua.
DE102009001008A1 (de) 2009-02-19 2010-08-26 Evonik Degussa Gmbh Reaktivextraktion von freien organischen Säuren aus deren Ammoniumsalzen
DE102009009580A1 (de) 2009-02-19 2010-08-26 Evonik Degussa Gmbh Verfahren zur Herstellung freier Säuren aus ihren Salzen
US20120021473A1 (en) * 2010-04-01 2012-01-26 Bioamber S.A.S. Processes for producing carboxylic acids from fermentation broths containing their ammonium salts
US8409834B2 (en) 2010-06-18 2013-04-02 Butamax(Tm) Advanced Biofuels Llc Extraction solvents derived from oil for alcohol removal in extractive fermentation
US9040263B2 (en) 2010-07-28 2015-05-26 Butamax Advanced Biofuels Llc Production of alcohol esters and in situ product removal during alcohol fermentation
DE102010025167A1 (de) 2010-06-25 2011-12-29 Uhde Gmbh Verfahren zur Abtrennung, Gewinnung und Reinigung von Bernsteinsäure
KR20120054387A (ko) * 2010-11-19 2012-05-30 삼성정밀화학 주식회사 디알킬락타미드류의 제조방법
CN102351686B (zh) * 2011-08-16 2013-11-06 武汉三江航天固德生物科技有限公司 甲醇酯化耦合真空蒸馏法乳酸提取纯化生产方法
DE102011120632A1 (de) 2011-12-09 2013-06-13 Thyssenkrupp Uhde Gmbh Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen
RU2535680C2 (ru) * 2012-04-24 2014-12-20 Валерий Федорович Швец Способ переработки лактата аммония в молочную кислоту и ее сложные эфиры
WO2014018896A1 (en) 2012-07-27 2014-01-30 Deka Products Limited Partnership Control of conductivity in product water outlet for evaporation apparatus
EP2745905A1 (de) 2012-12-21 2014-06-25 ThyssenKrupp Uhde GmbH Verfahren zur Reinigung von Carboxylsäuren durch subkritische oder superkritische Chromatography
DE102013000027A1 (de) 2013-01-03 2014-07-03 Thyssenkrupp Industrial Solutions Ag Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen
WO2014108163A2 (de) 2013-01-11 2014-07-17 Thyssenkrupp Uhde Gmbh Verfahren zur herstellung von dicarbonsäuren
BE1021574B1 (fr) * 2013-01-23 2015-12-14 Man To Tree S.A. Procede continu de synthese d'oligoesters a partir d'un sel d'ammonium d'un acide dicarboxylique et d'un diol et dispositif de mise en oeuvre.
KR101828769B1 (ko) * 2013-02-14 2018-02-13 푸락 바이오켐 비.브이. 석신산 에스테르의 제조 방법
EP2970076A1 (de) * 2013-03-15 2016-01-20 Dow Global Technologies LLC Thermische salzspaltung von ammoniumpropionat
BR112017025594A2 (pt) 2015-05-29 2018-08-07 Mallinath Lali Arvind separação de ácidos orgânicos de misturas que contêm sais de amônio de ácidos orgânicos
RU2664125C2 (ru) * 2015-12-11 2018-08-15 Федеральное государственное бюджетное образовательное учреждение высшего образования "Российский химико-технологический университет имени Д.И. Менделеева" (РХТУ им. Д.И. Менделеева) Способ переработки лактата аммония в молочную кислоту и её сложные эфиры

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US1668806A (en) 1926-11-29 1928-05-08 Commercial Solvents Corp Normal butyl lactate
US2029694A (en) 1934-07-30 1936-02-04 Commercial Soivents Corp Esterification process
US2334524A (en) 1942-04-14 1943-11-16 Apex Chem Co Inc Purifying hydroxy aliphatic acids
US2465772A (en) 1944-02-17 1949-03-29 Nat Dairy Res Lab Inc Preparation of alkyl lactates
US2565487A (en) 1948-12-27 1951-08-28 Edward M Filachione Production of esters
US2722541A (en) 1950-08-02 1955-11-01 Henry E Schulz Process of esterifying butyl lactate
FR2308611A1 (fr) 1975-04-24 1976-11-19 Rhone Poulenc Ind Procede de recuperation de l'acide acetique a partir de ses solutions aqueuses de faible concentration
US4444881A (en) * 1981-10-26 1984-04-24 Cpc International Inc. Recovery of organic acids from a fermentation broth
US5252473A (en) * 1990-01-23 1993-10-12 Battelle Memorial Institute Production of esters of lactic acid, esters of acrylic acid, lactic acid, and acrylic acid
US5071754A (en) 1990-01-23 1991-12-10 Battelle Memorial Institute Production of esters of lactic acid, esters of acrylic acid, lactic acid, and acrylic acid
US5210296A (en) * 1990-11-19 1993-05-11 E. I. Du Pont De Nemours And Company Recovery of lactate esters and lactic acid from fermentation broth
CN1033024C (zh) * 1992-01-15 1996-10-16 黄玉龙 从已二酸生产废液中提取二羧酸及其酯类的方法
JP3502419B2 (ja) * 1993-03-02 2004-03-02 株式会社武蔵野化学研究所 乳酸および乳酸エステルの製造方法
US5510526A (en) * 1993-06-29 1996-04-23 Cargill, Incorporated Lactic acid production, separation and/or recovery process
US5426219A (en) 1993-07-26 1995-06-20 A.E. Staley Manufacturing Co. Process for recovering organic acids
CN1102325A (zh) * 1993-11-05 1995-05-10 段和平 脑活素口服液的制备方法及其产品
DE4341770A1 (de) * 1993-12-08 1995-06-14 Basf Ag Verfahren zur Herstellung von Milchsäureestern
US5723639A (en) 1995-10-16 1998-03-03 University Of Chicago Esterification of fermentation-derived acids via pervaporation
US5766439A (en) * 1996-10-10 1998-06-16 A. E. Staley Manufacturing Co. Production and recovery of organic acids

Also Published As

Publication number Publication date
WO2000064850A1 (en) 2000-11-02
EP1173402A4 (de) 2002-08-14
EP1173402B1 (de) 2006-06-21
ATE330929T1 (de) 2006-07-15
AU4473200A (en) 2000-11-10
EP1173402A1 (de) 2002-01-23
BR0011220A (pt) 2003-11-18
CN1382114A (zh) 2002-11-27
DK1173402T3 (da) 2006-10-23
DE60028958T2 (de) 2007-02-08
ES2267528T3 (es) 2007-03-16
PT1173402E (pt) 2006-10-31
US6291708B1 (en) 2001-09-18
CN1315772C (zh) 2007-05-16

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Legal Events

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8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee