EP0887701A1 - Method for preparing photosensitive image forming medium coating solution, and photothermographic elements - Google Patents
Method for preparing photosensitive image forming medium coating solution, and photothermographic elements Download PDFInfo
- Publication number
- EP0887701A1 EP0887701A1 EP98111438A EP98111438A EP0887701A1 EP 0887701 A1 EP0887701 A1 EP 0887701A1 EP 98111438 A EP98111438 A EP 98111438A EP 98111438 A EP98111438 A EP 98111438A EP 0887701 A1 EP0887701 A1 EP 0887701A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- silver salt
- mol
- dispersion
- photosensitive
- organic silver
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- LCLHHZYHLXDRQG-ZNKJPWOQSA-N pectic acid Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)O[C@H](C(O)=O)[C@@H]1OC1[C@H](O)[C@@H](O)[C@@H](OC2[C@@H]([C@@H](O)[C@@H](O)[C@H](O2)C(O)=O)O)[C@@H](C(O)=O)O1 LCLHHZYHLXDRQG-ZNKJPWOQSA-N 0.000 description 1
- ULDDEWDFUNBUCM-UHFFFAOYSA-N pentyl prop-2-enoate Chemical compound CCCCCOC(=O)C=C ULDDEWDFUNBUCM-UHFFFAOYSA-N 0.000 description 1
- 230000008447 perception Effects 0.000 description 1
- JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical compound C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 1
- CMCWWLVWPDLCRM-UHFFFAOYSA-N phenidone Chemical compound N1C(=O)CCN1C1=CC=CC=C1 CMCWWLVWPDLCRM-UHFFFAOYSA-N 0.000 description 1
- NFBAXHOPROOJAW-UHFFFAOYSA-N phenindione Chemical compound O=C1C2=CC=CC=C2C(=O)C1C1=CC=CC=C1 NFBAXHOPROOJAW-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 229950000688 phenothiazine Drugs 0.000 description 1
- 229920006287 phenoxy resin Polymers 0.000 description 1
- 239000013034 phenoxy resin Substances 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- QIWKUEJZZCOPFV-UHFFFAOYSA-N phenyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC1=CC=CC=C1 QIWKUEJZZCOPFV-UHFFFAOYSA-N 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- WRAQQYDMVSCOTE-UHFFFAOYSA-N phenyl prop-2-enoate Chemical compound C=CC(=O)OC1=CC=CC=C1 WRAQQYDMVSCOTE-UHFFFAOYSA-N 0.000 description 1
- 229940067157 phenylhydrazine Drugs 0.000 description 1
- 150000003018 phosphorus compounds Chemical class 0.000 description 1
- XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 description 1
- 239000001007 phthalocyanine dye Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920002037 poly(vinyl butyral) polymer Polymers 0.000 description 1
- 239000004584 polyacrylic acid Substances 0.000 description 1
- 229920002239 polyacrylonitrile Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000768 polyamine Chemical class 0.000 description 1
- 229920000515 polycarbonate Polymers 0.000 description 1
- 239000004417 polycarbonate Substances 0.000 description 1
- 229920006289 polycarbonate film Polymers 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920006290 polyethylene naphthalate film Polymers 0.000 description 1
- 239000010318 polygalacturonic acid Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 238000012673 precipitation polymerization Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- BOQSSGDQNWEFSX-UHFFFAOYSA-N propan-2-yl 2-methylprop-2-enoate Chemical compound CC(C)OC(=O)C(C)=C BOQSSGDQNWEFSX-UHFFFAOYSA-N 0.000 description 1
- NHARPDSAXCBDDR-UHFFFAOYSA-N propyl 2-methylprop-2-enoate Chemical compound CCCOC(=O)C(C)=C NHARPDSAXCBDDR-UHFFFAOYSA-N 0.000 description 1
- PNXMTCDJUBJHQJ-UHFFFAOYSA-N propyl prop-2-enoate Chemical compound CCCOC(=O)C=C PNXMTCDJUBJHQJ-UHFFFAOYSA-N 0.000 description 1
- JEXVQSWXXUJEMA-UHFFFAOYSA-N pyrazol-3-one Chemical class O=C1C=CN=N1 JEXVQSWXXUJEMA-UHFFFAOYSA-N 0.000 description 1
- 150000003217 pyrazoles Chemical class 0.000 description 1
- NDGRWYRVNANFNB-UHFFFAOYSA-N pyrazolidin-3-one Chemical class O=C1CCNN1 NDGRWYRVNANFNB-UHFFFAOYSA-N 0.000 description 1
- PBMFSQRYOILNGV-UHFFFAOYSA-N pyridazine Chemical compound C1=CC=NN=C1 PBMFSQRYOILNGV-UHFFFAOYSA-N 0.000 description 1
- HBCQSNAFLVXVAY-UHFFFAOYSA-N pyrimidine-2-thiol Chemical compound SC1=NC=CC=N1 HBCQSNAFLVXVAY-UHFFFAOYSA-N 0.000 description 1
- ZVJHJDDKYZXRJI-UHFFFAOYSA-N pyrroline Natural products C1CC=NC1 ZVJHJDDKYZXRJI-UHFFFAOYSA-N 0.000 description 1
- QEIQICVPDMCDHG-UHFFFAOYSA-N pyrrolo[2,3-d]triazole Chemical class N1=NC2=CC=NC2=N1 QEIQICVPDMCDHG-UHFFFAOYSA-N 0.000 description 1
- GZTPJDLYPMPRDF-UHFFFAOYSA-N pyrrolo[3,2-c]pyrazole Chemical compound N1=NC2=CC=NC2=C1 GZTPJDLYPMPRDF-UHFFFAOYSA-N 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- JWVCLYRUEFBMGU-UHFFFAOYSA-N quinazoline Chemical compound N1=CN=CC2=CC=CC=C21 JWVCLYRUEFBMGU-UHFFFAOYSA-N 0.000 description 1
- 229920005604 random copolymer Polymers 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000012260 resinous material Substances 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
- 229910052702 rhenium Inorganic materials 0.000 description 1
- WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- KIWUVOGUEXMXSV-UHFFFAOYSA-N rhodanine Chemical compound O=C1CSC(=S)N1 KIWUVOGUEXMXSV-UHFFFAOYSA-N 0.000 description 1
- 150000003283 rhodium Chemical class 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- MMRXYMKDBFSWJR-UHFFFAOYSA-K rhodium(3+);tribromide Chemical compound [Br-].[Br-].[Br-].[Rh+3] MMRXYMKDBFSWJR-UHFFFAOYSA-K 0.000 description 1
- VXNYVYJABGOSBX-UHFFFAOYSA-N rhodium(3+);trinitrate Chemical compound [Rh+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VXNYVYJABGOSBX-UHFFFAOYSA-N 0.000 description 1
- 229910052707 ruthenium Inorganic materials 0.000 description 1
- 125000002914 sec-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 229920002050 silicone resin Polymers 0.000 description 1
- IZXSLAZMYLIILP-ODZAUARKSA-M silver (Z)-4-hydroxy-4-oxobut-2-enoate Chemical compound [Ag+].OC(=O)\C=C/C([O-])=O IZXSLAZMYLIILP-ODZAUARKSA-M 0.000 description 1
- AQRYNYUOKMNDDV-UHFFFAOYSA-M silver behenate Chemical compound [Ag+].CCCCCCCCCCCCCCCCCCCCCC([O-])=O AQRYNYUOKMNDDV-UHFFFAOYSA-M 0.000 description 1
- YRSQDSCQMOUOKO-KVVVOXFISA-M silver;(z)-octadec-9-enoate Chemical compound [Ag+].CCCCCCCC\C=C/CCCCCCCC([O-])=O YRSQDSCQMOUOKO-KVVVOXFISA-M 0.000 description 1
- JKOCEVIXVMBKJA-UHFFFAOYSA-M silver;butanoate Chemical compound [Ag+].CCCC([O-])=O JKOCEVIXVMBKJA-UHFFFAOYSA-M 0.000 description 1
- MNMYRUHURLPFQW-UHFFFAOYSA-M silver;dodecanoate Chemical compound [Ag+].CCCCCCCCCCCC([O-])=O MNMYRUHURLPFQW-UHFFFAOYSA-M 0.000 description 1
- LTYHQUJGIQUHMS-UHFFFAOYSA-M silver;hexadecanoate Chemical compound [Ag+].CCCCCCCCCCCCCCCC([O-])=O LTYHQUJGIQUHMS-UHFFFAOYSA-M 0.000 description 1
- ORYURPRSXLUCSS-UHFFFAOYSA-M silver;octadecanoate Chemical compound [Ag+].CCCCCCCCCCCCCCCCCC([O-])=O ORYURPRSXLUCSS-UHFFFAOYSA-M 0.000 description 1
- OHGHHPYRRURLHR-UHFFFAOYSA-M silver;tetradecanoate Chemical compound [Ag+].CCCCCCCCCCCCCC([O-])=O OHGHHPYRRURLHR-UHFFFAOYSA-M 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 235000011150 stannous chloride Nutrition 0.000 description 1
- 239000001119 stannous chloride Chemical class 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000011115 styrene butadiene Substances 0.000 description 1
- 229920000468 styrene butadiene styrene block copolymer Polymers 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 229960002317 succinimide Drugs 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- PXQLVRUNWNTZOS-UHFFFAOYSA-N sulfanyl Chemical class [SH] PXQLVRUNWNTZOS-UHFFFAOYSA-N 0.000 description 1
- 238000010557 suspension polymerization reaction Methods 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- SJMYWORNLPSJQO-UHFFFAOYSA-N tert-butyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OC(C)(C)C SJMYWORNLPSJQO-UHFFFAOYSA-N 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- ISXSCDLOGDJUNJ-UHFFFAOYSA-N tert-butyl prop-2-enoate Chemical compound CC(C)(C)OC(=O)C=C ISXSCDLOGDJUNJ-UHFFFAOYSA-N 0.000 description 1
- IKRMQEUTISXXQP-UHFFFAOYSA-N tetrasulfane Chemical compound SSSS IKRMQEUTISXXQP-UHFFFAOYSA-N 0.000 description 1
- 150000003536 tetrazoles Chemical class 0.000 description 1
- 238000001931 thermography Methods 0.000 description 1
- VLLMWSRANPNYQX-UHFFFAOYSA-N thiadiazole Chemical compound C1=CSN=N1.C1=CSN=N1 VLLMWSRANPNYQX-UHFFFAOYSA-N 0.000 description 1
- CBDKQYKMCICBOF-UHFFFAOYSA-N thiazoline Chemical compound C1CN=CS1 CBDKQYKMCICBOF-UHFFFAOYSA-N 0.000 description 1
- 150000003556 thioamides Chemical class 0.000 description 1
- ZEMGGZBWXRYJHK-UHFFFAOYSA-N thiouracil Chemical compound O=C1C=CNC(=S)N1 ZEMGGZBWXRYJHK-UHFFFAOYSA-N 0.000 description 1
- 229950000329 thiouracil Drugs 0.000 description 1
- FYOWZTWVYZOZSI-UHFFFAOYSA-N thiourea dioxide Chemical class NC(=N)S(O)=O FYOWZTWVYZOZSI-UHFFFAOYSA-N 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- AAAQKTZKLRYKHR-UHFFFAOYSA-N triphenylmethane Chemical compound C1=CC=CC=C1C(C=1C=CC=CC=1)C1=CC=CC=C1 AAAQKTZKLRYKHR-UHFFFAOYSA-N 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 description 1
- 235000020681 well water Nutrition 0.000 description 1
- 239000002349 well water Substances 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/494—Silver salt compositions other than silver halide emulsions; Photothermographic systems ; Thermographic systems using noble metal compounds
- G03C1/498—Photothermographic systems, e.g. dry silver
- G03C1/49881—Photothermographic systems, e.g. dry silver characterised by the process or the apparatus
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/494—Silver salt compositions other than silver halide emulsions; Photothermographic systems ; Thermographic systems using noble metal compounds
- G03C1/498—Photothermographic systems, e.g. dry silver
- G03C1/49809—Organic silver compounds
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/494—Silver salt compositions other than silver halide emulsions; Photothermographic systems ; Thermographic systems using noble metal compounds
- G03C1/498—Photothermographic systems, e.g. dry silver
- G03C1/49836—Additives
- G03C1/49863—Inert additives, e.g. surfactants, binders
Abstract
Description
Designation | Units | Mn |
P-1 | -MMA(70)-EA(27)-MAA(3)- latex | 37,000 |
P-2 | -MMA(70)-2EHA(20)-St(5)-AA(5)- latex | 40,000 |
P-3 | -St(70)-Bu(25)-AA(5)- latex | 60,000 |
P-4 | -St(60)-Bu(35)-DVB(3)-MAA(2)- latex | 150,000 |
P-5 | -VC(50)-MMA(20)-EA(20)-AN(5)-AA(5)- latex | 80,000 |
P-6 | -VDC(85)-MMA(5)-EA(5)-MAA(5)- latex | 67,000 |
P-7 | -Et(90)-MAA(10)- latex | 12,000 |
MMA: methyl methacrylate EA: ethyl acrylate MAA: methacrylic acid 2EHA: 2-ethylhexyl acrylate St: styrene Bu: butadiene AA: acrylic acid DVB: divinyl benzene VC: vinyl chloride AN: acrylonitrile VDC: vinylidene chloride Et: ethylene |
Binder: | |
LACSTAR 3307B SBR latex | 430 g |
Developing addenda: | |
Tetrachlorophthalic acid | 5 g |
1,1-bis(2-hydroxy-3,5-dimethylphenyl)-3,5,5-trimethylhexane | 98 g |
Phthalazine | 9.2 g |
Tribromomethylphenylsulfone | 12 g |
4-methylphthalic acid | 7 g |
Dye: | |
Dye A (as dyed polymer particle dispersion) | 4 g |
Sample No. | Organic silver salt dispersion prepared and its grain size | Coated sample using organic silver salt dispersion and its characteristics | ||||
Designation of dispersion | Grain size | Addition of photosensitive silver salt (mol% based on organic silver) | Haze | Fog | Sensitivity | |
101 | Dispersion A | 0.93 µm | Silver halide A added (10 mol%) | 10.0 | 0.11 | 100 |
102 | Dispersion B | 0.98 µm | NO | 12.0 | 0.90 | 10 |
103 | Dispersion C | 1.25 µm | Silver halide A added (10 mol%) | 38.0 | 1.00 | 70 |
104 | Dispersion D | 0.82 µm | Silver halide A added (10 mol%) | 10.0 | 0.13 | 105 |
105 | Dispersion E | 1.20 µm | Silver halide A added (10 mol%) | 15.0 | 0.11 | 98 |
106 | Dispersion F | 1.22 µm | Silver halide A added (10 mol%) | 15.0 | 0.10 | 95 |
107 | Dispersion G | 1.60 µm | Silver halide A added (10 mol%) | 19.0 | 0.10 | 90 |
108 | Dispersion H | 1.05 µm | Silver halide A added (10 mol%) | 12.0 | 0.13 | 97 |
109 | Dispersion I | 1.12 µm | Silver halide A added (10 mol%) | 13.0 | 0.14 | 95 |
110 | Dispersion J | 1.65 µm | Silver halide A added (10 mol%) | 20.0 | 1.10 | 85 |
111 | Dispersion K | 0.93 µm | Organic silver salt partially converted into silver halide (10 mol%) | 11.0 | 0.12 | 50 |
Rating | Number of specks |
o ○ | 0 to 5 |
○ | 6 to 20 |
▵ | 20 to 100 |
X | more than 100 |
Rating | Perception |
o ○ | black |
○ | a slight tone change from black, but inoffensive |
▵ | brown, yellow, red or otherwise at a certain exposure |
X | brown, yellow, red or otherwise |
Sample No. | Photosensitive layer binder | Organic silver salt dispersion | Coating solvent | Coating surface quality | Silver tone | |
Type | Moisture content (wt%) | |||||
101 | LACSTAR 3307B | 0.6 | Dispersion A | Water | o ○ | o ○ |
201 | LACSTAR 3307B | 0.6 | Dispersion A | Water/methanol= 70/30 | o ○ | o ○ |
202 | LACSTAR 3307B | 0.6 | Dispersion A | Water/methanol =40/60 | ○ | o ○ |
203 | LACSTAR 3307B | 0.6 | Dispersion A | Water/methanol =20/80 | X | o ○ |
204 | PVA-205 | 3.2 | Dispersion A | Water | ○ | X |
205 | Gelatin | 10.5 | Dispersion A | Water | X | ▵ |
206 | P-1 | 0.6 | Dispersion A | Water | o ○ | ○ |
207 | P-2 | 0.4 | Dispersion A | Water | o ○ | ○ |
208 | P-3 | 0.3 | Dispersion A | Water | o ○ | ○ |
209 | P-4 | 0.5 | Dispersion A | Water | o ○ | ○ |
210 | P-5 | 0.3 | Dispersion A | Water | o ○ | ○ |
211 | P-6 | 0.3 | Dispersion A | Water | o ○ | ○ |
Claims (15)
- A method for preparing a photothermographic image forming medium coating solution, comprising the steps of:converting a water dispersion containing at least an organic silver salt, but substantially free of a photosensitive silver salt into a high pressure, high speed flow,causing a pressure drop to the flow, andthereafter, mixing the flow with a photosensitive silver salt.
- The method of claim 1 wherein the pressure drop is in the range of 900 to 3,000 kg/cm2.
- The method of claim 1 wherein the pressure drop is in the range of 1,500 to 3,000 kg/cm2.
- The method of claim 1 further comprising a cooling step prior to the conversion step and/or after the pressure drop step whereby said water dispersion is maintained at a temperature in the range of 5 to 90°C.
- The method of claim 1 wherein said water dispersion contains as a dispersant a compound of the following formula (I) or (II): wherein R1 represents alkyl of 1 to 4 carbon atoms, A represents recurring units of a copolymerizable ethylenically unsaturated monomer, and letters x, y and z represent the molar fractions of the respective components, x is 50 to 90 mol%, y is 0 to 50 mol%, z is 0 to 30 mol%, and x + y + z = 100 mol%, wherein R represents alkyl having at least 8 carbon atoms or aryl, R1 represents alkyl of 1 to 4 carbon atoms, A represents recurring units of a copolymerizable ethylenically unsaturated monomer, and letters x', y' and z' represent the molar fractions of the respective components, x' is 50 to 99.9 mol%, y' is 0 to 50 mol%, z' is 0 to 30 mol%, and x' + y' + z' = 100 mol%.
- The method of claim 1 wherein the conversion step uses a pressure of 100 to 600 kg/cm2 and a flow velocity of from several meters per second to about 30 m/sec.
- The method of claim 1 wherein the conversion and pressure drop steps include dispersing the flow at a flow velocity of 200 to 600 m/sec and a differential pressure upon pressure drop of 900 to 3,000 kg/cm2.
- The method of claim 7 wherein the number of dispersing cycles is 1 to 10.
- The method of claim 5 wherein the dispersant is contained in an amount of 1 to 30% by weight of the organic silver salt.
- A method for preparing a photothermographic element, comprising the steps of:converting a water dispersion containing at least a non-photosensitive organic silver salt, but substantially free of a photosensitive silver salt into a high pressure, high speed flow,causing a pressure drop to the flow,thereafter, mixing the flow with at least a photosensitive silver salt and a binder to form a coating solution, andcoating the coating solution onto a support.
- The method of claim 10 wherein the coating solution further contains a reducing agent.
- The method of claim 10 wherein the support has an undercoat layer on which the coating solution is coated.
- A photothermographic element which has been prepared using the photosensitive image forming medium coating solution of any one of claims 1 to 9, said element comprising at least a photosensitive silver salt, an organic silver salt, a reducing agent, and a binder on a support.
- The photothermographic element of claim 13 wherein said photosensitive image forming medium coating solution is based on a solvent containing at least 30% by weight of water.
- The photothermographic element of claim 13 wherein a binder in a layer containing the organic silver salt is a polymer latex having an equilibrium moisture content of up to 2% by weight at 25°C and RH 60%.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP18572497 | 1997-06-26 | ||
JP185724/97 | 1997-06-26 | ||
JP18572497A JP3821407B2 (en) | 1997-06-26 | 1997-06-26 | Method for producing photosensitive image forming medium coating solution and photothermographic material |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0887701A1 true EP0887701A1 (en) | 1998-12-30 |
EP0887701B1 EP0887701B1 (en) | 2002-11-06 |
Family
ID=16175755
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP98111438A Expired - Lifetime EP0887701B1 (en) | 1997-06-26 | 1998-06-22 | Method for preparing photosensitive image forming medium coating solution, and photothermographic elements |
Country Status (4)
Country | Link |
---|---|
EP (1) | EP0887701B1 (en) |
JP (1) | JP3821407B2 (en) |
AT (1) | ATE227441T1 (en) |
DE (1) | DE69809133T2 (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0911692A2 (en) * | 1997-10-27 | 1999-04-28 | Fuji Photo Film Co., Ltd. | Photothermographic elements |
EP1069469A1 (en) * | 1999-07-16 | 2001-01-17 | Fuji Photo Film Co., Ltd. | Thermally processed image forming material |
EP1069468A1 (en) * | 1999-07-15 | 2001-01-17 | Fuji Photo Film Co., Ltd. | A method for preparing non-photosensitive fatty acid silver salt grains and an apparatus for preparing the same |
EP1150161A2 (en) * | 2000-04-25 | 2001-10-31 | Konica Corporation | Photothermographic material and image forming method |
US6613253B1 (en) | 1999-10-01 | 2003-09-02 | Fuji Photo Film Co., Ltd. | Deformation correcting method, cutting method, deformation correcting apparatus and cutting apparatus for sheet materials |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4369876B2 (en) | 2004-03-23 | 2009-11-25 | 富士フイルム株式会社 | Silver halide photosensitive material and photothermographic material |
US20060057512A1 (en) | 2004-09-14 | 2006-03-16 | Fuji Photo Film Co., Ltd. | Photothermographic material |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5424182A (en) * | 1993-01-15 | 1995-06-13 | Labelon Corporation | Aqueous coating composition for thermal imaging film |
DE4440337A1 (en) * | 1994-11-11 | 1996-05-15 | Dds Drug Delivery Services Ges | Pharmaceutical nanosuspensions for drug application as systems with increased saturation solubility and dissolution rate |
JPH08137044A (en) * | 1994-11-04 | 1996-05-31 | Canon Inc | Manufacture of image forming medium, image forming medium and image forming method |
EP0736799A1 (en) * | 1995-04-05 | 1996-10-09 | Fuji Photo Film Co., Ltd. | Recording material and process for producing the same |
WO1997004355A1 (en) * | 1995-07-18 | 1997-02-06 | Agfa-Gevaert Naamloze Vennootschap | Photothermographic recording material coated from an aqueous medium |
-
1997
- 1997-06-26 JP JP18572497A patent/JP3821407B2/en not_active Expired - Lifetime
-
1998
- 1998-06-22 DE DE69809133T patent/DE69809133T2/en not_active Expired - Lifetime
- 1998-06-22 EP EP98111438A patent/EP0887701B1/en not_active Expired - Lifetime
- 1998-06-22 AT AT98111438T patent/ATE227441T1/en not_active IP Right Cessation
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5424182A (en) * | 1993-01-15 | 1995-06-13 | Labelon Corporation | Aqueous coating composition for thermal imaging film |
JPH08137044A (en) * | 1994-11-04 | 1996-05-31 | Canon Inc | Manufacture of image forming medium, image forming medium and image forming method |
DE4440337A1 (en) * | 1994-11-11 | 1996-05-15 | Dds Drug Delivery Services Ges | Pharmaceutical nanosuspensions for drug application as systems with increased saturation solubility and dissolution rate |
EP0736799A1 (en) * | 1995-04-05 | 1996-10-09 | Fuji Photo Film Co., Ltd. | Recording material and process for producing the same |
WO1997004355A1 (en) * | 1995-07-18 | 1997-02-06 | Agfa-Gevaert Naamloze Vennootschap | Photothermographic recording material coated from an aqueous medium |
Non-Patent Citations (1)
Title |
---|
DATABASE WPI Section Ch Week 9632, Derwent World Patents Index; Class G06, AN 96-312982, XP002078175 * |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0911692A2 (en) * | 1997-10-27 | 1999-04-28 | Fuji Photo Film Co., Ltd. | Photothermographic elements |
EP0911692A3 (en) * | 1997-10-27 | 2000-02-02 | Fuji Photo Film Co., Ltd. | Photothermographic elements |
EP1069468A1 (en) * | 1999-07-15 | 2001-01-17 | Fuji Photo Film Co., Ltd. | A method for preparing non-photosensitive fatty acid silver salt grains and an apparatus for preparing the same |
US6472546B1 (en) | 1999-07-15 | 2002-10-29 | Fuji Photo Film Co., Ltd. | Method for preparing non-photosensitive fatty acid silver salt grains and an apparatus for preparing the same |
US6818190B2 (en) | 1999-07-15 | 2004-11-16 | Fuji Photo Film Co., Ltd. | Apparatus for preparing non-photosensitive fatty acid silver salt grains |
EP1069469A1 (en) * | 1999-07-16 | 2001-01-17 | Fuji Photo Film Co., Ltd. | Thermally processed image forming material |
US6783925B1 (en) | 1999-07-16 | 2004-08-31 | Fuji Photo Film Co., Ltd | Thermally processed image forming material |
US6613253B1 (en) | 1999-10-01 | 2003-09-02 | Fuji Photo Film Co., Ltd. | Deformation correcting method, cutting method, deformation correcting apparatus and cutting apparatus for sheet materials |
US7182008B2 (en) | 1999-10-01 | 2007-02-27 | Fuji Photo Film Co., Ltd. | Sheet material cutting method for cutting thermal imaging material |
EP1150161A2 (en) * | 2000-04-25 | 2001-10-31 | Konica Corporation | Photothermographic material and image forming method |
EP1150161A3 (en) * | 2000-04-25 | 2004-09-08 | Konica Corporation | Photothermographic material and image forming method |
Also Published As
Publication number | Publication date |
---|---|
JPH1115105A (en) | 1999-01-22 |
EP0887701B1 (en) | 2002-11-06 |
DE69809133T2 (en) | 2003-04-24 |
ATE227441T1 (en) | 2002-11-15 |
DE69809133D1 (en) | 2002-12-12 |
JP3821407B2 (en) | 2006-09-13 |
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