DE69921229D1 - Verfahren zur Herstellung von Lithium enthaltendes Manganoxid - Google Patents

Verfahren zur Herstellung von Lithium enthaltendes Manganoxid

Info

Publication number
DE69921229D1
DE69921229D1 DE69921229T DE69921229T DE69921229D1 DE 69921229 D1 DE69921229 D1 DE 69921229D1 DE 69921229 T DE69921229 T DE 69921229T DE 69921229 T DE69921229 T DE 69921229T DE 69921229 D1 DE69921229 D1 DE 69921229D1
Authority
DE
Germany
Prior art keywords
preparation
manganese oxide
oxide containing
containing lithium
lithium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69921229T
Other languages
English (en)
Other versions
DE69921229T2 (de
Inventor
Akshaya Kumar Padhi
Chithambarathanu Pillai
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Carus LLC
Original Assignee
Carus LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Carus LLC filed Critical Carus LLC
Application granted granted Critical
Publication of DE69921229D1 publication Critical patent/DE69921229D1/de
Publication of DE69921229T2 publication Critical patent/DE69921229T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/02Oxides; Hydroxides
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00Compounds of manganese
    • C01G45/12Manganates manganites or permanganates
    • C01G45/1221Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof
    • C01G45/1242Manganates or manganites with a manganese oxidation state of Mn(III), Mn(IV) or mixtures thereof of the type [Mn2O4]-, e.g. LiMn2O4, Li[MxMn2-x]O4
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/131Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/13Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139Processes of manufacture
    • H01M4/1391Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/30Three-dimensional structures
    • C01P2002/32Three-dimensional structures spinel-type (AB2O4)
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/51Particles with a specific particle size distribution
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries
DE69921229T 1998-05-21 1999-05-14 Verfahren zur Herstellung von Lithium enthaltendes Manganoxid Expired - Fee Related DE69921229T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/082,329 US5955052A (en) 1998-05-21 1998-05-21 Method for making lithiated manganese oxide
US82329 1998-05-21

Publications (2)

Publication Number Publication Date
DE69921229D1 true DE69921229D1 (de) 2004-11-25
DE69921229T2 DE69921229T2 (de) 2006-03-09

Family

ID=22170526

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69921229T Expired - Fee Related DE69921229T2 (de) 1998-05-21 1999-05-14 Verfahren zur Herstellung von Lithium enthaltendes Manganoxid

Country Status (8)

Country Link
US (2) US5955052A (de)
EP (1) EP0959045B1 (de)
JP (1) JP2000034127A (de)
KR (1) KR100636446B1 (de)
CA (1) CA2271516C (de)
DE (1) DE69921229T2 (de)
HK (1) HK1023979A1 (de)
TW (1) TW504498B (de)

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US6482374B1 (en) * 1999-06-16 2002-11-19 Nanogram Corporation Methods for producing lithium metal oxide particles
US6083475A (en) * 1999-04-02 2000-07-04 Rentech, Inc. Method for making lithiated metal oxide
EP1089365B1 (de) * 1999-10-01 2016-07-20 Tosoh Corporation Lithium-Mangan-Oxid und Verfahren zu seiner Herstellung und es verwendende Sekundärzelle.
JP2001273898A (ja) * 2000-01-20 2001-10-05 Japan Storage Battery Co Ltd 非水電解質二次電池用正極活物質およびその製造方法並びにそれを使用した非水電解質二次電池
US6759167B2 (en) 2001-11-19 2004-07-06 The Gillette Company Primary lithium electrochemical cell
US6783893B2 (en) * 2001-11-19 2004-08-31 The Gillette Company Alkaline battery
US8137842B2 (en) * 2004-01-22 2012-03-20 The Gillette Company Battery cathodes
US20080119350A1 (en) * 2006-11-20 2008-05-22 Korea Institute Of Geosciences And Mineral Resources Ion exchange type lithium adsorbent using filter and method for preparing the same
KR100912095B1 (ko) 2006-11-20 2009-08-13 한국지질자원연구원 중공사막 필터를 이용한 이온 교환형 리튬 흡착제 및 그의제조 방법
JP5014218B2 (ja) * 2007-03-22 2012-08-29 三洋電機株式会社 非水電解質二次電池
US8137761B2 (en) * 2008-06-13 2012-03-20 Caterpillar Inc. Method of coating and induction heating a component
JP2010108912A (ja) * 2008-09-30 2010-05-13 Sanyo Electric Co Ltd 非水電解質二次電池、その電池に用いられる正極活物質、及び、その正極活物質の製造方法
US8142933B2 (en) * 2009-09-30 2012-03-27 Conocophillips Company Anode material for high power lithium ion batteries
US20110219607A1 (en) * 2010-03-12 2011-09-15 Nanjundaswamy Kirakodu S Cathode active materials and method of making thereof
US20110223477A1 (en) * 2010-03-12 2011-09-15 Nelson Jennifer A Alkaline battery including lambda-manganese dioxide and method of making thereof
US8303840B2 (en) * 2010-03-12 2012-11-06 The Gillette Company Acid-treated manganese dioxide and methods of making thereof
US8298706B2 (en) 2010-03-12 2012-10-30 The Gillette Company Primary alkaline battery
CN102070199B (zh) * 2010-11-18 2012-09-05 清华大学 微米框状锰系锂离子电池阴极电极材料的制备方法
US9570741B2 (en) 2012-03-21 2017-02-14 Duracell U.S. Operations, Inc. Metal-doped nickel oxide active materials
US9028564B2 (en) 2012-03-21 2015-05-12 The Gillette Company Methods of making metal-doped nickel oxide active materials
US8703336B2 (en) 2012-03-21 2014-04-22 The Gillette Company Metal-doped nickel oxide active materials
JP6222235B2 (ja) * 2013-10-04 2017-11-08 日産自動車株式会社 非水電解質二次電池用正極活物質およびその製造方法
US9793542B2 (en) 2014-03-28 2017-10-17 Duracell U.S. Operations, Inc. Beta-delithiated layered nickel oxide electrochemically active cathode material and a battery including said material
CN110582467B (zh) 2017-05-09 2022-07-26 杜拉塞尔美国经营公司 包含β-脱锂层状氧化镍电化学活性阴极材料的电池
CN107492648B (zh) * 2017-08-18 2019-12-27 湖北文理学院 棉花基碳纤维/MnO/C材料、制备方法及应用
CN112563564B (zh) * 2020-11-13 2021-11-09 上海空间电源研究所 一种制备钠离子固体电解质的软化学合成方法
KR102492040B1 (ko) * 2021-01-08 2023-01-27 고려대학교 산학협력단 양극 활물질 제조 방법

