US20040156935A1 - Distribution system for a pastillation machie - Google Patents
Distribution system for a pastillation machie Download PDFInfo
- Publication number
- US20040156935A1 US20040156935A1 US10/764,907 US76490704A US2004156935A1 US 20040156935 A1 US20040156935 A1 US 20040156935A1 US 76490704 A US76490704 A US 76490704A US 2004156935 A1 US2004156935 A1 US 2004156935A1
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- US
- United States
- Prior art keywords
- bar
- diffuser
- distribution system
- distribution
- flowable substance
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 238000009826 distribution Methods 0.000 title claims abstract description 99
- 229910000619 316 stainless steel Inorganic materials 0.000 claims description 2
- 229910000831 Steel Inorganic materials 0.000 claims 1
- 239000010959 steel Substances 0.000 claims 1
- 230000009969 flowable effect Effects 0.000 abstract description 50
- 239000000126 substance Substances 0.000 abstract description 49
- 239000003337 fertilizer Substances 0.000 abstract description 18
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 8
- 239000005864 Sulphur Substances 0.000 abstract description 8
- 239000007788 liquid Substances 0.000 abstract description 7
- 239000000203 mixture Substances 0.000 abstract description 5
- 239000004927 clay Substances 0.000 abstract description 2
- 229910052802 copper Inorganic materials 0.000 abstract description 2
- 229910052742 iron Inorganic materials 0.000 abstract description 2
- 235000021073 macronutrients Nutrition 0.000 abstract description 2
- 229910052748 manganese Inorganic materials 0.000 abstract description 2
- 239000011159 matrix material Substances 0.000 abstract description 2
- 239000011785 micronutrient Substances 0.000 abstract description 2
- 235000013369 micronutrients Nutrition 0.000 abstract description 2
- 230000008961 swelling Effects 0.000 abstract description 2
- 229910052725 zinc Inorganic materials 0.000 abstract description 2
- 235000010603 pastilles Nutrition 0.000 description 14
- 238000004140 cleaning Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 5
- UQMRAFJOBWOFNS-UHFFFAOYSA-N butyl 2-(2,4-dichlorophenoxy)acetate Chemical compound CCCCOC(=O)COC1=CC=C(Cl)C=C1Cl UQMRAFJOBWOFNS-UHFFFAOYSA-N 0.000 description 4
- 238000004891 communication Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 238000005054 agglomeration Methods 0.000 description 3
- 230000002776 aggregation Effects 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 238000003892 spreading Methods 0.000 description 3
- 230000007480 spreading Effects 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 238000012423 maintenance Methods 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 229910001018 Cast iron Inorganic materials 0.000 description 1
- 244000299461 Theobroma cacao Species 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 230000008642 heat stress Effects 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012768 molten material Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/26—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic on endless conveyor belts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
Definitions
- the present invention relates to an improved distribution system for use in a pastillation machine, and more particularly, a distribution system that provides for an essentially even distribution of a flowable substance at the outlet thereof.
- Pastillation machines typically include an inner cylinder that receives a flowable substance from a source.
- An outer cylinder rotates about the inner cylinder and has rows of openings formed therein.
- the flowable substance is delivered under pressure from the inner cylinder, through the rows of openings in the outer cylinder.
- the flowable substance is then dropped onto a moving conveyor device and cooled to form hemispherical pastilles.
- Pastillation machines are particularly useful for forming elemental sulphur and sulpher based fertilizer pastilles.
- a distribution bar for a machine for extruding flowable substances is disclosed in Froeschke, U.S. Pat. No. 4,623,307.
- the distribution bar is located in a groove that is formed in the outer surface of the inner cylinder of the machine.
- the distribution bar has a series of inlet holes that receive the flowable substance from the inner cylinder.
- the flowable substance passes through these inlet holes into an elongated slot that is formed along the length of the distribution bar.
- the slot is located adjacent to the inner wall of the outer cylinder.
- the holes of the distribution bar are placed very close together in an attempt to distribute the flowable substance evenly within the elongated slot of the distribution bar.
- Pastillation machines typically operate at high temperatures in order to keep the hot liquid flowable. At such temperatures, the distribution bar is subjected to heat stress, which may cause the distribution bar to lose its seal with the flowable substance inlet holes. In addition, warping of the distribution bar causes uneven wear, particularly on the surface of the distribution bar that is in constant contact with the rotating outer cylinder. More importantly, the warped distribution bar may score the outer cylinder. The outer cylinder is an expensive component to replace and therefore any unnecessary wear on the outer cylinder is undesirable.
- an improved distribution system for a flowable substance to be formed into pastilles comprises: a bar having a bore extending therethrough, a series of holes located on an inlet surface of the bar, a series of slots located on an outlet surface of the bar, and a diffuser located in the bore of the bar, the diffuser being spaced between the inlet surface and the outlet surface wherein the series of holes is aligned with flowable substance outlets of the pastillation machine.
- a diffuser for a distribution system for use in a pastillation machine.
- the diffuser comprises: an elongate body sized to fit into a bore of the distribution bar, and a centering device coupled to the elongate body for engaging at least one surface of the bore of the distribution bar wherein the centering device maintains the elongate body generally spaced from at least one wall of the bore of a distribution bar of the distribution system.
- a pastillation machine comprising: a first cylinder having a first end and a second end and an outer surface, the first cylinder being supported at the first end and the second end, a cavity formed in the first cylinder, the cavity being in communication with a source of a flowable substance, a slot formed in the outer surface of the first cylinder, the slot being located between the first and the second end, fluid outlets located in the slot, the outlets being in communication with the cavity of the first cylinder, a second cylinder surrounding the first cylinder and being rotatable thereon, the second cylinder having rows of openings therein, a distribution bar sized to fit into the slot and being sandwiched between the inner cylinder and the outer cylinder, the distribution bar having an inlet surface and an outlet surface and a bore extending therethrough, a series of holes located on the inlet surface, the holes being aligned with the fluid outlets of the first cylinder for receiving the flowable substance therefrom, a series of slots
- the distribution system distributes essentially evenly the flowable substance to produce hemispherical pastilles having similar size.
- FIG. 1 is a perspective view of parts of a pastillation machine with an outer cylinder partially cut away;
- FIG. 2 is a perspective bottom view of a portion of the machine of FIG. 1;
- FIG. 3 is an exploded view of portions of the machine of FIG. 1 incorporating a distribution system of the present invention
- FIG. 4 is an isometric view of a portion of the distribution system of FIG. 3;
- FIG. 5 is top view of a portion of the distribution system of FIG. 3;
- FIG. 6 is a side view of a portion of the distribution system of FIG. 3;
- FIG. 7 is a bottom view of a portion of the distribution bar of FIG. 3;
- FIG. 8 is an isometric view of an end piece of the distribution system
- FIG. 9 is an isometric view of the diffuser of FIG. 3;
- FIG. 10 is a cross-sectional view of the machine of FIG. 3.
- Pastillation machines are used to convert hot liquid mixtures such as molten elemental sulphur, for example, into tiny essentially hemispherical, solid pastilles.
- the hot liquid mixture is deposited as droplets onto a moving conveyor and the droplets are subsequently cooled to form solid pastilles.
- Pastilles can be formed from virtually any hot liquid mixture including viscous fluids, semi-solid slurries, molten materials, fertilizers, chocolates, waxes, resins and other flowable industrial products.
- Pastillation machines are also referred to as drop forming or RotoformerTM machines of Sandvik Process Systems.
- a preferred application of pastillation machines is the production of elemental sulphur pastilles and fertilizer pastilles such as those containing elemental sulphur and swelling clay matrix, and macronutrients (N, P, K) and micronutrients (Fe, Cu, Zn, Mn etc.).
- a pastillation machine 20 is generally shown.
- the machine 20 comprises a double cylinder assembly 22 having an inner cylinder 24 that is surrounded by a rotatable outer cylinder 26 .
- the double cylinder assembly 22 is supported at a first end by a first support assembly 30 and at a second end by a second support assembly (not shown).
- First support assembly 30 comprises a strut 32 that extends upwardly from a machine housing 34 .
- a horizontal support 36 joins strut 32 to a bearing housing 38 .
- Bearing housing 38 has a sprocket (not shown) connected thereto that cooperates with a pulley arrangement (not shown).
- a motor 28 typically 5 HP, drives the pulley arrangement.
- the inner cylinder 24 is supported by the bearing housing 38 and extends horizontally therefrom in a cantilevered arrangement. The inner cylinder 24 is stationary and does not rotate.
- the outer cylinder 26 is driven by the motor 28 to rotate about the inner cylinder 24 .
- the outer cylinder 26 is axially slidable onto the inner cylinder 24 from the second end.
- the outer cylinder 26 includes a perforated shell 40 having enlarged end pieces 42 and 44 , that are located at the first and second ends of the shell 40 respectively.
- the enlarged end piece 42 is formed to engage the bearing housing 38 so that the rotation created by motor 28 is transferred to the outer cylinder 26 .
- a spring loaded tension plate supported by a cradle (not shown) is coupled to the second end of the double cylinder assembly 22 .
- Tension plate 48 also includes a second bearing housing 58 . Second bearing housing 58 allows the outer cylinder 26 to rotate about the inner cylinder 24 .
- Tension plate 48 provides a seal at the second end of the double cylinder assembly 22 to prevent any flowable substance from escaping. Tension plate 48 rests on the cradle when it is installed, which provides support to the second end of the double cylinder assembly 22 .
- the pastillation machine further comprises a conveyor device 50 .
- the conveyor device 50 includes a conveyor belt 52 , which is located below the double cylinder assembly 22 .
- the conveyor belt 52 is formed of stainless steel and moves in the direction indicated by arrow 54 .
- a cooling device (not shown) is located downstream of the double cylinder assembly 22 .
- the cooling device is typically comprised of a water jet that sprays the underside of the conveyor belt 52 .
- the conveyor belt 52 is constructed of stainless steel in order to conduct the cooling effect of the water spray, however, the conveyor may be constructed of any material that is highly heat conductive.
- a flowable substance source (not shown) is connected to a pipeline 56 .
- the flowable substance in a preferred embodiment is a liquid sulphur based fertilizer.
- the pipeline 56 is coupled to the inner cylinder 24 and delivers the flowable substance thereto under pressure.
- the flowable substance passes from the inner cylinder through momentarily aligned openings 46 that are formed in rows about the circumference of the perforated shell 40 of the outer cylinder.
- Droplets (not shown) of the flowable substance fall from the outer cylinder 26 once the momentary opening 46 is closed and are deposited onto the moving conveyor belt 52 .
- the droplets subsequently travel past the cooling device to form hemispherical solid pastilles (not shown).
- the inner cylinder 24 is oriented so that a channel 100 , which is formed in the outer surface thereof, is directed downwardly towards the conveyor device 50 .
- the channel 100 of the inner cylinder 24 includes a generally planar base 108 that is surrounded by a ridge 102 having a generally planar surface.
- a series of flowable substance outlets 104 project from the base 108 of the channel 100 .
- Each outlet 104 has a spring located therein, which is biased radially outward. The outlets 104 expel the flowable substance that is fed into the inner cylinder 24 from the flowable substance source.
- Adjacent each outlet 104 is an alternate outlet 106 .
- the alternate outlets 106 function the same way as the outlets 104 , however, in this embodiment, the alternate outlets 106 have been plugged.
- the outer surface of the inner cylinder 24 has a first step 110 and a second step 112 formed therein.
- the second step 112 is slightly larger in size and is located adjacent the first end of the inner cylinder 24 .
- the steps 110 and 112 engage complementing steps formed on the inner surface of the outer cylinder 26 and serve to locate the outer cylinder 26 axially on the inner cylinder 24 .
- a distribution system 60 including a diffuser bar 90 is shown.
- the distribution system 60 is sized to fit into the channel 100 of the inner cylinder 24 .
- the diffuser 90 fits inside the distribution system 60 and the outer cylinder 26 sandwiches the distribution system 60 between itself and the inner cylinder 24 .
- the flowable substance flows out of the outlets 104 , through the distribution system 60 and out of openings 46 of the perforated shell 40 of the outer cylinder 26 .
- Distribution system 60 is comprised of a distribution bar 62 having a bore 68 , that extends therethrough, and a feeder bar 64 .
- the distribution bar 62 and feeder bar 64 are coupled together as shown in FIGS. 4 - 7 .
- the feeder bar 64 is secured to the distribution bar 62 by fasteners 66 .
- the feeder bar 64 is secured to the distribution bar 62 by welding or any other suitable attachment means.
- the construction of the distribution bar 62 and feeder bar 64 of the distribution system 60 provides a tolerance for heat expansion so that warping of the distribution system 60 is kept to a minimum.
- the distribution bar 62 is made of stainless steel. This material is preferred because it provides high corrosion resistance and low thermal expansion. Type 316 stainless steel is preferred, however, any material exhibiting the desired properties could also be used.
- the feeder bar 64 is subject to increased wear due to constant contact with the outer cylinder 26 as it rotates. In order to ensure that the feeder bar 64 wears out and the outer cylinder 26 does not, the feeder bar 64 is made of ductile material.
- the construction of the distribution system 60 allows for replacement of only the feeder bar 64 , once it has been sufficiently worn, rather than the entire distribution system 60 .
- the feeder bar 64 could alternatively be made of carbon steel, cast iron, aluminum or any material that wears faster than outer rotating cylinder 26 .
- the distribution system 60 has an inlet surface 80 and an opposing outlet surface 82 .
- the inlet surface 80 is located on a side of the distribution bar 62 and comprises a series of holes 84 that are spaced along the length thereof.
- the outlet surface 82 is located on an opposing side of the distribution bar 62 and has a series of slots 86 that are spaced along the length thereof.
- the feeder bar 64 has a wear surface 63 that is curved slightly to complement the curvature of the inner wall of the outer cylinder 26 .
- a continuous slot 65 extends along the length of the feeder bar 64 and exposes the series of slots 86 of the distribution bar 62 . Continuous slot 65 is wider than series of slots 86 and provides a reservoir for containing the flowable substance prior to extrusion of the substance through the rows of openings 46 .
- the series of holes 84 and series of slots 86 do not need to be on opposite surfaces of the distribution bar 62 .
- a path between the holes 84 to the slots 86 must be established, however, the actual location of the holes 84 and slots 86 is not important.
- the holes 84 and slots 86 are on opposite surfaces of the distribution bar 62 .
- FIGS. 5 - 7 an end portion of the distribution bar 62 and feeder bar 64 assembly is shown.
- An end piece 70 of the feeder bar 64 is located at the distal end of the feeder bar 64 .
- end pieces 70 are located at opposite ends of the feeder bar 64 and are removable to allow for the diffuser 90 to slide into the distribution bar 62 in order to assemble the distribution system 60 .
- An insert 71 projects from each end piece 70 to plug into an end of bore 68 of the distribution bar 62 .
- the insert 71 helps to secure the end piece 70 in place and additionally provides a seal so that flowable substance does not escape from the ends of the distribution bar 62 .
- Fasteners are located through countersunk apertures 72 for securing the end pieces 70 to the feeder bar 64 .
- distribution bar 62 and feeder bar 64 may be integrated to form a single part.
- diffuser 90 is inserted into the bore 68 of the distribution bar 62 .
- diffuser 90 is comprised of an elongate body 92 having a centering device that comprises multiple tabs 94 . Pairs of tabs 94 extend outwardly from opposing edges 93 of the body 92 at regular intervals along the length thereof. Alternating pairs of tabs 94 are bent at approximately 45 degree angles from the plane of the body 92 in opposing directions so that an alternating pattern is produced. The pairs of tabs 94 serve to secure the body 92 in a generally centered location in the bore 68 .
- the diffuser 90 effects spreading of the flowable substance so that the flowable substance fills the bore 68 of the distribution bar 62 and thus, exits the distribution bar 62 evenly through the series of slots 86 .
- the spreading effect is achieved by the impact of the flowable substance on the body 92 of the diffuser 90 .
- the flowable substance is forced to flow to the edges 93 of the diffuser 90 .
- the flowable substance is essentially evenly distributed along the length of the body 92 as it flows around the edges 93 of the diffuser 90 and out through the series of slots 86 .
- the diffuser 90 is shown in section and the centering effect of the alternating tabs 94 can be seen.
- the diffuser 90 may be of any construction having an elongate body 92 that is generally centered in the bore 68 of the distribution bar 62 . If the inlet holes 84 and outlet slots 86 are not located on opposing surfaces of the distribution bar 62 , the diffuser 90 is oriented so as to present a surface, for spreading the flowable substance, between the holes 84 and slots 86 .
- the diffuser 90 is a rod that is located in the bore 68 .
- the rod may be secured in the bore 68 using tabs 74 in the manner that has been disclosed.
- the diffuser 90 may be comprised of any rod or bar having a non-flat surface. A partially porous surface may also be used. The degree of porousness of the diffuser 90 must be controlled to ensure that the flowable substance does not simply pass through the diffuser 90 from hole 84 straight into a slot 86 . A surface that is too porous will not spread the liquid between the inlet holes 84 and outlet slots 86 , and thus will be ineffective.
- the centering device of the diffuser 90 is a pair of springs that are coupled to the ends of the diffuser 90 .
- the springs are compressed against the inserts 71 , which are plugged into the ends of the distribution bar 62 , in order to maintain the diffuser 90 generally centered within the bore.
- the springs may be coupled to opposing faces or edges of the diffuser 90 and abut the walls of the bore 68 .
- FIG. 10 shows the inner cylinder 24 , outer cylinder 26 and distribution system 60 , which includes the distribution bar 62 , feeder bar 64 and diffuser 90 , in the assembled condition.
- the inner cylinder 24 has an internal cavity 96 that extends along the length thereof.
- the internal cavity 96 is in communication with the flowable substance source via the pipeline 56 .
- the outlets 104 are joined to the internal cavity 96 of the inner cylinder.
- the outlets 104 abut the distribution bar 62 and form a seal therebetween.
- the outer cylinder 26 surrounds the inner cylinder 24 and rotates thereabout so that openings 46 are momentarily aligned with the series of slots 86 of the distribution bar 62 in succession.
- Passages 98 extend along the length of the inner cylinder 24 .
- a heated medium flows through the passages in order to maintain the flowable substance in a melted state.
- Heated mediums that are typically used include steam and hot oil, however, any suitable material may be used.
- the molted fertilizer composition flows under pressure from the source through pipeline 56 to the internal cavity 96 of the inner cylinder 24 .
- the molten fertilizer is forced out of the internal cavity 96 through the outlets 104 .
- the molten fertilizer passes from the outlets 104 into the bore 68 of the distribution bar 62 through holes 84 .
- the molten fertilizer impacts the diffuser 90 and spreads over the length thereof.
- the molten fertilizer flows over the edges 93 of the diffuser 90 so that the molten fertilizer is evenly distributed within the bore 68 of the distribution bar 62 .
- the molten fertilizer then flows out of the slots 86 and fills the feeder slot 65 .
- the void-free molten fertilizer is contained within the feeder slot 65 prior to being extruded through the outer cylinder 26 .
- the molten fertilizer is extruded through the openings 46 .
- the molten fertilizer is formed into droplets as the openings 46 of the outer cylinder 26 rotate past the distribution bar 62 to temporarily halt the flow of molten fertilizer through the outer cylinder 26 .
- The. droplets fall in rows from the outer cylinder 26 onto the moving conveyor belt 52 .
- the conveyor belt 52 moves the droplets past the cooling device, located underneath moving conveyor belt 52 , to form fertilizer pastilles.
- the distribution system 60 is effective in receiving the flowable substance through a series of inlet holes 84 and distributing the flowable substance along the length and width of a distribution bar 62 so that it flows essentially evenly through a series of outlet slots 86 .
- the feeder slot 65 receives the flowable substance from the series of slots 86 and continuously contains a void-free volume of flowable substance under pressure. This void-free volume of flowable substance is then essentially evenly extruded from the openings 46 of the outer cylinder 26 to form pastilles that are generally equal in size.
- the inlet holes 84 and outlet slots 86 are of a size that is sufficient for clustering and agglomeration of the flowable substance to be unlikely and cleaning of the distribution system 60 can be performed with relative ease.
- the distribution system 60 is easily removed from the pastillation machine. First, first tension plate 48 is unscrewed and then the outer cylinder 26 is slid towards the second end of the inner cylinder 24 . This allows the distribution system 60 to be set free. The outer cylinder 26 does not need to be removed entirely, only withdrawn far enough to allow the distribution system 60 to be removed from channel 100 . The end piece 70 is then removed from the distribution system 60 and the diffuser 90 is slid out from the bore 68 . The distribution system 60 may then be cleaned or further disassembled in order to perform other cleaning or maintenance. The distribution system 60 is designed so that cleaning without disassembly or removal of the diffuser bar 90 is also highly effective. Typically, the distribution system 60 is immersed in a hot oil bath for cleaning.
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
- Fertilizers (AREA)
Abstract
In a pastillation machine, an improved distribution system is provided. The distribution system comprises: a distribution bar having a bore extending therethrough, a series of holes located on an inlet surface of the bar, a series of slots located on an outlet surface of the bar, and a diffuser located in the bore of the bar, the diffuser being spaced between the inlet surface and the outlet surface. The series of holes of the distribution system aligns with flowable substance outlets of the pastillation machine. The pastillation machine can be used to form various hot liquid mixtures, including elemental sulphur and sulphur based fertilizers containing clay swelling matrix, and macronutrients (N, P, K) and micronutrients (Fe, Cu, Zn, Mn etc.).
Description
- This application is a divisional of copending and commonly assigned U.S. application Ser. No. 09/995,243, filed Nov. 26, 2001, entitled IMPROVED DISTRIBUTION SYSTEM FOR A PASTILLATION MACHINE.
- The present invention relates to an improved distribution system for use in a pastillation machine, and more particularly, a distribution system that provides for an essentially even distribution of a flowable substance at the outlet thereof.
- Pastillation machines typically include an inner cylinder that receives a flowable substance from a source. An outer cylinder rotates about the inner cylinder and has rows of openings formed therein. The flowable substance is delivered under pressure from the inner cylinder, through the rows of openings in the outer cylinder. The flowable substance is then dropped onto a moving conveyor device and cooled to form hemispherical pastilles. Pastillation machines are particularly useful for forming elemental sulphur and sulpher based fertilizer pastilles.
- A distribution bar for a machine for extruding flowable substances is disclosed in Froeschke, U.S. Pat. No. 4,623,307. The distribution bar is located in a groove that is formed in the outer surface of the inner cylinder of the machine. The distribution bar has a series of inlet holes that receive the flowable substance from the inner cylinder. The flowable substance passes through these inlet holes into an elongated slot that is formed along the length of the distribution bar. The slot is located adjacent to the inner wall of the outer cylinder. The holes of the distribution bar are placed very close together in an attempt to distribute the flowable substance evenly within the elongated slot of the distribution bar.
- Even distribution of the flowable substance is an important consideration, in order for the flowable substance to be forced out through the holes of the outer cylinder evenly and thus, to form pastilles that are similar in size. The many holes in the distribution bar of the prior art are subject to clustering and agglomeration of the flowable substance, which results in product of inferior quality and inconsistent sizing. The holes also require frequent cleaning in order to minimize the clustering and agglomeration of the flowable substance, which results in increased equipment downtime.
- Pastillation machines typically operate at high temperatures in order to keep the hot liquid flowable. At such temperatures, the distribution bar is subjected to heat stress, which may cause the distribution bar to lose its seal with the flowable substance inlet holes. In addition, warping of the distribution bar causes uneven wear, particularly on the surface of the distribution bar that is in constant contact with the rotating outer cylinder. More importantly, the warped distribution bar may score the outer cylinder. The outer cylinder is an expensive component to replace and therefore any unnecessary wear on the outer cylinder is undesirable.
- It is therefore the object of an aspect of the present invention to provide a distribution system that improves the distribution of the flowable substance at an outlet thereof.
- According to one aspect of the present invention there is provided in a pastillation machine, an improved distribution system for a flowable substance to be formed into pastilles. The distribution system comprises: a bar having a bore extending therethrough, a series of holes located on an inlet surface of the bar, a series of slots located on an outlet surface of the bar, and a diffuser located in the bore of the bar, the diffuser being spaced between the inlet surface and the outlet surface wherein the series of holes is aligned with flowable substance outlets of the pastillation machine.
- According to another aspect of the present invention there is provided a diffuser for a distribution system for use in a pastillation machine. The diffuser comprises: an elongate body sized to fit into a bore of the distribution bar, and a centering device coupled to the elongate body for engaging at least one surface of the bore of the distribution bar wherein the centering device maintains the elongate body generally spaced from at least one wall of the bore of a distribution bar of the distribution system.
- According to yet another aspect of the present invention there is provided a pastillation machine. The machine comprises: a first cylinder having a first end and a second end and an outer surface, the first cylinder being supported at the first end and the second end, a cavity formed in the first cylinder, the cavity being in communication with a source of a flowable substance, a slot formed in the outer surface of the first cylinder, the slot being located between the first and the second end, fluid outlets located in the slot, the outlets being in communication with the cavity of the first cylinder, a second cylinder surrounding the first cylinder and being rotatable thereon, the second cylinder having rows of openings therein, a distribution bar sized to fit into the slot and being sandwiched between the inner cylinder and the outer cylinder, the distribution bar having an inlet surface and an outlet surface and a bore extending therethrough, a series of holes located on the inlet surface, the holes being aligned with the fluid outlets of the first cylinder for receiving the flowable substance therefrom, a series of slots located on the outer surface, the series of slots of the distribution bar being in communication with the rows of openings in succession, and a diffuser bar extending axially through the bore of the distribution bar wherein as the openings of the outer cylinder pass over the series of slots of the distribution bar, a predetermined amount of flowable substance passes through the openings and drops onto a moving conveyor located below the pastillation machine.
- It is an advantage of an aspect of the present invention that the distribution system distributes essentially evenly the flowable substance to produce hemispherical pastilles having similar size.
- Embodiments of the present invention will now be described more fully with reference to the accompanying drawings in which:
- FIG. 1 is a perspective view of parts of a pastillation machine with an outer cylinder partially cut away;
- FIG. 2 is a perspective bottom view of a portion of the machine of FIG. 1;
- FIG. 3 is an exploded view of portions of the machine of FIG. 1 incorporating a distribution system of the present invention;
- FIG. 4 is an isometric view of a portion of the distribution system of FIG. 3;
- FIG. 5 is top view of a portion of the distribution system of FIG. 3;
- FIG. 6 is a side view of a portion of the distribution system of FIG. 3;
- FIG. 7 is a bottom view of a portion of the distribution bar of FIG. 3;
- FIG. 8 is an isometric view of an end piece of the distribution system;
- FIG. 9 is an isometric view of the diffuser of FIG. 3;
- FIG. 10 is a cross-sectional view of the machine of FIG. 3.
- Pastillation machines are used to convert hot liquid mixtures such as molten elemental sulphur, for example, into tiny essentially hemispherical, solid pastilles. The hot liquid mixture is deposited as droplets onto a moving conveyor and the droplets are subsequently cooled to form solid pastilles. Pastilles can be formed from virtually any hot liquid mixture including viscous fluids, semi-solid slurries, molten materials, fertilizers, chocolates, waxes, resins and other flowable industrial products. Pastillation machines are also referred to as drop forming or Rotoformer™ machines of Sandvik Process Systems.
- A preferred application of pastillation machines is the production of elemental sulphur pastilles and fertilizer pastilles such as those containing elemental sulphur and swelling clay matrix, and macronutrients (N, P, K) and micronutrients (Fe, Cu, Zn, Mn etc.).
- Referring to FIG. 1, a
pastillation machine 20 is generally shown. Themachine 20 comprises adouble cylinder assembly 22 having aninner cylinder 24 that is surrounded by a rotatableouter cylinder 26. Thedouble cylinder assembly 22 is supported at a first end by afirst support assembly 30 and at a second end by a second support assembly (not shown). -
First support assembly 30 comprises astrut 32 that extends upwardly from amachine housing 34. Ahorizontal support 36 joinsstrut 32 to abearing housing 38. Bearinghousing 38 has a sprocket (not shown) connected thereto that cooperates with a pulley arrangement (not shown). Amotor 28, typically 5 HP, drives the pulley arrangement. Theinner cylinder 24 is supported by thebearing housing 38 and extends horizontally therefrom in a cantilevered arrangement. Theinner cylinder 24 is stationary and does not rotate. - The
outer cylinder 26 is driven by themotor 28 to rotate about theinner cylinder 24. Theouter cylinder 26 is axially slidable onto theinner cylinder 24 from the second end. Theouter cylinder 26 includes aperforated shell 40 having enlargedend pieces shell 40 respectively. Theenlarged end piece 42 is formed to engage the bearinghousing 38 so that the rotation created bymotor 28 is transferred to theouter cylinder 26. - A spring loaded tension plate, supported by a cradle (not shown) is coupled to the second end of the
double cylinder assembly 22.Tension plate 48 also includes asecond bearing housing 58. Second bearinghousing 58 allows theouter cylinder 26 to rotate about theinner cylinder 24.Tension plate 48 provides a seal at the second end of thedouble cylinder assembly 22 to prevent any flowable substance from escaping.Tension plate 48 rests on the cradle when it is installed, which provides support to the second end of thedouble cylinder assembly 22. - The pastillation machine further comprises a
conveyor device 50. Theconveyor device 50 includes aconveyor belt 52, which is located below thedouble cylinder assembly 22. Theconveyor belt 52 is formed of stainless steel and moves in the direction indicated by arrow 54. A cooling device (not shown) is located downstream of thedouble cylinder assembly 22. The cooling device is typically comprised of a water jet that sprays the underside of theconveyor belt 52. Theconveyor belt 52 is constructed of stainless steel in order to conduct the cooling effect of the water spray, however, the conveyor may be constructed of any material that is highly heat conductive. - A flowable substance source (not shown) is connected to a
pipeline 56. The flowable substance in a preferred embodiment is a liquid sulphur based fertilizer. Thepipeline 56 is coupled to theinner cylinder 24 and delivers the flowable substance thereto under pressure. The flowable substance passes from the inner cylinder through momentarily alignedopenings 46 that are formed in rows about the circumference of theperforated shell 40 of the outer cylinder. Droplets (not shown) of the flowable substance fall from theouter cylinder 26 once themomentary opening 46 is closed and are deposited onto the movingconveyor belt 52. The droplets subsequently travel past the cooling device to form hemispherical solid pastilles (not shown). - In the operating condition, the
inner cylinder 24 is oriented so that achannel 100, which is formed in the outer surface thereof, is directed downwardly towards theconveyor device 50. - Referring to FIG. 2, details of the
inner cylinder 24 are shown. Thechannel 100 of theinner cylinder 24 includes a generallyplanar base 108 that is surrounded by aridge 102 having a generally planar surface. A series offlowable substance outlets 104 project from thebase 108 of thechannel 100. Eachoutlet 104 has a spring located therein, which is biased radially outward. Theoutlets 104 expel the flowable substance that is fed into theinner cylinder 24 from the flowable substance source. - Adjacent each
outlet 104 is analternate outlet 106. Thealternate outlets 106 function the same way as theoutlets 104, however, in this embodiment, thealternate outlets 106 have been plugged. - The outer surface of the
inner cylinder 24 has afirst step 110 and asecond step 112 formed therein. Thesecond step 112 is slightly larger in size and is located adjacent the first end of theinner cylinder 24. Thesteps outer cylinder 26 and serve to locate theouter cylinder 26 axially on theinner cylinder 24. - Referring to FIG. 3, a
distribution system 60 including adiffuser bar 90 is shown. Thedistribution system 60 is sized to fit into thechannel 100 of theinner cylinder 24. In the assembled condition, thediffuser 90 fits inside thedistribution system 60 and theouter cylinder 26 sandwiches thedistribution system 60 between itself and theinner cylinder 24. In this arrangement, the flowable substance flows out of theoutlets 104, through thedistribution system 60 and out ofopenings 46 of theperforated shell 40 of theouter cylinder 26. -
Distribution system 60 is comprised of adistribution bar 62 having abore 68, that extends therethrough, and afeeder bar 64. Thedistribution bar 62 andfeeder bar 64 are coupled together as shown in FIGS. 4-7. Thefeeder bar 64 is secured to thedistribution bar 62 byfasteners 66. Alternatively, thefeeder bar 64 is secured to thedistribution bar 62 by welding or any other suitable attachment means. - The construction of the
distribution bar 62 andfeeder bar 64 of thedistribution system 60 provides a tolerance for heat expansion so that warping of thedistribution system 60 is kept to a minimum. Thedistribution bar 62 is made of stainless steel. This material is preferred because it provides high corrosion resistance and low thermal expansion. Type 316 stainless steel is preferred, however, any material exhibiting the desired properties could also be used. - The
feeder bar 64 is subject to increased wear due to constant contact with theouter cylinder 26 as it rotates. In order to ensure that thefeeder bar 64 wears out and theouter cylinder 26 does not, thefeeder bar 64 is made of ductile material. The construction of thedistribution system 60 allows for replacement of only thefeeder bar 64, once it has been sufficiently worn, rather than theentire distribution system 60. Thefeeder bar 64 could alternatively be made of carbon steel, cast iron, aluminum or any material that wears faster than outerrotating cylinder 26. - The
distribution system 60 has aninlet surface 80 and an opposingoutlet surface 82. Theinlet surface 80 is located on a side of thedistribution bar 62 and comprises a series ofholes 84 that are spaced along the length thereof. Theoutlet surface 82 is located on an opposing side of thedistribution bar 62 and has a series ofslots 86 that are spaced along the length thereof. Thefeeder bar 64 has awear surface 63 that is curved slightly to complement the curvature of the inner wall of theouter cylinder 26. Acontinuous slot 65 extends along the length of thefeeder bar 64 and exposes the series ofslots 86 of thedistribution bar 62.Continuous slot 65 is wider than series ofslots 86 and provides a reservoir for containing the flowable substance prior to extrusion of the substance through the rows ofopenings 46. - It will be understood by a person skilled in the art that the series of
holes 84 and series ofslots 86 do not need to be on opposite surfaces of thedistribution bar 62. A path between theholes 84 to theslots 86 must be established, however, the actual location of theholes 84 andslots 86 is not important. In a preferred embodiment, theholes 84 andslots 86 are on opposite surfaces of thedistribution bar 62. - Referring to FIGS.5-7, an end portion of the
distribution bar 62 andfeeder bar 64 assembly is shown. Anend piece 70 of thefeeder bar 64 is located at the distal end of thefeeder bar 64. Referring also to FIGS. 5-7,end pieces 70 are located at opposite ends of thefeeder bar 64 and are removable to allow for thediffuser 90 to slide into thedistribution bar 62 in order to assemble thedistribution system 60. An insert 71 projects from eachend piece 70 to plug into an end ofbore 68 of thedistribution bar 62. Theinsert 71 helps to secure theend piece 70 in place and additionally provides a seal so that flowable substance does not escape from the ends of thedistribution bar 62. Fasteners are located through countersunkapertures 72 for securing theend pieces 70 to thefeeder bar 64. - In an alternate embodiment of the
distribution bar 62 andfeeder bar 64 may be integrated to form a single part. - As indicated by
arrow 74 in FIG. 3, thediffuser 90 is inserted into thebore 68 of thedistribution bar 62. Referring also to FIG. 9,diffuser 90 is comprised of anelongate body 92 having a centering device that comprisesmultiple tabs 94. Pairs oftabs 94 extend outwardly from opposingedges 93 of thebody 92 at regular intervals along the length thereof. Alternating pairs oftabs 94 are bent at approximately 45 degree angles from the plane of thebody 92 in opposing directions so that an alternating pattern is produced. The pairs oftabs 94 serve to secure thebody 92 in a generally centered location in thebore 68. - The
diffuser 90 effects spreading of the flowable substance so that the flowable substance fills thebore 68 of thedistribution bar 62 and thus, exits thedistribution bar 62 evenly through the series ofslots 86. The spreading effect is achieved by the impact of the flowable substance on thebody 92 of thediffuser 90. The flowable substance is forced to flow to theedges 93 of thediffuser 90. Thus, the flowable substance is essentially evenly distributed along the length of thebody 92 as it flows around theedges 93 of thediffuser 90 and out through the series ofslots 86. - Referring to FIG. 10, the
diffuser 90 is shown in section and the centering effect of the alternatingtabs 94 can be seen. Thediffuser 90 may be of any construction having anelongate body 92 that is generally centered in thebore 68 of thedistribution bar 62. If the inlet holes 84 andoutlet slots 86 are not located on opposing surfaces of thedistribution bar 62, thediffuser 90 is oriented so as to present a surface, for spreading the flowable substance, between theholes 84 andslots 86. - In an alternate embodiment, the
diffuser 90 is a rod that is located in thebore 68. The rod may be secured in thebore 68 usingtabs 74 in the manner that has been disclosed. - It will be appreciated by a person skilled in the art that the
diffuser 90 may be comprised of any rod or bar having a non-flat surface. A partially porous surface may also be used. The degree of porousness of thediffuser 90 must be controlled to ensure that the flowable substance does not simply pass through thediffuser 90 fromhole 84 straight into aslot 86. A surface that is too porous will not spread the liquid between the inlet holes 84 andoutlet slots 86, and thus will be ineffective. - In another alternate embodiment, the centering device of the
diffuser 90 is a pair of springs that are coupled to the ends of thediffuser 90. The springs are compressed against theinserts 71, which are plugged into the ends of thedistribution bar 62, in order to maintain thediffuser 90 generally centered within the bore. In a further embodiment, the springs may be coupled to opposing faces or edges of thediffuser 90 and abut the walls of thebore 68. - FIG. 10 shows the
inner cylinder 24,outer cylinder 26 anddistribution system 60, which includes thedistribution bar 62,feeder bar 64 anddiffuser 90, in the assembled condition. Theinner cylinder 24 has aninternal cavity 96 that extends along the length thereof. Theinternal cavity 96 is in communication with the flowable substance source via thepipeline 56. Theoutlets 104 are joined to theinternal cavity 96 of the inner cylinder. Theoutlets 104 abut thedistribution bar 62 and form a seal therebetween. Theouter cylinder 26 surrounds theinner cylinder 24 and rotates thereabout so thatopenings 46 are momentarily aligned with the series ofslots 86 of thedistribution bar 62 in succession. -
Passages 98 extend along the length of theinner cylinder 24. A heated medium flows through the passages in order to maintain the flowable substance in a melted state. Heated mediums that are typically used include steam and hot oil, however, any suitable material may be used. - Now that the apparatus has been described, operation of the apparatus to produce sulphur based fertilizer pastilles will now be described.
- In operation, the molted fertilizer composition flows under pressure from the source through
pipeline 56 to theinternal cavity 96 of theinner cylinder 24. The molten fertilizer is forced out of theinternal cavity 96 through theoutlets 104. The molten fertilizer passes from theoutlets 104 into thebore 68 of thedistribution bar 62 throughholes 84. The molten fertilizer impacts thediffuser 90 and spreads over the length thereof. At the same time, the molten fertilizer flows over theedges 93 of thediffuser 90 so that the molten fertilizer is evenly distributed within thebore 68 of thedistribution bar 62. The molten fertilizer then flows out of theslots 86 and fills thefeeder slot 65. The void-free molten fertilizer is contained within thefeeder slot 65 prior to being extruded through theouter cylinder 26. As theopenings 46 of theouter cylinder 26 align with theslots 86, the molten fertilizer is extruded through theopenings 46. The molten fertilizer is formed into droplets as theopenings 46 of theouter cylinder 26 rotate past thedistribution bar 62 to temporarily halt the flow of molten fertilizer through theouter cylinder 26. The. droplets fall in rows from theouter cylinder 26 onto the movingconveyor belt 52. Theconveyor belt 52 moves the droplets past the cooling device, located underneath movingconveyor belt 52, to form fertilizer pastilles. - The
distribution system 60 is effective in receiving the flowable substance through a series of inlet holes 84 and distributing the flowable substance along the length and width of adistribution bar 62 so that it flows essentially evenly through a series ofoutlet slots 86. Thefeeder slot 65 receives the flowable substance from the series ofslots 86 and continuously contains a void-free volume of flowable substance under pressure. This void-free volume of flowable substance is then essentially evenly extruded from theopenings 46 of theouter cylinder 26 to form pastilles that are generally equal in size. The inlet holes 84 andoutlet slots 86 are of a size that is sufficient for clustering and agglomeration of the flowable substance to be unlikely and cleaning of thedistribution system 60 can be performed with relative ease. - For cleaning and maintenance purposes, the
distribution system 60 is easily removed from the pastillation machine. First,first tension plate 48 is unscrewed and then theouter cylinder 26 is slid towards the second end of theinner cylinder 24. This allows thedistribution system 60 to be set free. Theouter cylinder 26 does not need to be removed entirely, only withdrawn far enough to allow thedistribution system 60 to be removed fromchannel 100. Theend piece 70 is then removed from thedistribution system 60 and thediffuser 90 is slid out from thebore 68. Thedistribution system 60 may then be cleaned or further disassembled in order to perform other cleaning or maintenance. Thedistribution system 60 is designed so that cleaning without disassembly or removal of thediffuser bar 90 is also highly effective. Typically, thedistribution system 60 is immersed in a hot oil bath for cleaning. - Although preferred embodiments of the present invention have been described, those of skill in the art will appreciate that variations and modifications may be made without departing from the spirit and scope thereof as defined by the appended claims.
Claims (7)
1. A diffuser for a distribution system for use in a pastillation machine, said diffuser comprising:
an elongate body sized to fit into a bore of said distribution bar;
a centering device coupled to said elongate body for engaging at least one surface of said bore of said distribution bar; and
wherein said centering device maintains said elongate body generally spaced from at least one wall of said bore of a distribution bar of said distribution system.
2. A diffuser as claimed in claim 1 wherein said centering device maintains said elongate body generally in the center of said bore.
3. A diffuser as claimed in claim 2 wherein said elongate body is a bar.
4. A diffuser as claimed in claim 3 wherein said elongate body is comprised of steel.
5. A diffuser as claimed in claim 4 wherein said elongate body is comprised of type 316 stainless steel.
6. A diffuser as claimed in claim 3 wherein said centering device comprises a series of tabs extending outwardly from opposing edges of said bar.
7. A diffuser as claimed in claim 6 wherein said tabs are formed in pairs along the length of said bar and alternating pairs of said tabs are bent in opposing directions.
Priority Applications (1)
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US10/764,907 US20040156935A1 (en) | 2001-11-26 | 2004-01-26 | Distribution system for a pastillation machie |
Applications Claiming Priority (2)
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US09/995,243 US6716015B2 (en) | 2001-11-26 | 2001-11-26 | Distribution system for a pastillation machine |
US10/764,907 US20040156935A1 (en) | 2001-11-26 | 2004-01-26 | Distribution system for a pastillation machie |
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US09/995,243 Division US6716015B2 (en) | 2001-11-26 | 2001-11-26 | Distribution system for a pastillation machine |
Publications (1)
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US20040156935A1 true US20040156935A1 (en) | 2004-08-12 |
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US09/995,243 Expired - Lifetime US6716015B2 (en) | 2001-11-26 | 2001-11-26 | Distribution system for a pastillation machine |
US10/764,907 Abandoned US20040156935A1 (en) | 2001-11-26 | 2004-01-26 | Distribution system for a pastillation machie |
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US09/995,243 Expired - Lifetime US6716015B2 (en) | 2001-11-26 | 2001-11-26 | Distribution system for a pastillation machine |
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US20100242556A1 (en) * | 2009-03-31 | 2010-09-30 | Smith Michael R | Pastillation of Ammonium Sulfate Nitrate |
DE102010032021A1 (en) * | 2010-07-16 | 2012-01-19 | Sandvik Materials Technology Deutschland Gmbh | Process for producing particles containing ammonium nitrate |
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DE10138333C2 (en) * | 2001-07-27 | 2003-08-28 | Santrade Ltd | Device for squeezing flowable substances |
US6716015B2 (en) * | 2001-11-26 | 2004-04-06 | Enersul, Inc. | Distribution system for a pastillation machine |
DE102007061408A1 (en) * | 2007-12-11 | 2009-06-18 | Sandvik Materials Technology Deutschland Gmbh | Method and drop former for producing pastilles and method for producing a sulfur-containing fertilizer |
EP2305371A1 (en) | 2009-09-10 | 2011-04-06 | Stamicarbon B.V. | Process for producing granules |
US8476219B2 (en) * | 2009-11-05 | 2013-07-02 | The Procter & Gamble Company | Laundry scent additive |
DE102015212353B3 (en) * | 2015-07-01 | 2016-07-07 | Sandvik Materials Technology Deutschland Gmbh | Apparatus and method for dripping a flowable product |
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US8268279B2 (en) * | 2009-03-31 | 2012-09-18 | Honeywell International Inc. | Pastillation of ammonium sulfate nitrate |
WO2010117751A3 (en) * | 2009-03-31 | 2011-03-03 | Uop Llc | Pastillation of ammonium sulfate nitrate |
US7985393B2 (en) * | 2009-03-31 | 2011-07-26 | Uop Llc | Pastillation of ammonium sulfate nitrate |
US20110277522A1 (en) * | 2009-03-31 | 2011-11-17 | Honeywell International Inc. | Pastillation of ammonium sulfate nitrate |
CN102448911A (en) * | 2009-03-31 | 2012-05-09 | 环球油品有限责任公司 | Pastillation of ammonium sulfate nitrate |
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JP2012521959A (en) * | 2009-03-31 | 2012-09-20 | ハネウェル・インターナショナル・インコーポレーテッド | Tableting ammonium sulfate |
AU2010234908B2 (en) * | 2009-03-31 | 2014-06-26 | Advansix Resins & Chemicals Llc | Pastillation of ammonium sulfate nitrate |
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DE102010032021B4 (en) * | 2010-07-16 | 2016-09-29 | Sandvik Materials Technology Deutschland Gmbh | Process for producing particles containing ammonium nitrate |
Also Published As
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US6716015B2 (en) | 2004-04-06 |
US20030099733A1 (en) | 2003-05-29 |
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