EP1149627A2 - Dynamic mixer - Google Patents

Dynamic mixer Download PDF

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Publication number
EP1149627A2
EP1149627A2 EP01106102A EP01106102A EP1149627A2 EP 1149627 A2 EP1149627 A2 EP 1149627A2 EP 01106102 A EP01106102 A EP 01106102A EP 01106102 A EP01106102 A EP 01106102A EP 1149627 A2 EP1149627 A2 EP 1149627A2
Authority
EP
European Patent Office
Prior art keywords
mixing
dynamic mixer
mixer according
longitudinal direction
chamber part
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP01106102A
Other languages
German (de)
French (fr)
Other versions
EP1149627B1 (en
EP1149627A3 (en
Inventor
Alfred Von Schuckmann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kulzer GmbH
Original Assignee
Heraeus Kulzer GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE10015133A external-priority patent/DE10015133C1/en
Priority claimed from DE10043489A external-priority patent/DE10043489A1/en
Application filed by Heraeus Kulzer GmbH filed Critical Heraeus Kulzer GmbH
Priority to DK01106102T priority Critical patent/DK1149627T3/en
Publication of EP1149627A2 publication Critical patent/EP1149627A2/en
Publication of EP1149627A3 publication Critical patent/EP1149627A3/en
Application granted granted Critical
Publication of EP1149627B1 publication Critical patent/EP1149627B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/07—Stirrers characterised by their mounting on the shaft
    • B01F27/072—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • B01F27/0722—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis perpendicular with respect to the rotating axis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/07—Stirrers characterised by their mounting on the shaft
    • B01F27/072—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis
    • B01F27/0724—Stirrers characterised by their mounting on the shaft characterised by the disposition of the stirrers with respect to the rotating axis directly mounted on the rotating axis
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F33/00—Other mixers; Mixing plants; Combinations of mixers
    • B01F33/50—Movable or transportable mixing devices or plants
    • B01F33/501—Movable mixing devices, i.e. readily shifted or displaced from one place to another, e.g. portable during use
    • B01F33/5011—Movable mixing devices, i.e. readily shifted or displaced from one place to another, e.g. portable during use portable during use, e.g. hand-held
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/50—Mixing receptacles
    • B01F35/52—Receptacles with two or more compartments
    • B01F35/522—Receptacles with two or more compartments comprising compartments keeping the materials to be mixed separated until the mixing is initiated
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/19—Mixing dentistry compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2305—Mixers of the two-component package type, i.e. where at least two components are separately stored, and are mixed in the moment of application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/112—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades
    • B01F27/1125—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades with vanes or blades extending parallel or oblique to the stirrer axis
    • B01F27/11251—Stirrers characterised by the configuration of the stirrers with arms, paddles, vanes or blades with vanes or blades extending parallel or oblique to the stirrer axis having holes in the surface

Definitions

  • the invention relates to a dynamic mixer, in particular for viscous dental materials, with: a chamber part, with a discharge opening at the front end of the chamber part, with a closure part arranged at the rear end of the chamber part with inlet openings for individual components to be introduced, and a central bore for a mixing element which is rotatable in the chamber part about its longitudinal axis.
  • static mixer includes such to understand, which contain fixed mixing devices for example flow pins, which the individual materials to be mixed flow past and swirl and other interference.
  • dynamic mixer are to be understood as those, the active mixing devices, for example in the form of rotating Mixing blades included. In these, the components to be mixed are replaced by active ones Transport mixed together.
  • Static mixers are less because of the high friction loss with tough consistencies suitable, which is why mixers with rotating mixing elements are used in such cases.
  • EP 0 492 412 B1 discloses a dynamic mixer which essentially has a housing with a Cylindrical chamber part includes a discharge opening at its front end for the mixture, a closing body provided at the rear end of the chamber part with protruding pipe pins behind for direct insertion into outlet openings of the storage containers containing the components to be mixed, and one in the Has chamber part rotatable about its longitudinal axis mixer element that with its rear End is rotatably mounted in a bore of the end body.
  • the mixing element at least one wiper carries, with a cutting edge pointing forward in the direction of rotation, the front surface of the Cover plate sweeps, and a rising in the direction of the cutting edge on the cutting edge Adjoining the inclined surface.
  • a disadvantage of this mixer is u. a. the fact that it is a partially uncontrolled Escape of the components to be mixed between the end body and the rotating mixer element due to leaks. In addition, the degree of homogenization not satisfactory in every case, since the individual components adapt to the Push the mixer element past the molded mixer blades.
  • the underlying problem is, in particular, an inexpensive dynamic Mixer for single use with low-viscosity to tough, stable multi-component materials to develop a very high degree of homogenization or tightness guaranteed.
  • this problem is solved by a dynamic mixer according to claim 1 solved.
  • the dynamic mixer according to the invention has a chamber part, a discharge opening on front end of the chamber part, a closure part arranged at the rear end of the chamber part with inlet openings for individual components to be inserted and a central one Bore for a mixing element that is rotatable about its longitudinal axis in the chamber part.
  • the Mixing element has at least two inches on its side facing the closure part Longitudinally arranged mixing blades on the wall of the Chamber part are not designed to strip material, and the axially free passages have, wherein in the axial direction the passages of a mixing wing each through the free part of the other mixing wing are covered.
  • not stripping material is to understand the fact that the mixing blades used are not wall-accessible and act as a scraper, but keep a certain distance from the individual walls.
  • the staggered arrangement of the mixing blades ensures that Material not recorded by the first mixing wing with a very high probability by the second Mixing blades are recorded, sheared and then mixed with the other components.
  • the sleeve increases the stator area (under the term “Stator surface” are all fixed and for the mixing of the individual components necessary surfaces) and the sealing surface (under the term “sealing surface” are to be understood as areas that allow the individual to flow out in an uncontrolled manner Prevent or reduce constituents or the mixed constituents to the outside and thus perform a sealing function).
  • the mixing blades are free of rises in the longitudinal direction in which they are spread are formed (i.e. have no inclined blades in the plane of rotation), because in this way there is no discharge effect when the mixing blades rotate and thus the mixing element and its connection point to the drive axis of a not too high one are exposed to mechanical stress. Discharge is only done by pressing in the longitudinal direction of the chamber part accomplished.
  • the first arranged at the rear end of the chamber part Mixing wing molded in the direction of the closure part in the longitudinal direction at least one mixing pin is that the viscous material entering from the inlet openings is free of cuts is passed since this enables a very high shear rate.
  • At least one essentially in the longitudinal direction is advantageously on the closure part Aligned inner pin arranged as a flow disturbance to increase the mixing effect serves.
  • the first mixing wing is advantageously dome-shaped in the deploying longitudinal direction trained in this way a low mixing and dead volume in dynamic Mixer remaining amount (after use) between the first and second To provide mixing blades.
  • the first mixing wing has inner and / or outer recesses has to ensure a better material throughput.
  • the inner recesses can be configured, for example, in the form of circles or ellipses, while the outer recesses, for example semicircular or parabolic circular segments can represent.
  • the second mixing wing for example, outer recesses in the form of circular segments to ensure a higher material throughput.
  • the second mixing blade has a material reinforcement in the longitudinal direction of the chamber part, for example in the form of a doubled round cross, in order in this way and Way to provide material redundancy for high mechanical resilience.
  • the mixing element has at least one in the dispensing longitudinal direction third mixing wing on, for further homogenization of the mixed to be applied Material.
  • in at least one inlet opening at least one transverse to the Passage-oriented web-shaped element is arranged so that any hardening when removing the used mixer from the tubular bag / cartridge be pulled out with.
  • Web-shaped elements that have oval, diamond, are elliptical, polygonal or circular.
  • Sprayable plastics such as polyethylene, polypropylene or polystyrene have become particularly popular Proven for housing and end body (chamber part or closure part).
  • plastics such as polyethylene, polypropylene or polystyrene
  • FIG. 1 shows a cross section through a dynamic mixer according to the invention.
  • the dynamic mixer has a chamber part 1, a discharge opening 13 at the front end of the chamber part 1, a closure part 2 arranged at the rear end of the chamber part 1 Inlet openings 11 for individual components to be introduced and a central bore for a mixing element and a mixing element 3 rotatable about its longitudinal axis in the chamber part 1 on.
  • the mixing element 3 has two in the longitudinal direction one behind the other and radially offset in this way arranged stripping function-free mixing blades 5, 6 that the free passages of the first Mixing wing 5 are covered by the second mixing wing 6.
  • On the closure part 2 is a arranged essentially in the longitudinal direction of the sleeve 4, which is the rear end of the Mixing element 3 encompasses.
  • the mixing blades 5, 6 are designed to be free of rises in the deploying longitudinal direction (no inclined provided blades).
  • the first mixing wing 5 is in the direction of the closure part 2 in the longitudinal direction a mixing pin 10 integrally formed.
  • the first mixing wing 5 does not run in the wall part 1, d. H. it does not touch the housing wall 9 and forms between this and the first Mixing blades 5 two spacing volumes 7.
  • the closure part 2 has a rear base plate 8 on.
  • the mixing element 3 has four third mixing blades 14, 15, 16, 17 in the dispensing direction on.
  • FIG. 2 shows an excerpted cross section with respect to a further variant of the mixer according to the invention.
  • two pins 12 which are oriented essentially in the longitudinal direction are arranged on the closure part 2.
  • Figure 3 shows a cross section of a mixing element.
  • the mixing element 3 consists essentially of two in the longitudinal direction and one behind the other radially offset staggered mixing blades 5, 6, the free Passages of the first mixing wing 5 are covered by the second mixing wing 6. In spreading In the longitudinal direction, the mixing element 3 has four further third mixing blades 14, 15, 16, 17 on.
  • FIG. 4 shows a top view of a first mixing blade.
  • the first mixing blade 5 has inner and outer recesses 18, 19.
  • FIG. 5 shows a top view of a second mixing blade.
  • the second mixing blade 6 has a material reinforcement 21 in the longitudinal direction of the chamber part 1 and outer recesses 20.
  • Figures 6 and 7 show a cross section or a sketchy bottom view of the invention Mixer.
  • An inlet opening 11 has a diamond-shaped, transverse to the flow direction aligned web-shaped element 22.

Abstract

Dynamic mixer has a mixing element (3) with mixing wings (5, 6) arranged on the side facing the closing part (2). The wings are non material-stripping with respect to the wall of the chamber part (1) and have axially free recesses, where the recesses of one wing are covered by the non-free part of the other wing. An inner sleeve (4) which extends up to the first mixing wing is arranged on the closing part. Preferred Features: The mixing wings are arranged in the longitudinal direction. An inner peg (12) is arranged on the closing part. The first mixing wing has inner and/or outer recesses and the second mixing wing has only outer recesses. The mixer has a third mixing wing (14, 15, 16, 17).

Description

Die Erfindung betrifft einen dynamischen Mischer, insbesondere für viskose Dentalmaterialien, mit:
   einem Kammerteil, mit einer Ausbringöffnung am vorderen Ende des Kammerteils, mit einem am hinteren Ende des Kammerteils angeordneten Verschlussteil mit Eintrittsöffnungen für einzubringende Einzelkomponenten sowie einer zentrischen Bohrung für ein Mischelement, das im Kammerteil um seine Längsachse drehbar ist.The invention relates to a dynamic mixer, in particular for viscous dental materials, with:
a chamber part, with a discharge opening at the front end of the chamber part, with a closure part arranged at the rear end of the chamber part with inlet openings for individual components to be introduced, and a central bore for a mixing element which is rotatable in the chamber part about its longitudinal axis.

Beim maschinellen kontinuierlichen Anmischen von Mehrkomponentenmaterialien, beispielsweise von Klebstoffen oder dentalen Abdruckmassen, ist es üblich, je nach Konsistenz dynamische oder statische Mischer zu verwenden. Unter dem Begriff "statischer Mischer" sind solche zu verstehen, die feststehende Mischeinrichtungen beispielsweise Strömungsstifte enthalten, an denen die zu vermischenden einzelnen Materialien vorbeiströmen und sich durch Verwirbelung und anderen Störungen miteinander mischen. Unter dem Begriff "dynamischer Mischer" sind solche zu verstehen, die aktive Mischeinrichtungen beispielsweise in Form von rotierenden Mischflügeln enthalten. Bei diesen werden die zu vermischenden Bestandteile durch aktiven Transport miteinander vermischt.When continuously mixing multicomponent materials, for example of adhesives or dental impression materials, it is common, depending on the consistency dynamic or use static mixers. The term "static mixer" includes such to understand, which contain fixed mixing devices for example flow pins, which the individual materials to be mixed flow past and swirl and other interference. Under the term "dynamic mixer" are to be understood as those, the active mixing devices, for example in the form of rotating Mixing blades included. In these, the components to be mixed are replaced by active ones Transport mixed together.

Statische Mischer sind wegen des hohen Reibungsverlustes bei zähen Konsistenzen weniger geeignet, weshalb in solchen Fällen Mischer mit rotierenden Mischelementen verwendet werden.Static mixers are less because of the high friction loss with tough consistencies suitable, which is why mixers with rotating mixing elements are used in such cases.

In DE 297 05 741 U1 ist ein dynamischer Mischer für zähe Massen, insbesondere für die Komponenten von zahnärztlichen Abdruckmassen, offenbart, der einerseits mit einem Masseausbringgerät verbindbar und andererseits eine Ausbringdüse für das Gemisch bildet oder damit verbindbar ist und ein Mischrohr, eine darin umlaufend antreibbare, mit dem Mischrohr einen ringförmigen Mischkanal bildende Mischerwelle und Mischerflügel umfasst, die ausschließlich von der Mischerwelle etwa radial zur Mischrohrwand vorspringen, wobei der dynamische Mischer dadurch gekennzeichnet ist, dass die radiale Weite des Mischkanals nicht größer als 2 mm ist.DE 297 05 741 U1 describes a dynamic mixer for viscous masses, especially for the components of dental impression compounds, disclosed on the one hand with a mass application device connectable and on the other hand forms a discharge nozzle for the mixture or so is connectable and a mixing tube, one can be driven circumferentially therein, with the mixing tube one annular mixing channel forming mixer shaft and mixer blades, which exclusively Project from the mixer shaft approximately radially to the wall of the mixing tube, the dynamic mixer characterized in that the radial width of the mixing channel is not greater than Is 2 mm.

In EP 0 492 412 B1 ist ein dynamischer Mischer offenbart, der ein Gehäuse mit einem im wesentlichen zylindrischen Kammerteil umfasst, der an seinem vorderen Ende einer Ausbringöffnung für das Gemisch, einen am hinteren Ende des Kammerteils vorgesehenen Abschlusskörper mit nach hinter herausragenden Rohrzapfen zum unmittelbaren Einführen in Austrittsöffnungen von die zu mischenden Komponenten enthaltenden Vorratsbehältern, und ein in dem Kammerteil um dessen Längsachse drehbares Mischerelement aufweist, dass mit seinem hinteren Ende in einer Bohrung des Abschlusskörpers drehbar gelagert ist. Dabei ist der Abschlusskörper als Platte ausgebildet, wobei das Mischelement mindestens einen Abstreifer trägt, der mit einer in Drehrichtung nach vorne weisenden Schneidkante die vordere Fläche der Abschlussplatte überstreicht, und sich an die Schneidkante eine in Ausbringrichtung ansteigende Schrägfläche anschliesst.EP 0 492 412 B1 discloses a dynamic mixer which essentially has a housing with a Cylindrical chamber part includes a discharge opening at its front end for the mixture, a closing body provided at the rear end of the chamber part with protruding pipe pins behind for direct insertion into outlet openings of the storage containers containing the components to be mixed, and one in the Has chamber part rotatable about its longitudinal axis mixer element that with its rear End is rotatably mounted in a bore of the end body. Here is the final body formed as a plate, the mixing element at least one wiper carries, with a cutting edge pointing forward in the direction of rotation, the front surface of the Cover plate sweeps, and a rising in the direction of the cutting edge on the cutting edge Adjoining the inclined surface.

Nachteilig an diesem Mischer ist u. a. die Tatsache, dass es zu einem teilweise unkontrollierten Austreten der zu mischenden Komponenten zwischen Abschlusskörper und drehbarem Mischerelement aufgrund von Undichtigkeiten kommt. Darüber hinaus ist der Homogenisierungsgrad nicht in jedem Fall befriedigend, da sich die einzelnen Komponenten zu schnell an den am Mischerelement angeformten Mischerflügeln vorbeischieben.A disadvantage of this mixer is u. a. the fact that it is a partially uncontrolled Escape of the components to be mixed between the end body and the rotating mixer element due to leaks. In addition, the degree of homogenization not satisfactory in every case, since the individual components adapt to the Push the mixer element past the molded mixer blades.

Aus dem Vorgenannten ergibt sich das Problem, mit Hilfe eines neuartigen dynamischen Mischers die oben genannten Nachteile zumindest teilweise zu beseitigen. Das der Erfindung zugrundeliegende Problem liegt insbesondere darin, einen preiswert herzustellenden dynamischen Mischer für die Einmalverwendung bei niedrigviskosen bis zähen standfesten Mehrkomponentenmaterialien zu entwickeln, der einen sehr hohen Homogenisierungs- bzw. Dichtigkeitsgrad gewährleistet.The problem arises from the above, with the aid of a novel dynamic mixer to at least partially eliminate the disadvantages mentioned above. That of the invention the underlying problem is, in particular, an inexpensive dynamic Mixer for single use with low-viscosity to tough, stable multi-component materials to develop a very high degree of homogenization or tightness guaranteed.

Dieses Problem wird erfindungsgemäss durch einen dynamischen Mischer nach Anspruch 1 gelöst.According to the invention, this problem is solved by a dynamic mixer according to claim 1 solved.

Der erfindungsgemäße dynamische Mischer weist ein Kammerteil, eine Ausbringöffnung am vorderen Ende des Kammerteils, ein am hinteren Ende des Kammerteils angeordnetes Verschlussteil mit Eintrittsöffnungen für einzubringende Einzelkomponenten sowie eine zentrische Bohrung für ein Mischelement, das im Kammerteil um seine Längsachse drehbar ist, auf. Das Mischelement weist auf seiner dem Verschlussteil zugewandten Seite mindestens zwei in Längsrichtung hintereinander angeordnete Mischflügel auf, die bezüglich der Wandung des Kammerteils nicht materialabstreifend ausgestaltet sind, und die jeweils axial freie Durchlässe aufweisen, wobei in axialer Richtung die Durchlässe eines Mischflügels jeweils durch den nicht freien Teil des anderen Mischflügels abgedeckt sind. Unter dem Begriff "nicht Material abstreifend" ist die Tatsache zu verstehen, dass die eingesetzten Mischflügel nicht wandgängig sind und als Abstreifer fungieren, sondern einen gewissen Abstand zu den einzelnen Wänden einhalten. Durch die versetzte Anordnung der Mischflügel untereinander wird gewährleistet, dass vom ersten Mischflügel nicht erfasstes Material mit sehr hoher Wahrscheinlichkeit vom zweiten Mischflügel erfasst, geschert und anschließend mit den anderen Komponenten vermischt wird.The dynamic mixer according to the invention has a chamber part, a discharge opening on front end of the chamber part, a closure part arranged at the rear end of the chamber part with inlet openings for individual components to be inserted and a central one Bore for a mixing element that is rotatable about its longitudinal axis in the chamber part. The Mixing element has at least two inches on its side facing the closure part Longitudinally arranged mixing blades on the wall of the Chamber part are not designed to strip material, and the axially free passages have, wherein in the axial direction the passages of a mixing wing each through the free part of the other mixing wing are covered. Under the term "not stripping material" is to understand the fact that the mixing blades used are not wall-accessible and act as a scraper, but keep a certain distance from the individual walls. The staggered arrangement of the mixing blades ensures that Material not recorded by the first mixing wing with a very high probability by the second Mixing blades are recorded, sheared and then mixed with the other components.

Am Verschlussteil ist eine das hintere Ende des Mischelementes umgreifende im wesentlichen in Längsrichtung ausgerichtete innere Hülse angeordnet, die sich nahezu bis zum ersten Mischflügel erstreckt. Die Hülse sorgt für eine Erhöhung der Statorfläche (unter dem Begriff "Statorfläche" sind sämtliche stehenden festen und für die Vermischung der einzelnen Komponenten notwendigen Flächen zu verstehen) und der Dichtungsfläche (unter dem Begriff "Dichtungsfläche" sind solche Flächen zu verstehen, die ein unkontrolliertes Herausfließen der einzelnen Bestandteile bzw. der gemischen Bestandteile nach außen verhindern bzw. vermindern und so eine dichtende Funktion ausüben). Durch die Anordnung als am hinteren Ende des Mischelementes umgreifende Hülse ist eine hohe Dichtwirkung erzielbar.At the closure part there is essentially one that encompasses the rear end of the mixing element arranged in the longitudinal direction inner sleeve, which extends almost to the first Mixing wing extends. The sleeve increases the stator area (under the term "Stator surface" are all fixed and for the mixing of the individual components necessary surfaces) and the sealing surface (under the term "sealing surface" are to be understood as areas that allow the individual to flow out in an uncontrolled manner Prevent or reduce constituents or the mixed constituents to the outside and thus perform a sealing function). By the arrangement as at the rear end of the A high sealing effect can be achieved by the sleeve encompassing the mixing element.

Zunächst ist es vorteilhaft, wenn die Mischflügel in ausbringender Längsrichtung anstiegsfrei ausgebildet sind (d. h. in der Rotationsebene keine schräggestellten Flügelblätter aufweisen), da auf diese Art und Weise keine Austragswirkung bei Rotation der Mischflügel resultiert und somit das Mischelement und deren Verbindungsstelle zur Antriebsachse einer nicht allzu hohen mechanischen Belastung ausgesetzt sind. Ein Austrag wird lediglich durch Pressen in Längsrichtung des Kammerteils bewerkstelligt.First of all, it is advantageous if the mixing blades are free of rises in the longitudinal direction in which they are spread are formed (i.e. have no inclined blades in the plane of rotation), because in this way there is no discharge effect when the mixing blades rotate and thus the mixing element and its connection point to the drive axis of a not too high one are exposed to mechanical stress. Discharge is only done by pressing in the longitudinal direction of the chamber part accomplished.

Weiterhin ist es vorteilhaft, dass am am hinteren Ende des Kammerteils angeordneten ersten Mischflügel in Richtung Verschlussteil in Längsrichtung derart mindestens ein Mischzapfen angeformt ist, dass das aus den Eintrittsöffnungen eintretende viskose Material zerschneidungsfrei verstrichen wird, da auf diese Art und Weise eine sehr hohe Scherungsrate ermöglicht wird.Furthermore, it is advantageous that the first arranged at the rear end of the chamber part Mixing wing molded in the direction of the closure part in the longitudinal direction at least one mixing pin is that the viscous material entering from the inlet openings is free of cuts is passed since this enables a very high shear rate.

Am Verschlussteil ist in vorteilhafter Weise mindestens ein im wesentlichen in Längsrichtung ausgerichteter innerer Zapfen angeordnet, der als Strömungsstörer zur Erhöhung der Mischwirkung dient. At least one essentially in the longitudinal direction is advantageously on the closure part Aligned inner pin arranged as a flow disturbance to increase the mixing effect serves.

Der erste Mischflügel ist in vorteilhafter Weise in ausbringender Längsrichtung kuppelförmig ausgebildet, um auf diese Art und Weise ein geringes Misch- und Totvolumen der im dynamischen Mischer verbleibenden Restmenge (nach Gebrauch) zwischen dem ersten und zweiten Mischflügel bereitzustellen.The first mixing wing is advantageously dome-shaped in the deploying longitudinal direction trained in this way a low mixing and dead volume in dynamic Mixer remaining amount (after use) between the first and second To provide mixing blades.

Weiterhin ist es von Vorteil, wenn der erste Mischflügel innere und/oder äussere Ausnehmungen aufweist, um einen besseren Materialdurchsatz zu gewährleisten. Die inneren Ausnehmungen können beispielsweise in Form von Kreisen oder Ellipsen ausgestaltet sein, während die äusseren Ausnehmungen beispielsweise halbkreisförmige oder paraboloide Kreissegmente darstellen können.It is also advantageous if the first mixing wing has inner and / or outer recesses has to ensure a better material throughput. The inner recesses can be configured, for example, in the form of circles or ellipses, while the outer recesses, for example semicircular or parabolic circular segments can represent.

Weiterhin ist es von Vorteil, wenn der zweite Mischflügel äussere Ausnehmungen, beispielsweise in Form von Kreissegmenten aufweist, um einen höheren Materialdurchsatz zu gewährleisten.It is also advantageous if the second mixing wing, for example, outer recesses in the form of circular segments to ensure a higher material throughput.

Weiterhin weist der zweite Mischflügel in Längsrichtung des Kammerteils eine Materialverstärkung, beispielsweise in Form eines aufgedoppelten Rundkreuzes, auf, um auf diese Art und Weise eine Materialredundanz zur hohen mechanischen Belastbarkeit bereitzustellen.Furthermore, the second mixing blade has a material reinforcement in the longitudinal direction of the chamber part, for example in the form of a doubled round cross, in order in this way and Way to provide material redundancy for high mechanical resilience.

Darüber hinaus, weist das Mischelement in ausbringender Längsrichtung mindestens einen dritten Mischflügel auf, der zur weiteren Homogenisierung des auszubringenden gemischten Materials dient.In addition, the mixing element has at least one in the dispensing longitudinal direction third mixing wing on, for further homogenization of the mixed to be applied Material.

Schließlich ist es von Vorteil, wenn in mindestens einer Eintrittsöffnung mindestens ein quer zur Durchlassöffnung ausgerichtetes stegförmiges Element angeordnet ist, damit eventuelle Aushärtungen beim Abnehmen des gebrauchten Mischers vom Schlauchbeutel/von der Kartusche mit herausgezogen werden.Finally, it is advantageous if in at least one inlet opening at least one transverse to the Passage-oriented web-shaped element is arranged so that any hardening when removing the used mixer from the tubular bag / cartridge be pulled out with.

Besonders bewährt haben sich stegförmige Elemente, die in Durchflussrichtung oval-, rauten-, ellipsen-, vieleck- oder kreisförmig sind.Web-shaped elements that have oval, diamond, are elliptical, polygonal or circular.

Spritzbare Kunststoffe wie Polyethylen, Polypropylen oder Polystyiol haben sich insbesondere für Gehäuse und Abschlusskörper (Kammerteil bzw. Verschlussteil) bewährt. Für den Einsatz bei zäheren Mischungen ist insbesondere beim Mischelement die Verwendung von hochwertigeren Kunststoffen wie z. B. Polyamid, Polyoximethylen oder anderen schlagzäheren Polymeren/Blends vorteilhaft. Sprayable plastics such as polyethylene, polypropylene or polystyrene have become particularly popular Proven for housing and end body (chamber part or closure part). For use in the case of tougher mixtures, in particular in the case of the mixing element, the use of higher quality is required Plastics such. B. polyamide, polyoxymethylene or other impact-resistant polymers / blends advantageous.

Die Erfindung wird anhand eines nachfolgenden Beispiels näher erläutert.The invention is explained in more detail with the aid of the following example.

Die Zeichnungen zeigen:

Figur 1 -
einen Querschnitt durch einen erfindungsgemässen dynamischen Mischer;
Figur 2 -
einen auszugsweisen Querschnitt bezüglich einer weiteren Variante des erfindungsgemässen Mischers;
Figur 3 -
einen Querschnitt eines Mischelements;
Figur 4 -
eine Aufsicht eines ersten Mischflügels;
Figur 5 -
eine Aufsicht eines zweiten Mischflügels;
Figur 6-
einen Querschnitt des erfindungsgemäßen dynamischen Mischers und
Figur 7 -
eine skizzenhafte untere Aufsicht des in Figur 6 dargestellten erfindungsgemäßen Mischers.
The drawings show:
Figure 1 -
a cross section through a dynamic mixer according to the invention;
Figure 2 -
an excerpt cross section with respect to a further variant of the mixer according to the invention;
Figure 3 -
a cross section of a mixing element;
Figure 4 -
a top view of a first mixing wing;
Figure 5 -
a top view of a second mixing wing;
Figure 6-
a cross section of the dynamic mixer according to the invention and
Figure 7 -
a sketchy bottom view of the mixer according to the invention shown in Figure 6.

In Figur 1 ist ein Querschnitt durch einen erfindungsgemässen dynamischen Mischer abgebildet.1 shows a cross section through a dynamic mixer according to the invention.

Der dynamische Mischer weist ein Kammerteil 1, eine Ausbringöffnung 13 am vorderen Ende des Kammerteils 1, ein am hinteren Ende des Kammerteils 1 angeordnetes Verschlussteil 2 mit Eintrittsöffnungen 11 für einzubringende Einzelkomponenten sowie eine zentrische Bohrung für ein Mischelement und ein um dessen Längsachse im Kammerteil 1 drehbares Mischelement 3 auf. Das Mischelement 3 weist zwei in Längsrichtung hintereinander und radial derart versetzt angeordnete abstreifenfunktionsfreie Mischflügel 5, 6 auf, dass die freien Durchlässe des ersten Mischflügels 5 vom zweiten Mischflügel 6 abgedeckt werden. Am Verschlussteil 2 ist eine im wesentlichen in Längsrichtung ausgerichtete Hülse 4 angeordnet, die das hintere Ende des Mischelements 3 umgreift.The dynamic mixer has a chamber part 1, a discharge opening 13 at the front end of the chamber part 1, a closure part 2 arranged at the rear end of the chamber part 1 Inlet openings 11 for individual components to be introduced and a central bore for a mixing element and a mixing element 3 rotatable about its longitudinal axis in the chamber part 1 on. The mixing element 3 has two in the longitudinal direction one behind the other and radially offset in this way arranged stripping function-free mixing blades 5, 6 that the free passages of the first Mixing wing 5 are covered by the second mixing wing 6. On the closure part 2 is a arranged essentially in the longitudinal direction of the sleeve 4, which is the rear end of the Mixing element 3 encompasses.

Die Mischflügel 5, 6 sind in ausbringender Längsrichtung anstiegsfrei ausgebildet (keine schräg gestellten Flügelblätter). Am ersten Mischflügel 5 ist in Richtung Verschlussteil 2 in Längsrichtung ein Mischzapfen 10 angeformt. Der erste Mischflügel 5 läuft im Kammerteil 1 nicht wandgängig, d. h. er berührt nicht die Gehäusewandung 9 und bildet zwischen dieser und dem ersten Mischflügel 5 zwei Abstandvolumen 7. Das Verschlussteil 2 weist eine hintere Bodenplatte 8 auf. Das Mischelement 3 weist in ausbringender Richtung vier dritte Mischflügel 14, 15, 16, 17 auf. The mixing blades 5, 6 are designed to be free of rises in the deploying longitudinal direction (no inclined provided blades). The first mixing wing 5 is in the direction of the closure part 2 in the longitudinal direction a mixing pin 10 integrally formed. The first mixing wing 5 does not run in the wall part 1, d. H. it does not touch the housing wall 9 and forms between this and the first Mixing blades 5 two spacing volumes 7. The closure part 2 has a rear base plate 8 on. The mixing element 3 has four third mixing blades 14, 15, 16, 17 in the dispensing direction on.

In Figur 2 ist ein auszugsweiser Querschnitt bezüglich einer weiteren Variante des erfindungsgemässen Mischers dargestellt.
Bei dieser Variante sind am Verschlussteil 2 zwei im wesentlichen in Längsrichtung ausgerichtete Zapfen 12 angeordnet.FIG. 2 shows an excerpted cross section with respect to a further variant of the mixer according to the invention.
In this variant, two pins 12 which are oriented essentially in the longitudinal direction are arranged on the closure part 2.

Figur 3 zeigt einen Querschnitt eines Mischelementes.Figure 3 shows a cross section of a mixing element.

Das Mischelement 3 besteht im wesentlichen aus zwei in Längsrichtung hintereinander und radial derart versetzt angeordnete abstreifenfunktionsfreie Mischflügel 5, 6, wobei die freien Durchlässe des ersten Mischflügels 5 vom zweiten Mischflügel 6 abgedeckt werden. In ausbringender Längsrichtung weist das Mischelement 3 vier weitere dritte Mischflügel 14, 15, 16, 17 auf.The mixing element 3 consists essentially of two in the longitudinal direction and one behind the other radially offset staggered mixing blades 5, 6, the free Passages of the first mixing wing 5 are covered by the second mixing wing 6. In spreading In the longitudinal direction, the mixing element 3 has four further third mixing blades 14, 15, 16, 17 on.

Figur 4 zeigt eine Aufsicht eines ersten Mischflügels.FIG. 4 shows a top view of a first mixing blade.

Der erste Mischflügel 5 weist innere und äussere Ausnehmungen 18, 19 auf.The first mixing blade 5 has inner and outer recesses 18, 19.

Figur 5 zeigt eine Aufsicht eines zweiten Mischflügels.FIG. 5 shows a top view of a second mixing blade.

Der zweite Mischflügel 6 weist in Längsrichtung des Kammerteils 1 eine Materialverstärkung 21 und äussere Ausnehmungen 20 auf.The second mixing blade 6 has a material reinforcement 21 in the longitudinal direction of the chamber part 1 and outer recesses 20.

Figuren 6 und 7 zeigen einen Querschnitt bzw. eine skizzenhafte untere Aufsicht des erfindungsgemäßen Mischers. Eine Eintrittsöffnung 11 weist ein rautenförmiges, quer zur Durchflussrichtung ausgerichtetes stegförmiges Element 22 auf.Figures 6 and 7 show a cross section or a sketchy bottom view of the invention Mixer. An inlet opening 11 has a diamond-shaped, transverse to the flow direction aligned web-shaped element 22.

Claims (12)

Dynamischer Mischer, insbesondere für viskose Dentalmaterialien, mit einem Kammerteil (1), mit einer Ausbringöffnung (13) am vorderen Ende des Kammerteils (1), mit einem am hinteren Ende des Kammerteils (1) angeordneten Verschlussteil (2) mit Eintrittsöffnungen (11) für einzubringende Einzelkomponenten sowie einer zentrischen Bohrung für ein Mischelement (3), das im Kammerteil (1) um seine Längsachse drehbar ist, dadurch gekennzeichnet, dass das Mischelement (3) auf seiner dem Verschlussteil (2) zugewandten Seite mindestens zwei in Längsrichtung hintereinander angeordnete Mischflügel (5, 6) aufweist, die bezüglich der Wandung des Kammerteils (1) nicht materialabstreifend ausgestaltet sind, und die jeweils axial freie Durchlässe (18, 19, 20) aufweisen, wobei in axialer Richtung die Durchlässe (18, 19, 20) eines Mischflügels (5, 6) jeweils durch den nicht freien Teil des anderen Mischflügels (6, 5) abgedeckt sind, und dass am Verschlussteil (2) eine das hintere Ende des Mischelements (3) umgreifende, im wesentlichen in Längsrichtung ausgerichtete innere Hülse (4) angeordnet ist, die sich nahezu bis zum ersten Mischflügel (5) erstreckt.Dynamic mixer, in particular for viscous dental materials, with a chamber part (1), with a discharge opening (13) at the front end of the chamber part (1), with a closure part (2) with inlet openings (11) arranged at the rear end of the chamber part (1) for individual components to be introduced and a central bore for a mixing element (3) which can be rotated about its longitudinal axis in the chamber part (1), characterized in that the mixing element (3) on its side facing the closure part (2) has at least two arranged one behind the other in the longitudinal direction Has mixing blades (5, 6) which are not designed to strip material with respect to the wall of the chamber part (1) and which each have axially free passages (18, 19, 20), the passages (18, 19, 20) in the axial direction a mixing wing (5, 6) are each covered by the non-free part of the other mixing wing (6, 5), and that on the closure part (2) one the rear end of the Misc helements (3) encompassing, essentially longitudinally oriented inner sleeve (4) is arranged, which extends almost to the first mixing wing (5). Dynamischer Mischer nach Anspruch 1, dadurch gekennzeichnet, dass die Mischflügel (5, 6) in ausbringender Längsrichtung anstiegsfrei ausgebildet sind.Dynamic mixer according to claim 1, characterized in that the mixing blades (5, 6) are constructed without a rise in the longitudinal direction in which they are brought out. Dynamischer Mischer nach einem der Ansprüche 1 bis 2, dadurch gekennzeichnet, dass am am hinteren Ende des Kammerteils (1) angeordneten ersten Mischflügel (5) in Richtung Verschlussteil (2) in Längsrichtung derart mindestens ein Mischzapfen (10) angeformt ist, dass das aus den Eintrittsöffnungen (11) eintretende viskose Material zerschneidungsfrei verstrichen wird. Dynamic mixer according to one of Claims 1 to 2, characterized in that at least one mixing spigot (10) is integrally formed on the first mixing wing (5) arranged at the rear end of the chamber part (1) in the direction of the closure part (2) in the longitudinal direction in such a way that the the viscous material entering the inlet openings (11) is passed without cutting. Dynamischer Mischer nach einem der Ansprüche 1 bis 3, dadurch gekennzeichnet, dass am Verschlussteil (2) mindestens ein im wesentlichen in Längsrichtung ausgerichteter innerer Zapfen (12) angeordnet ist.Dynamic mixer according to one of Claims 1 to 3, characterized in that at least one inner pin (12) which is oriented essentially in the longitudinal direction is arranged on the closure part (2). Dynamischer Mischer nach einem der Ansprüche 1 bis 4, dadurch gekennzeichnet, dass der erste Mischflügel (5) in ausbringender Längsrichtung kuppelförmig ausgebildet ist.Dynamic mixer according to one of claims 1 to 4, characterized in that the first mixing blade (5) is dome-shaped in the discharging longitudinal direction. Dynamischer Mischer nach einem der Ansprüche 1 bis 5, dadurch gekennzeichnet, dass der erste Mischflügel (5) innere und/oder äussere Ausnehmungen (18, 19) aufweist.Dynamic mixer according to one of claims 1 to 5, characterized in that the first mixing blade (5) has inner and / or outer recesses (18, 19). Dynamischer Mischer nach einem der Ansprüche 1 bis 6, dadurch gekennzeichnet, dass der zweite Mischflügel (6) äussere Ausnehmungen (20) aufweist.Dynamic mixer according to one of claims 1 to 6, characterized in that the second mixing blade (6) has outer recesses (20). Dynamischer Mischer nach einem der Ansprüche 1 bis 7, dadurch gekennzeichnet, dass der zweite Mischflügel (6) in Längsrichtung des Kammerteils (1) eine Materialverstärkung (21) aufweist.Dynamic mixer according to one of Claims 1 to 7, characterized in that the second mixing blade (6) has a material reinforcement (21) in the longitudinal direction of the chamber part (1). Dynamischer Mischer nach einem der Ansprüche 1 bis 8, dadurch gekennzeichnet, dass das Mischelement (3) in ausbringender Längsrichtung mindestens einen dritten Mischflügel (14, 15, 16, 17) aufweist.Dynamic mixer according to one of Claims 1 to 8, characterized in that the mixing element (3) has at least a third mixing blade (14, 15, 16, 17) in the longitudinal direction in which it is discharged. Dynamischer Mischer nach einem der Ansprüche 1 bis 9, dadurch gekennzeichnet, dass in mindestens einer Eintrittsöffnung (11) mindestens ein quer zur Durchflussrichtung ausgerichtetes stegförmiges Element angeordnet ist.Dynamic mixer according to one of claims 1 to 9, characterized in that at least one web-shaped element oriented transversely to the flow direction is arranged in at least one inlet opening (11). Dynamischer Mischer nach Anspruch 10, dadurch gekennzeichnet, dass das stegförmige Element (22) in Durchflussrichtung oval-, rauten-, ellipsen-, vieleck- oder kreisförmig ist.Dynamic mixer according to claim 10, characterized in that the web-shaped element (22) in the flow direction is oval, diamond, elliptical, polygonal or circular. Verwendung eines dynamischen Mischers nach einem der Ansprüche 1 bis 11 zum Anmischen von viskosen Mehrkomponentenmaterialien, insbesondere von Dentalmaterialien.Use of a dynamic mixer according to one of claims 1 to 11 for mixing of viscous multi-component materials, in particular of dental materials.
EP01106102A 2000-03-29 2001-03-13 Dynamic mixer Expired - Lifetime EP1149627B1 (en)

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DE10015133A DE10015133C1 (en) 2000-03-29 2000-03-29 Dynamic mixer for dental materials has at least two paddles in succession at the mixer on the side towards the chamber closure which do not strip the chamber walls
DE10015133 2000-03-29
DE10043489 2000-09-01
DE10043489A DE10043489A1 (en) 2000-09-01 2000-09-01 Dynamic mixer used for mixing viscous multiple component materials, especially dental material has a mixing element with mixing wings arranged on the side facing the closing part

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ES (1) ES2223666T3 (en)
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EP1510249A1 (en) * 2003-09-01 2005-03-02 GC Corporation Stirring mixer for dental impression material
JP2005512801A (en) * 2001-12-28 2005-05-12 ケッテンバッハ ゲゼルシャフト ミット ベシュレンクテル ハフツング ウント コンパニー コマンディートゲゼルシャフト Apparatus for mixing two pasty materials, in particular for mixing dental impression materials with catalyst materials
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CN101801511B (en) * 2007-09-10 2013-03-27 苏舍米克斯帕克有限公司 Dynamic mixer
WO2013127534A1 (en) * 2012-03-02 2013-09-06 Udo Tartler Device for mixing at least two fluid components, rotary-driven mixer insert therefor, and system of the two
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Cited By (26)

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Publication number Priority date Publication date Assignee Title
US6394643B1 (en) * 1998-10-14 2002-05-28 Kettenbach Gmbh & Co. Kg Device for mixing two pasty materials, especially for mixing a dental impression material with a catalyst material
US6854621B2 (en) 1999-07-29 2005-02-15 Mixpac Systems Ag Cartridge dispenser including drive for dynamic mixer
US6523992B1 (en) * 1999-11-12 2003-02-25 Kettenbach Gmbh & Co. Kg Device for mixing two pasty substances, particularly for mixing a dental impression substance with catalyst substance
US6443612B1 (en) * 1999-12-02 2002-09-03 Wilhelm A. Keller Dynamic mixer
US6932243B2 (en) * 1999-12-02 2005-08-23 Mixpac Systems Ag Dispensing assembly with dynamic mixer
US6540395B2 (en) * 1999-12-23 2003-04-01 Ernst Mühlbauer KG Dynamic mixer for dental impression compounds
US7287898B2 (en) 2001-03-15 2007-10-30 3M Espe Ag Dynamic mixer
US7674033B2 (en) 2001-03-15 2010-03-09 3M Espe Ag Dynamic mixer
JP2005512801A (en) * 2001-12-28 2005-05-12 ケッテンバッハ ゲゼルシャフト ミット ベシュレンクテル ハフツング ウント コンパニー コマンディートゲゼルシャフト Apparatus for mixing two pasty materials, in particular for mixing dental impression materials with catalyst materials
US8147122B2 (en) * 2003-03-06 2012-04-03 Dentsply International Inc. Dispensing and mixing tip for reactive componets
US7320541B2 (en) 2003-08-14 2008-01-22 3M Espe Ag Mixer element for a mixer for multi-component pastes, and mixer using the same
EP1510249A1 (en) * 2003-09-01 2005-03-02 GC Corporation Stirring mixer for dental impression material
US7172338B2 (en) 2003-09-01 2007-02-06 Gc Corporation Stirring mixer for dental impression material
AU2004205312B2 (en) * 2003-09-01 2009-01-29 Gc Corporation Stirring mixer for dental impression material
WO2005099913A1 (en) 2004-04-19 2005-10-27 3M Espe Ag Combination of dynamic mixer and containers
US8322909B2 (en) 2004-09-22 2012-12-04 3M Deutschland Gmbh Mixer for multi-component pastes, kit, and method of mixing paste components
WO2006032467A1 (en) 2004-09-22 2006-03-30 3M Espe Ag Mixer for multi-component pastes, kit, and method of mixing paste components
EP1640060A1 (en) * 2004-09-22 2006-03-29 3M Espe Ag Mixer for multi-component pastes, kit, and method of mixing paste components
CN101060917B (en) * 2004-09-22 2013-02-13 3M德国有限公司 Mixer for multi-component pastes, kit, and method of mixing paste components
US8579497B2 (en) 2006-03-10 2013-11-12 3M Innovative Properties Company Device, mixer and system for mixing and dispensing of a material and method of use
CN101801511B (en) * 2007-09-10 2013-03-27 苏舍米克斯帕克有限公司 Dynamic mixer
US9522366B2 (en) 2011-02-28 2016-12-20 Sulzer Mixpac Ag Dynamic mixer
TWI568492B (en) * 2011-02-28 2017-02-01 素路彩米克斯派克股份有限公司 Dynamic mixer
WO2013026722A1 (en) 2011-08-24 2013-02-28 Kettenbach Gmbh & Co. Kg Mixer
US9463079B2 (en) 2011-08-24 2016-10-11 Kettenbach Gmbh & Co. Kg Mixer
WO2013127534A1 (en) * 2012-03-02 2013-09-06 Udo Tartler Device for mixing at least two fluid components, rotary-driven mixer insert therefor, and system of the two

Also Published As

Publication number Publication date
DK1149627T3 (en) 2004-11-22
PT1149627E (en) 2004-11-30
DE50103064D1 (en) 2004-09-09
ES2223666T3 (en) 2005-03-01
TR200401986T4 (en) 2004-10-21
EP1149627B1 (en) 2004-08-04
ATE272440T1 (en) 2004-08-15
EP1149627A3 (en) 2003-06-04

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