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US4312930A (en) * 1978-09-29 1982-01-26 Union Carbide Corporation MnO2 Derived from LiMn2 O4
US4246253A (en) * 1978-09-29 1981-01-20 Union Carbide Corporation MnO2 derived from LiMn2 O4
US4590059A (en) * 1983-09-30 1986-05-20 Union Carbide Corporation Process for the production of manganese dioxide
JPH0746607B2 (ja) * 1987-01-29 1995-05-17 三洋電機株式会社 非水系二次電池
CA1331506C (en) * 1988-07-12 1994-08-23 Michael Makepeace Thackeray Method of synthesizing a lithium manganese oxide
FR2644295A1 (fr) * 1989-03-09 1990-09-14 Accumulateurs Fixes Generateur electrochimique rechargeable a anode de lithium
US5153081A (en) * 1989-07-28 1992-10-06 Csir Lithium manganese oxide compound
FR2659075B1 (fr) 1990-03-01 1992-05-29 France Etat Armement Procede de preparation d'oxydes de manganese par voie sol-gel.
US5135732A (en) * 1991-04-23 1992-08-04 Bell Communications Research, Inc. Method for preparation of LiMn2 O4 intercalation compounds and use thereof in secondary lithium batteries
US5211933A (en) * 1991-04-23 1993-05-18 Bell Communications Research, Inc. Method for preparation of LiCoO2 intercalation compound for use in secondary lithium batteries
CA2096264A1 (en) * 1993-05-14 1994-11-15 Jeffrey Raymond Dahn Novel method for preparing solid solution materials for secondary non-aqueous batteries
US5506077A (en) * 1993-06-14 1996-04-09 Koksbang; Rene Manganese oxide cathode active material
FR2707426B1 (fr) * 1993-07-09 1995-08-18 Accumulateurs Fixes Générateur électrochimique rechargeable au lithium et son procédé de réalisation.
US5478672A (en) * 1993-12-24 1995-12-26 Sharp Kabushiki Kaisha Nonaqueous secondary battery, positive-electrode active material
US5558961A (en) 1994-06-13 1996-09-24 Regents, University Of California Secondary cell with orthorhombic alkali metal/manganese oxide phase active cathode material
US5766569A (en) * 1995-09-07 1998-06-16 Kerr-Mcgee Chemical Corporation Lithium manganese oxide compound and method of preparation
US5702679A (en) * 1995-10-06 1997-12-30 Kerr-Mcgee Chemical Corp. Method of preparing Li1+X- Mn2-X O4 for use as secondary battery
US5604057A (en) * 1995-11-27 1997-02-18 General Motors Corporation Secondary cell having a lithium intercolating manganese oxide
US5605773A (en) * 1995-12-06 1997-02-25 Kerr-Mcgee Corporation Lithium manganese oxide compound and method of preparation
GB9600772D0 (en) 1996-01-15 1996-03-20 Univ St Andrews Improvements in and relating to electrochemical cells
US5753202A (en) * 1996-04-08 1998-05-19 Duracell Inc. Method of preparation of lithium manganese oxide spinel
US5976489A (en) * 1996-04-10 1999-11-02 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds
US5770018A (en) * 1996-04-10 1998-06-23 Valence Technology, Inc. Method for preparing lithium manganese oxide compounds
US5759510A (en) * 1996-10-03 1998-06-02 Carus Chemical Company Lithiated manganese oxide
US5824285A (en) * 1996-10-23 1998-10-20 Valence Technology, Inc. Method of making lithium manganese oxide compounds
US6048645A (en) * 1997-08-21 2000-04-11 Valence Technology, Inc. Method of preparing lithium ion electrochemical cells

Also Published As

Publication number Publication date
EP0959045B1 (de) 2004-10-20
EP0959045A2 (de) 1999-11-24
KR19990088267A (ko) 1999-12-27
CA2271516C (en) 2005-08-23
US5955052A (en) 1999-09-21
CA2271516A1 (en) 1999-11-21
HK1023979A1 (en) 2000-09-29
US6207129B1 (en) 2001-03-27
TW504498B (en) 2002-10-01
JP2000034127A (ja) 2000-02-02
EP0959045A3 (de) 2000-05-10
KR100636446B1 (ko) 2006-10-18
DE69921229T2 (de) 2006-03-09

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Legal Events

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8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee