US20140044857A1 - Method for Preparing Water-Soluble Tobacco Flavor in Gel State - Google Patents
Method for Preparing Water-Soluble Tobacco Flavor in Gel State Download PDFInfo
- Publication number
- US20140044857A1 US20140044857A1 US14/002,539 US201114002539A US2014044857A1 US 20140044857 A1 US20140044857 A1 US 20140044857A1 US 201114002539 A US201114002539 A US 201114002539A US 2014044857 A1 US2014044857 A1 US 2014044857A1
- Authority
- US
- United States
- Prior art keywords
- tobacco flavor
- temperature
- gel state
- mixing
- uniform
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/002—Cigars; Cigarettes with additives, e.g. for flavouring
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/281—Treatment of tobacco products or tobacco substitutes by chemical substances the action of the chemical substances being delayed
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Landscapes
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
A method for preparing water-soluble tobacco flavor in gel state is disclosed. The method includes the following steps: mixing food thickener with glycerol in a mass ratio of 1:50 to 1:5 and mixing to uniform, heating to a temperature of 80° C. to 100 ° C. and keep stirring till dissolve thoroughly, homogenizing for 5 to 15 minutes, cooling to a temperature of 30° C. to 50° C., adding water-soluble tobacco flavor and mixing to uniform, and placing at least 12 hours at a temperature of 1° C. to 30 ° C. to obtain a final product. The product obtained by the method can greatly inhibit volatilization of the tobacco flavor, maintain fragrance completely, reduce the loss caused by volatile components, and can be easily transported and stored.
Description
- The present invention relates to the field of tobacco flavor, and more particularly to a method for making water-soluble tobacco flavor into gel state.
- Fragrance type and fragrance style of tobacco flavor determines, in a sense, the quality and taste of cigarette. Usually in the cigarette burning process, some organics with spicy taste will be generated. If some flavor is added into the cigarette, the spicy taste produced in the cigarette burning process will be concealed. Currently used tobacco flavor is mostly a direct extract in form of liquid, extractum or essential oil, which easily leads to the volatilization loss of fragrance.
- In the cigarette manufacturing process, in order to improve the fragrance of cigarette, it's necessary to add tobacco flavor into cigarette raw materials artificially. A current method for adding flavor is to spray tobacco flavoring essence, which is dissolved in some solvents such as water, ethanol, glycerol, propylene glycol, etc., onto the cigarette raw materials. The disadvantage of such method is that some tobacco flavor with bad solubility cannot be uniformly dissolved in the solvent; therefore the tobacco flavor cannot be sprayed and added to the cigarette raw materials uniformly. Furthermore, since the tobacco flavor is liquid, the loss or change of fragrance is easily to be caused by volatilization. Atomized liquid for electronic cigarette is usually a liquid, so it is also easy to cause volatilization loss of fragrance. In current related technologies, there is few report on preparing tobacco flavor into gel state.
- Based on the above, it is an object of the present invention to overcome the drawbacks of the prior technologies by providing a method for making water-soluble tobacco flavor into gel state, which can significantly improve fragrance retention of the tobacco flavor, and greatly reduce volatilization loss.
- According to one aspect of the invention, a method for preparing a water-soluble tobacco flavor in gel state includes: mixing food thickener with glycerol in a mass ratio of 1:50 to 1:5, mixing to uniform, heating to a temperature of 80° C. to 100° C. and keep stirring till dissolve thoroughly, homogenizing for 5 to 15 minutes, cooling to a temperature of 30° C. to 50° C., then adding water-soluble tobacco flavor, mixing to uniform, and placing at least 12 hours at a temperature of Ito 30° C. to obtain final product.
- Preferably, the food thickener is sodium polyacrylate.
- The significant advantages of preparing water-soluble tobacco flavor into gel state are as follows:
- (1) The water-soluble tobacco flavor is prepared into gel state in the present invention, which makes its use be easier and its package, shipping and store be more flexible.
- (2) The water-soluble tobacco flavor is prepared into gel state in the present invention, which greatly improves the heat resistance, light resistance and oxygen resistance abilities of the tobacco flavor, and therefore avoids discoloration and fragrance change caused by outside influences like direct light, heat, etc.
- (3) The water-soluble tobacco flavor is prepared into gel state in the present invention, which greatly inhibits the volatilization of the tobacco flavor, completely preserves the fragrance, and reduces the loss caused by some volatile components.
- (4) The water-soluble tobacco flavor is prepared into gel state in the present invention, which improves the quality of the product, and increases the fragrance retention.
- (5) The water-soluble tobacco flavor is prepared into gel state in the present invention, therefore the prepared product does not include water, and can be kept at a low temperature of −20° C. without freezing.
- (6) The present invention can be carried out with low cost, can easily obtain raw materials and relatively simple production process which is convenient to be actually implemented.
- In addition, sodium polyacrylate can be dissolved in glycerol to form a very viscous and transparent liquid, of which the viscosity is due to ionic phenomenons of many anionic groups making molecular chain increase, and making apparent viscosity increase, so as to produce a high viscous solution, which, when stored for a long time, has a viscosity minimally changing over time.
- 85 g glycerol and 5 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 80° C. to dissolve thoroughly, homogenized for 5 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 30° C., then added 10 g strawberry flavor, stirred uniformly, and placed or 13 hours in a circumstance with a temperature of 18° C. to obtain a final product.
- 25 g glycerol and 5 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 90° C. to dissolve thoroughly, and homogenized for 5 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 40° C., then added 10 g strawberry flavor, stirred uniformly, and placed for 18 hours in a circumstance with a temperature of 18° C. to obtain a final product.
- 250 g glycerol and 5 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 100° C. to dissolve thoroughly, and homogenized for 5 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 50° C., then added 10 g strawberry flavor, stirred uniformly, and placed for 24 hours in a circumstance with a temperature of 18° C. to obtain a final product.
- 40 g glycerol and 8 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 90° C. to dissolve thoroughly, and homogenized for 10 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 30° C., then added 15 g lemon flavor, stirred uniformly, and placed for 13 hours in a circumstance with a temperature of 15° C. to obtain a final product.
- 80 g glycerol and 8 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 80° C. to dissolve thoroughly, and homogenized for 10 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 35° C., then added 15 g lemon flavor, stirred uniformly, and placed for 18 hours in a circumstance with a temperature of 15° C. to obtain a final product.
- 400 g glycerol and 8 g sodium polyacrylate were mixed and stirred uniformly, heated to a temperature of 100° C. to dissolve thoroughly, and homogenized for 10 minutes to make the system more uniform. The mixture was stirred and at the same time cooled to a temperature of 50° C., then added 15 g lemon flavor, stirred uniformly, and placed for 24 hours in a circumstance with a temperature of 15° C. to obtain a final product.
Claims (2)
1. A method for preparing a water-soluble tobacco flavor in gel state, comprising:
mixing food thickener with glycerol in a mass ratio of 1:50 to 1:5 and mixing to uniform,
heating to a temperature of 80° C. to 100 ° C. and keep stirring till dissolve thoroughly,
homogenizing for 5 to 15 minutes,
cooling to a temperature of 30° C. to 50° C.,
adding water-soluble tobacco flavor and mixing to uniform, and
placing at least 12 hours at a temperature of 1° C. to 30° C. to obtain a final product.
2. The method of claim 1 , wherein the food thickener is sodium polyacrylate.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/CN2011/071440 WO2012116491A1 (en) | 2011-03-02 | 2011-03-02 | Method for preparing gel-state water soluble flavoring essence used for cigarette |
Publications (1)
Publication Number | Publication Date |
---|---|
US20140044857A1 true US20140044857A1 (en) | 2014-02-13 |
Family
ID=46757351
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US14/002,539 Abandoned US20140044857A1 (en) | 2011-03-02 | 2011-03-02 | Method for Preparing Water-Soluble Tobacco Flavor in Gel State |
Country Status (3)
Country | Link |
---|---|
US (1) | US20140044857A1 (en) |
EP (1) | EP2682006A4 (en) |
WO (1) | WO2012116491A1 (en) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9095175B2 (en) | 2010-05-15 | 2015-08-04 | R. J. Reynolds Tobacco Company | Data logging personal vaporizing inhaler |
US9259035B2 (en) | 2010-05-15 | 2016-02-16 | R. J. Reynolds Tobacco Company | Solderless personal vaporizing inhaler |
US9352288B2 (en) | 2010-05-15 | 2016-05-31 | Rai Strategic Holdings, Inc. | Vaporizer assembly and cartridge |
US9743691B2 (en) | 2010-05-15 | 2017-08-29 | Rai Strategic Holdings, Inc. | Vaporizer configuration, control, and reporting |
US9999250B2 (en) | 2010-05-15 | 2018-06-19 | Rai Strategic Holdings, Inc. | Vaporizer related systems, methods, and apparatus |
US10092713B2 (en) | 2010-05-15 | 2018-10-09 | Rai Strategic Holdings, Inc. | Personal vaporizing inhaler with translucent window |
US10136672B2 (en) | 2010-05-15 | 2018-11-27 | Rai Strategic Holdings, Inc. | Solderless directly written heating elements |
US10159278B2 (en) | 2010-05-15 | 2018-12-25 | Rai Strategic Holdings, Inc. | Assembly directed airflow |
CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
JP2022179818A (en) * | 2021-05-22 | 2022-12-05 | 翰林 李 | Manufacturing method of non-combustible granule |
Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103054177B (en) * | 2013-01-22 | 2015-03-04 | 深圳市凯神科技股份有限公司 | Preparation method of plant extract reducing hazardous substances in cigarettes |
CN103932381B (en) * | 2014-05-04 | 2015-12-02 | 广东中烟工业有限责任公司 | A kind of relieve sore throat cigarette enriching mouth-taste |
CN107772531B (en) * | 2017-10-20 | 2020-11-06 | 武汉力诚生物科技有限公司 | Manufacturing process and equipment of plant polysaccharide-based aerogel cigarette filter tip |
CN109135923A (en) * | 2018-07-27 | 2019-01-04 | 内蒙古昆明卷烟有限责任公司 | The milk sweet tea type essence of cigarette tipping paper cordyceps sinensis feature and its application and preparation method |
CN109055008A (en) * | 2018-07-27 | 2018-12-21 | 内蒙古昆明卷烟有限责任公司 | Cigarette connects the milk sweet tea type essence and its application and preparation method of mouth glue cordyceps sinensis feature |
CN109280579A (en) * | 2018-07-27 | 2019-01-29 | 内蒙古昆明卷烟有限责任公司 | The milk sweet tea type essence of cigarette overlapping glue cordyceps sinensis feature and its application and preparation method |
CN109770421B (en) * | 2019-03-26 | 2021-08-06 | 云南氪莱铂科技有限公司 | Flavoring slow-release gel particles for cigarette filter stick, preparation and application thereof |
CN109852476A (en) * | 2019-04-12 | 2019-06-07 | 薪火高科(深圳)有限公司 | A kind of essence for the smoking article that do not burn suitable for low temperature, preparation method and application |
CN112795428A (en) * | 2021-02-02 | 2021-05-14 | 河北中烟工业有限责任公司 | Lotus-fragrance-style tobacco essence and preparation method and application thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1991006288A1 (en) * | 1989-11-07 | 1991-05-16 | Anders Dam | A nicotine containing stimulant unit |
US20060153949A1 (en) * | 2005-01-11 | 2006-07-13 | Cadbury Adams Usa Llc. | Edible compositions containing swellable polymers |
US20090133703A1 (en) * | 2003-11-07 | 2009-05-28 | Strickland James A | Tobacco compositions |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2224167A (en) * | 1937-12-09 | 1940-12-10 | Standard Brands Inc | Method of preparing gelating product |
US5240016A (en) * | 1991-04-19 | 1993-08-31 | Philip Morris Incorporated | Thermally releasable gel-based flavor source for smoking articles |
ITMI20081450A1 (en) * | 2008-08-04 | 2010-02-05 | Biofarmitalia Spa | SOLID RAPID DISSOLUTION FILM IN LIQUIDS |
CN101633864B (en) * | 2009-07-07 | 2013-01-30 | 广东中烟工业有限责任公司 | Apple-flavored essence for tobacco, preparation method and application thereof |
CN101766332B (en) * | 2009-12-31 | 2011-07-27 | 云南烟草科学研究院 | Pills capable of adding fragrance to cigarettes |
-
2011
- 2011-03-02 WO PCT/CN2011/071440 patent/WO2012116491A1/en active Application Filing
- 2011-03-02 EP EP11859948.9A patent/EP2682006A4/en not_active Withdrawn
- 2011-03-02 US US14/002,539 patent/US20140044857A1/en not_active Abandoned
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1991006288A1 (en) * | 1989-11-07 | 1991-05-16 | Anders Dam | A nicotine containing stimulant unit |
US20090133703A1 (en) * | 2003-11-07 | 2009-05-28 | Strickland James A | Tobacco compositions |
US20060153949A1 (en) * | 2005-01-11 | 2006-07-13 | Cadbury Adams Usa Llc. | Edible compositions containing swellable polymers |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US9095175B2 (en) | 2010-05-15 | 2015-08-04 | R. J. Reynolds Tobacco Company | Data logging personal vaporizing inhaler |
US9259035B2 (en) | 2010-05-15 | 2016-02-16 | R. J. Reynolds Tobacco Company | Solderless personal vaporizing inhaler |
US9352288B2 (en) | 2010-05-15 | 2016-05-31 | Rai Strategic Holdings, Inc. | Vaporizer assembly and cartridge |
US9427711B2 (en) | 2010-05-15 | 2016-08-30 | Rai Strategic Holdings, Inc. | Distal end inserted personal vaporizing inhaler cartridge |
US9555203B2 (en) | 2010-05-15 | 2017-01-31 | Rai Strategic Holdings, Inc. | Personal vaporizing inhaler assembly |
US9743691B2 (en) | 2010-05-15 | 2017-08-29 | Rai Strategic Holdings, Inc. | Vaporizer configuration, control, and reporting |
US9861773B2 (en) | 2010-05-15 | 2018-01-09 | Rai Strategic Holdings, Inc. | Communication between personal vaporizing inhaler assemblies |
US9861772B2 (en) | 2010-05-15 | 2018-01-09 | Rai Strategic Holdings, Inc. | Personal vaporizing inhaler cartridge |
US9999250B2 (en) | 2010-05-15 | 2018-06-19 | Rai Strategic Holdings, Inc. | Vaporizer related systems, methods, and apparatus |
US10092713B2 (en) | 2010-05-15 | 2018-10-09 | Rai Strategic Holdings, Inc. | Personal vaporizing inhaler with translucent window |
US10136672B2 (en) | 2010-05-15 | 2018-11-27 | Rai Strategic Holdings, Inc. | Solderless directly written heating elements |
US10159278B2 (en) | 2010-05-15 | 2018-12-25 | Rai Strategic Holdings, Inc. | Assembly directed airflow |
CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
JP2022179818A (en) * | 2021-05-22 | 2022-12-05 | 翰林 李 | Manufacturing method of non-combustible granule |
JP7307968B2 (en) | 2021-05-22 | 2023-07-13 | 翰林 李 | Method for producing non-combustible granules |
Also Published As
Publication number | Publication date |
---|---|
WO2012116491A1 (en) | 2012-09-07 |
EP2682006A1 (en) | 2014-01-08 |
EP2682006A4 (en) | 2014-11-05 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
AS | Assignment |
Owner name: FEELLIFE BIOSCIENCE INTERNATIONAL CO., LTD., CHINA Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:HUA, JIAN;CHANG, XINGHUI;REEL/FRAME:031490/0766 Effective date: 20131012 |
|
STCB | Information on status: application discontinuation |
Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION |