US2786025A - Sewage digestion process - Google Patents

Sewage digestion process Download PDF

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US2786025A
US2786025A US36028453A US2786025A US 2786025 A US2786025 A US 2786025A US 36028453 A US36028453 A US 36028453A US 2786025 A US2786025 A US 2786025A
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sludge
tank
gas
concentration
digester
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Miles A Lamb
Joseph J Klein
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Chicago Pump Co
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Chicago Pump Co
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/08Aerobic processes using moving contact bodies
    • C02F3/085Fluidized beds
    • C02F3/087Floating beds with contact bodies having a lower density than water
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/24Treatment of water, waste water, or sewage by flotation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/1205Particular type of activated sludge processes
    • C02F3/1221Particular type of activated sludge processes comprising treatment of the recirculated sludge
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/28Anaerobic digestion processes
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/30Aerobic and anaerobic processes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/30Fuel from waste, e.g. synthetic alcohol or diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/10Biological treatment of water, waste water, or sewage
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S210/00Liquid purification or separation
    • Y10S210/09Floating cover

Definitions

  • the invention relates to a process for the concentration of raw sludge in a sewage disposal system, and more particularly relates to a process of concentration of raw sewage sludge by flotation of the sludge.
  • Prior concentration by flotation processes have required the addition of various chemicals, or application of heat for a relatively long time. These prior processes do not use to advantage the products of the sewage disposal process itself in the concentration process to effect a more etlicient sewage disposal installation as in the case of the present invention to be hereinafter described.
  • digester gas gas produced in the digestion process
  • digester or methanecontaining gas itself promotes bacterial growth in the sludge undergoing concentration which further materially accelerates and promotes the flotation of the solid sludge particles in the sludge mixture undergoing concentration. lf the gas is introduced into the sludge mixture at too high a rate, excessive motion of the mixture will result which will materially hinder or prevent concentration of the solid particles on the top of the sludge mixture. The digester gas must therefore be gently circulated through the contents of the concentration tank to avoid agitation of the sludge.
  • the rate of introduction of digester gas into the mixture undergoing concentration should not exceed a maximum rate of 1/10 of a cubic foot per minute per foot of maximum horizontal internal cross-sectional dimension of a tank housing the sludge, where the tank has a substantially constant cross section. All of the solid sludge particles will then float to the top of the sludge mixture in a short time, relative to that required by existing commercial processes, leaving a clarified subnatant below.
  • the period of time re- ⁇ quired for complete concentration of raw sewage is further shortened by purposely seeding the sludge to be concentrated with activated or digested sludge.
  • the quantity of seed sludge to be incorporated in the raw sludge to be concentrated should preferably be from 2 to 20% of the raw sludge volume to which it is added.
  • the process of gas circulation above described has reduced the time necessary for complete concentration to as short a period as one day. This has resulted in a substantial reduction of the size and cost of a sewage disposal installation capable of handling a given volume of sewage since the volume of sludge fed to the digestion facilities 'for a given amount 0f sewage inuent to the entire system can be reduced by as much as 50% and the volume of the digestion apparatus needed for the relatively time consuming digestion process is reduced in the same amount as the reduction of raw sludge volume by concentration.
  • the present invention accomplishes this end by utilizing the products of digestion, such as digester gas and digested sludge, to carry out the concentration process to effect an inexpensive and eiicient operation.
  • Figure l illustrates a sewage treating system embodying the present invention, the parts being shown diagrammatically and in section;
  • Figure 2 is a plan view of the diffusing device in the concentration tank shown in Figure l.
  • the numeral 10 indicates a conduit through which the raw sewage from the sewage system of a small city, amounting to, say, about one million gallons per day, is discharged into the primary settling tank Il. in general, this raw sewage will have been preliminarily subjected to treatment in the customary comminuting and screening devices to break up and/ or remove large foreign objects and may also have been passed through a conventional sedimentation tank. These devices being conventional and in common use, are not shown.
  • the primary settling tank which is of sucient capacity to insure an adequate residence time to permit sedimentation of the sludge, is provided with the usual slow moving sludge collector, diagrammatically illustrated and designated by the numeral 12, and with a sump 13 for the collection of the sludge.
  • the amount of sludge collected daily in the tank 11 may be, for example,
  • the sewage eflluent after removal of the primary sludge, may be further treated for removal of additional sludge or may be disposed of in any suitable manner, as by dilution, by means of tiickling filters, or by other suitable means. As illustrated, it may be subjected to aeration, to eect the flocculation of additional sludge,
  • Patented Mar. 19, 1957 o which i s then permitted to settle and is preferably added to the sludge collected in the primary settling tank.
  • the eliiuent from the primary settling tank may pass through aconduit 14 to the aeration tank I5, through which the sewage travels slowly while air is forced into and through the sewage by means of the Vdiffusers 16, which are diagrammatically illustrated.
  • These ditusers may b e of any suitable type, for example, such as that shown in the United States patents to Lannert, No. 2,328,655, granted September 7, 1943, and Nordell, No. 2,555,201, granted December 5, 1950, or in the copending application of Lamb, Serial No. 206,237, tiled January 16, 1951, and Klein, Serial No. 246,854, tiled September 15, 1951.
  • the aerated sewage leaving the tank 15 passes through a conduit 17 into the iinal settling tank 13, which is of such capacity that the sewage moves slowly through it, permitting settling of the flocculated sludge.
  • This tank - is likewise provided with the usual slow moving sludge collector, illustrated diagrammatically and designated by the number 19'.
  • the sludge is collected in a sump 20.
  • the sludge collected in the sump 20 is withdrawn through pipe 21 by pump 22, which discharges it vthrough the pipe 23 into the primary settling tank 11, where it settles and collects in the sump 13 ⁇ in admixture with the primary sludge.
  • a part of the sludge collecte-d in settling tank 1S may be returned through the line -24 to the conduit 114 and the aeration tank 15.
  • the treated sewage efliuent from the settling tank 18 passes out through the cftiuent conduit 24 for disposal in the usual manner, such as filter beds, or may be handled in any-other desired manner.
  • the sewage effluent leaving the primary settling tank 11 may be disposed of in any other suitable manner; for example, by filtration or, where permissible, by stream dilution.
  • the sludge collected in primary settling tank 11 will consist entirely of primary or raw sludge, or of such sludge admixed with any ripe sludge that may be deposited from supernatant liquor from the anaerobic digestion of the sludge that may be Vreturned as hereinafter described.
  • the sludge collected in tank 11 is withdrawn from sump 13 through line 26 by pump 27 and discharged through line 28 into the aeration and mixing tank 29. While the withdrawal of the primary sludge from the tank 1'1 may be continuous, in ordinary operation, it is generally preferred that it be intermittent. Usually such withdrawal is effected about three times a day, about one-third of the total of the sludge collected per day being removed from tank 1i each time.
  • the amount of sludge removed from tank 11 at each time of such removal will, considering normal variations, be in the order of 3,000 to 3,500 gallons.
  • the capacity of the aerating and mixing tank 29 may have an effective'v volume equal to or greater than the raw sludge pump capacity per minute.
  • the sludge is aerated to a certain extent, preferably using air diifusers, of which one is illustrated at 30, these being the same or of the same character as the air diusers in the aeration tank 15 previously referred to.
  • the amount of air used is in the range of to 100% by volume on the sludge, preferably about,75%. Thus with the amount of sludge being handled per pumping period of about 3,500 gallons, the.
  • the amount of airV introduced would be in the range from 115 to- 470 cubic feet and preferably about 350 cubic feet.
  • the time of re'- tention of. the sludge in the aerating and mixing tank may. be from l ⁇ to 5 minutes.
  • the mixing of the air with the raw sludge may be carried out at any normal operating temperature above the freezing point,V say in the range of from 32 F. to 90 F.
  • the air utilized should be at a temperature of not less than 30 F. and its temperature may be higher, say up to 150 ii., and may contribute to maintaining the in the aeration tank 29 above freezing temperature during cold weather.
  • an adsorptive material is thoroughly admixed with the sewage sludge and suspended therein.
  • Preferably finely divided coke is employed, the coke being ground sufficiently finely so that the greater portion thereof, say will pass through a 200 mesh sieve and all of it wilt' pass through a 75 mesh sieve.
  • the powdered coke may be introduced into the aerating and mixing tank 29 in any suitable manner, for example, from the hopper 31. When introduced in the latter stages of the aeration process, the introduction of the air effects the desired admixture of the coke with the sludge. Supplementary mechanical mixing devices may be employed, if desired.
  • tlie powdered coke may also be admixed with the sludge promptly after its aeration or in its flow from the aeration and mixing tank 29 to the concentration tank hereinafter referred to, any suitable mixing means being employed.
  • the aeration of the raw sewage and addition of an adsorptive material, if utilized, should preferably precede rather than follow the concentration process to be described.
  • Other adsorptive materials may be employed instead of powdered coke, such as lfullers earth, silica gel, diatomaceous earth or the like. Coke is, however, preferred.
  • the proportion of finely dividedv adsorptiveV material, such as coke, that is added is suitably inthe order of ⁇ 0.5 to 2.5 parts per parts of sludge, Yby weight, and preferably, in the case of coke, is about 1- part per 100 parts of sludge by weight.
  • the primary operation to 'oe performedv in the digestion process of the present invention is one. of anaerobic digestion which does not require the presence of oxygen to effect digestion.
  • the sludge is ⁇ introduced into the concentration tank 32.
  • the sludge may suitably bewithdrawn from the aeration and mixing tank 29 through line 33 by pump 34.
  • the raw sludge entering concentration tank 32 is heated in a suitable heater 34 which may, for example, be similar to the heater. disclosed in copending application Serial No. 290,848, on ⁇ a Method and Apparatus for Treating Sewage Sludge, filedr May ⁇ 3l, 1952, by Milton Spiegel and MilesH. Lamb.
  • the temperature to which the raw sludge is ⁇ heated is not critical, but the sludge is preferably heated to a temperature of from 80 to 100 F.
  • the concentration tank 32 should'. beinsulated to prevent. the escape of heat therefrom.
  • the sludgel enteringthe concentration tank may, for example, consist of? from about 3 to 8% by weight of solids out-of which 40% to 70% may bevolatile solids.
  • sludge concentration tank 32 isrcorncentrated bybeing floated to the surface of the mixture therein in amanner to be described.
  • a relatively clarified liquor (subnantant) forms in the bottom of concentration tank 32 as a result of the concentration process, which is drawn off from the lower level of the concentration tank through one or more withdrawal pipes indicated generally by numeral 36.
  • the subnatant may then be discharged into primary settling tank l1 as by pump 39 via lines 38 and 37.
  • the concentrated sludge tloating in the upper portion of concentration tank 32 may be suitably withdrawn from this tank through line 40 by pump 41 and discharged through line 42 to a digester tank 43.
  • This concentrated sludge may include as much as 8% to 12% solids by weight.
  • Concentration tank 32 is preferably of square or circular cross section and includes a cover 32' of the tixed or floating variety, a fixed one being shown, to isolate the contents therein from the atmosphere.
  • the raw sludge is concentrated in concentration tank 32 as by digester gas fed from a digester tank, such as tank 43, by means of a blower 44 from a gas draw-ott line 45 communicating with the gas collecting dome 45 of digester tank 43.
  • the gas passes through line 48 and through a gas ditusing device 47, similar to difiusers 16, located preferably near the bottom and center of the concentration tank 32.
  • the dilfusing device 47 should produce a slowly rising column of gas extendingover a considerable area. This slowly rising column of gas should not agitate the sewage sludge or impart thereto a circulatory movement.
  • Diffusing device 47 preferably would include a series of diffusing elements or tubes arranged near the center of the bottom of concentration tank 32.
  • Figure 2 shows an exemplary arrangement ofv diffuser tubes which may be used in concentration tank 32.
  • a plurality of dituser tubes 100 extend radially from an enlarged end portion of gas feed line 48.
  • a relatively large cylindrical column of gas is thereby produced.
  • Other di'user tube arrangements may be used, if desired.
  • the various arrangements described and illustrated in said copending application Serial No. 360,282 may be used for ditfusing device 4,7.
  • the dituser tubes may take any one of a variety of forms, as for example the diffuser tank elements described in U. S. Patent No. 2,555,201 to Nordell granted December 5, 1950, or those disclosed in application Serial No. 206,237, tiled by Miles A. Lamb on January l6, 1951, and in application Serial No. 246,854, tiled by Joseph J. Klein on September 15, 1951. These tubes direct gas upward along their upper surfaces. Diiusing device 47 should preferably be located in the center and bottom third of the concentration tank and at least a few feet above the bottom of the tank.
  • the diffuser tube elements In order to generate a column of gas over a considerable area, the diffuser tube elements should be equally dispersed about a region extending no less than about 7% of the diameter of the tank, in the case of a tank of circular cross section, or about 7% of the diagonal of a rectangular tank. Circular or square tanks are preferred for use as concentration tanks.
  • the rate f ow of gas through gas diffusing device 47 is kept within the limits of from lo to 3A0 of a cubic foot per minute per foot of internal diameter of concentration tank 32, assuming that the concentration tank 32 has a substantially constant circular cross section. With this limited gas flow, sludge particles will be oated to the top of the raw sludge mixture until substantially all of the solid particles in the concentration tank are concentrated as a floating mass on the top of the mixture.
  • a clarified subnatant then remains below the concentrated sludge. If the rate of gas diffusion were increased above about /o of a cubic foot per minute per foot ofk tank diameter there would be excessive turbulence andthe solids concentration would not build up.
  • a valve 51 in gas line 48 is provided to control the amount of digester gas fed to concentration tank 32.
  • Cover 32 of the concentration tank includes a gas collecting dome 37 which communicates with a line 38 leading to the gas-drawotf line 45 of digester tank 43.
  • the gas fed to concentration tank 32 is thus recirculated through the system, resulting in an economical utilization of the gaseous products of digestion.
  • the vabove specified concentration process is applicable to concentration tanks having other than circular cross sections if the basis for the desirable gas tiow rate is taken, for example, on the basis of the longest diagonal of the horizontal cross section of the concentration tank, assuming that the tank has a constant rectangular cross section. This will be described in more detail hereinafter in connection with the description ofdigester tank 43, where the rate of flow of gas within the digester tank is also dependent on tank diameter or longest diagonal dimension.
  • a line 52 communicating with the bottom of digester tank 43 carries a portion of4 the digested sludge removed from digester tank 43 to the concentration tank 32 through branch lines 53 and 54, including pump 55 and heater 56.
  • Heater 56 maintains the temperature of the sludge at approximately the same temperature as the concentration tank contents.
  • the amount of seed sludge which is mixed with the raw sludge carried to concentration tank 32 should be about 2% to 20% of the raw sludge volume in concen-l tration tank 32 at the time of mixing. Accordingly, the Volume of raw sludge in concentration tank 32 to undergo concentration is determined by any suitable method' soon after it is pumped thereto, and the proper amount of seed sludge is metered to the concentration tank through valves 57 and 58 located, respectively, in lines' ⁇ 53 and 54 leading from the main draw-oft sludge line 52.
  • the combination of gas concentration and seeding of' the concentration tank above described material ly reducesv the time required to complete concentration from aboutY two days, more or less, to as little as one day.
  • the seeding feature has the further advantage that it increases the volume of subnatant produced by as much as'.
  • the use of seed sludge to improve the concentration' of raw sewage has also been found to shorten the time for concentration, when used with other concentrationy processes such as a flotation process utilizing only heat and ⁇ time to effect concentration. This is more fully described and is claimed in the copending application of Philip F. Morgan, Serial No. 361,019, tiled June ll, 1953.
  • the concentrated sludge from concentra-tion tank 32 is pumped to the digester tank 43 through lines 40 and 42 by a suitable pump 41.
  • gravity feed may be utilized to carry the concentrated sludge to the digester tank. This may be done by locating the inlet to the digester tank below the outlet of concentration tank 32.
  • the digester tank will be filled to its normal operating level with sludge undergoing digestion.
  • the supernatant digested sludge liquor in amount corresponding to the amount of concentrated sludge to be introduced will be drawn olf from an upper level in the digestion tank through one or more of provided with a floating roof 60 having a gas collecting dome 45', which is well known in the art.
  • a fixed roof many be used, if d-esired. The contents of the digester tank are thereby isolated from the atmosphere.
  • Gas drawotf line 4S communicates with gas collecting downe, 45 and carries the gaseous products of the digestion. processV to any one of a plurality of locations,
  • drawoff line 45' may communicate with a line 61 leading lto suitable equipment for utilizing such gas, such as gas engines or burners, or to a gas holder.
  • a valve 62 ccntrols the amount of ⁇ gas carried by line 6l.
  • Gas drawor' line 45 as previously state-communicates with valved line 48 leading to gas-diffusing device 47 in concentration tank 32.
  • Branch line 63 communicates with a gas diifusing device 63 which is similar to gas diffusing device 47 in concentration tank 32.
  • Valve 70 in line 63 controls the quantityot' gas circulated in the digester tank. These limits are described in our copending application, Serial No. 360,282, tiled June 8, i953.- f an insufficient amount of gas is circulated in the ⁇ digester tank, the sewage solids tend to accumulate as a floatingmass uponthe top of the sewage liquid, thereby seriously inhibiting the normal anaerobic digestion of the sewage solids. lf the amount of digester gas circulated is too great, excessive turbulence takes place Within the tank with the result that frothing ⁇ takes place and thereby interferes with the normal separation of the digester gas from the material undergoing digestion.
  • heater 56 In addition to the function of heating the seed sludge fed from digester tank 43 to concentration tank 32, heater 56 also performs the function of maintaining the temperature of the sludge in the digester tank 43 at a desired level, for example, from 90 to 95 F. Pump 55 ⁇ is thus periodically put into operation to circulate the contents of digester tank 43 through heater S6 vin line.53, through valve 66 and line 65 Where the heated sludge is discharged into the digester tank.
  • the recirculation of gas within the digestertank is stopped to allow the liquid and solid particles in the digested sludge to separate.
  • the digested sludge then settles to the bottom of the digester tank where it is discharged through Vline 66 and line 6% to sludge drying beds and/or is directed to some other location such as to concentration tank 32 or to another' digester tank where the sludge is utilized as seed sludge, as above described.
  • the digestion process is considered complete when judged yby either one of the following standards. Digestion is complete when 71/2 to l0 cubic ft. of gas per pound of volatile solids in the sludge added to the digester is evolved or when the volatile solids are reduced 40% to 50% by weight.
  • sewage sludge may be digested by the process of the present invention in about ten days.
  • the digestion of sewage sludge as it is generally being carried out commercially takes about thirty days.
  • the elfectiveness of the digestion process of the present invention may be maintained indefinitely by saturating the gas ⁇ which iscirculated within concentration tank 32 and digester tank 43 with moisture.
  • Vembodirrient of a digester tank installation is as follows:
  • Tank diameter inner diam. of circular tank
  • ft 70 Tank depth ft 25 Depth of sludge ft-- 25 Depth of diffusing device from top of sludge ft 23
  • Diameter of diffusing device (circular arrangement of Fig. 2) ft 5% Total rate of gas flow cu. ft;/min 5
  • the re-introduction or recirculation of the digester gas in the concentration tank 32 and digester tank 43 appears to provide a more favorable medium for the propagation and activity of the anaerobic bacteria which effects the concentration of raw sewage sludge and also the decomposition of the sludge.
  • the proportionsof sulfur'compounds, aromatic hydrocarbons, carbonr monoxide and other undesirable constituents inthe gas used should be controlled to such an extent as not toimpa'ir the effective action of the active organisms in thefdig'estion process.v
  • natural 'gas which has been treated withv the customary reagents for sulfur removal so as to make the gas suitable for use for synthesis gas may be employed in the present process.
  • methane-containing gas or digester gas gases including methane as the active constituent in proportions of from about 10% to 15% to 100% and preferably 50% to'70%, the remaining constituents being l inertl or in proportions innocuous tothe organisms active in the digestion process.
  • T he remaining ⁇ constituentsof the gas may thus be carbon dioxide, nitrogen, ⁇ helurn, hydrogen, ethane, propane or mixtures thereof.
  • the number and Vsize of the concentration and digester tanks may be varied to suit the particular needs of a situation.
  • the gas ow rate used in the concentration process of the present invention being based on the cross sectional dimensions of the concentration tank, assumes a tank having a substantially constant cross section. If a concentration tank has a widely varying cross section, the figures given above for the desired range of gas ow rate may need to be adjusted somewhat. However, economical and other considerations favor the use of tanks having a substantially uniform cross section. Concentration tanks are generally of uniform cross section.

Description

March 19, 1957 M. A. LAMB ETAL 2,785,025
SEWAGE DIGESTION PROCESS Filed June 8. 1953 @mm w M MW y I NJ w J RM1 S .MN s
XZE. ON NN X25 uzkum tl 3 United States Patent sEwAGn mcEsrIoN PROCESS Miles A. Lamb, Chicago, and Joseph J. Klein, Glencoe,
Ill., assignors to Chicago Pump Company, a corporation of Delaware Application June 8, 1953, Serial No. 360,284
4 Claims. (Cl. 210-2) The invention relates to a process for the concentration of raw sludge in a sewage disposal system, and more particularly relates to a process of concentration of raw sewage sludge by flotation of the sludge.
The problem of concentrating raw and activated sludge has been the subject of much study and research in recent years for the reason that concentration substantially reduces the cost, size, and complexity of sludge disposal facilities. For example, the cost of installation and operation of digestion facilities due in part to the problem of handling great quantities of supernatant formed during digestion, may be reduced almost in proportion to reduction in moisture content of the raw sludge. Dewatering facilities likewise are troublesome and expensive and could be reduced in size and cost if sludge could be more simply concentrated.
Prior concentration by flotation processes have required the addition of various chemicals, or application of heat for a relatively long time. These prior processes do not use to advantage the products of the sewage disposal process itself in the concentration process to effect a more etlicient sewage disposal installation as in the case of the present invention to be hereinafter described.
ln accordance with the present invention, it has been found that concentration of raw sewage may be more effectively and eciently carried out by introducing gas produced in the digestion process, hereinafter to be referred as digester gas, within the sewage to be concentrated, to gasify the solid particles in the sludge.
undergoing concentration, to reduce the density thereof, and to thereby cause the solid particles to float to the top of the sludge mixture.
It appears that the specific use of digester or methanecontaining gas itself promotes bacterial growth in the sludge undergoing concentration which further materially accelerates and promotes the flotation of the solid sludge particles in the sludge mixture undergoing concentration. lf the gas is introduced into the sludge mixture at too high a rate, excessive motion of the mixture will result which will materially hinder or prevent concentration of the solid particles on the top of the sludge mixture. The digester gas must therefore be gently circulated through the contents of the concentration tank to avoid agitation of the sludge.
The rate of introduction of digester gas into the mixture undergoing concentration should not exceed a maximum rate of 1/10 of a cubic foot per minute per foot of maximum horizontal internal cross-sectional dimension of a tank housing the sludge, where the tank has a substantially constant cross section. All of the solid sludge particles will then float to the top of the sludge mixture in a short time, relative to that required by existing commercial processes, leaving a clarified subnatant below.
If conditions for anaerobic digestion are present, and the gas circulation rate does not exceed a second maximum prescribed limit, regular digestion rather ithan concentration by flotation will take place. The proper control of the rate of digester vgas circulation therefore de.
and claimed in copending application S. N. 360,282, l'ed- I une 8, 1953.
In accordance with a further feature of the present invention, it has been found that the period of time re-` quired for complete concentration of raw sewage is further shortened by purposely seeding the sludge to be concentrated with activated or digested sludge. The quantity of seed sludge to be incorporated in the raw sludge to be concentrated should preferably be from 2 to 20% of the raw sludge volume to which it is added.
The process of gas circulation above described has reduced the time necessary for complete concentration to as short a period as one day. This has resulted in a substantial reduction of the size and cost of a sewage disposal installation capable of handling a given volume of sewage since the volume of sludge fed to the digestion facilities 'for a given amount 0f sewage inuent to the entire system can be reduced by as much as 50% and the volume of the digestion apparatus needed for the relatively time consuming digestion process is reduced in the same amount as the reduction of raw sludge volume by concentration.
Further, the present invention accomplishes this end by utilizing the products of digestion, such as digester gas and digested sludge, to carry out the concentration process to effect an inexpensive and eiicient operation.
The invention will be fully understood from the following description, illustrated by the accompanying drawings in which:
Figure l illustrates a sewage treating system embodying the present invention, the parts being shown diagrammatically and in section; and
Figure 2 is a plan view of the diffusing device in the concentration tank shown in Figure l.
Before describing the novel features of the present invention, the description to follow will first deal with the conventional treatment of the sewage prior to the concentration of the primary or raw sludge obtained from such preliminary treatment in order to show the environment in which the present invention is practiced, to give an overall picture of a workable system incorporating features of the present invention.
Referring more particularly to Fig. l of the drawings, the numeral 10 indicates a conduit through which the raw sewage from the sewage system of a small city, amounting to, say, about one million gallons per day, is discharged into the primary settling tank Il. in general, this raw sewage will have been preliminarily subjected to treatment in the customary comminuting and screening devices to break up and/ or remove large foreign objects and may also have been passed through a conventional sedimentation tank. These devices being conventional and in common use, are not shown.
The primary settling tank, which is of sucient capacity to insure an adequate residence time to permit sedimentation of the sludge, is provided with the usual slow moving sludge collector, diagrammatically illustrated and designated by the numeral 12, and with a sump 13 for the collection of the sludge. `In a system handling,
say, one million gallons of sewage per day, the amount of sludge collected daily in the tank 11 may be, for example,
in the order of ten thousand gallons.
The sewage eflluent, after removal of the primary sludge, may be further treated for removal of additional sludge or may be disposed of in any suitable manner, as by dilution, by means of tiickling filters, or by other suitable means. As illustrated, it may be subjected to aeration, to eect the flocculation of additional sludge,
Patented Mar. 19, 1957 o which i s then permitted to settle and is preferably added to the sludge collected in the primary settling tank. Thus the eliiuent from the primary settling tank may pass through aconduit 14 to the aeration tank I5, through which the sewage travels slowly while air is forced into and through the sewage by means of the Vdiffusers 16, which are diagrammatically illustrated. These ditusers may b e of any suitable type, for example, such as that shown in the United States patents to Lannert, No. 2,328,655, granted September 7, 1943, and Nordell, No. 2,555,201, granted December 5, 1950, or in the copending application of Lamb, Serial No. 206,237, tiled January 16, 1951, and Klein, Serial No. 246,854, tiled September 15, 1951.
The aerated sewage leaving the tank 15 passes through a conduit 17 into the iinal settling tank 13, which is of such capacity that the sewage moves slowly through it, permitting settling of the flocculated sludge. This tank -is likewise provided with the usual slow moving sludge collector, illustrated diagrammatically and designated by the number 19'. The sludge is collected in a sump 20. As is customary, the sludge collected in the sump 20 is withdrawn through pipe 21 by pump 22, which discharges it vthrough the pipe 23 into the primary settling tank 11, where it settles and collects in the sump 13 `in admixture with the primary sludge. if desired, a part of the sludge collecte-d in settling tank 1S may be returned through the line -24 to the conduit 114 and the aeration tank 15.
The treated sewage efliuent from the settling tank 18 passes out through the cftiuent conduit 24 for disposal in the usual manner, such as filter beds, or may be handled in any-other desired manner.
Instead of being handled in an aeration system of the character illustrated, the sewage effluent leaving the primary settling tank 11 may be disposed of in any other suitable manner; for example, by filtration or, where permissible, by stream dilution. in such case, the sludge collected in primary settling tank 11 will consist entirely of primary or raw sludge, or of such sludge admixed with any ripe sludge that may be deposited from supernatant liquor from the anaerobic digestion of the sludge that may be Vreturned as hereinafter described.
The sludge collected in tank 11 is withdrawn from sump 13 through line 26 by pump 27 and discharged through line 28 into the aeration and mixing tank 29. While the withdrawal of the primary sludge from the tank 1'1 may be continuous, in ordinary operation, it is generally preferred that it be intermittent. Usually such withdrawal is effected about three times a day, about one-third of the total of the sludge collected per day being removed from tank 1i each time. Thus with a system as hereinbefore referred to, handling approximately 1,000,000 gallons of sewage per day and in which the total collection of sludge is about 10,000 gallons per day, the amount of sludge removed from tank 11 at each time of such removal will, considering normal variations, be in the order of 3,000 to 3,500 gallons. The capacity of the aerating and mixing tank 29 may have an effective'v volume equal to or greater than the raw sludge pump capacity per minute.
In the aeration tank 29 the sludge is aerated to a certain extent, preferably using air diifusers, of which one is illustrated at 30, these being the same or of the same character as the air diusers in the aeration tank 15 previously referred to. The amount of air used is in the range of to 100% by volume on the sludge, preferably about,75%. Thus with the amount of sludge being handled per pumping period of about 3,500 gallons, the.
amount of airV introduced would be in the range from 115 to- 470 cubic feet and preferably about 350 cubic feet. Depending upon the number of air diiusers used and the capacity-or Veach of thediiusers, the time of re'- tention of. the sludge in the aerating and mixing tankmay. be from l` to 5 minutes. Thuswith diffuser tubes,
they propernumher ofsuchairditfusers can be selected to furnish air at the approximate rate of raw sludge pumpage through the aeration tank, i. e. at approximately equal volumes.
The mixing of the air with the raw sludge may be carried out at any normal operating temperature above the freezing point,V say in the range of from 32 F. to 90 F. The air utilized should be at a temperature of not less than 30 F. and its temperature may be higher, say up to 150 ii., and may contribute to maintaining the in the aeration tank 29 above freezing temperature during cold weather.
Upon the completion of the introduction of the desired quantity of air, or preferably slightly before its completion, an adsorptive material is thoroughly admixed with the sewage sludge and suspended therein. Preferably finely divided coke is employed, the coke being ground sufficiently finely so that the greater portion thereof, say will pass through a 200 mesh sieve and all of it wilt' pass through a 75 mesh sieve. The powdered coke may be introduced into the aerating and mixing tank 29 in any suitable manner, for example, from the hopper 31. When introduced in the latter stages of the aeration process, the introduction of the air effects the desired admixture of the coke with the sludge. Supplementary mechanical mixing devices may be employed, if desired. As is readily apparent, tlie powdered coke may also be admixed with the sludge promptly after its aeration or in its flow from the aeration and mixing tank 29 to the concentration tank hereinafter referred to, any suitable mixing means being employed. The aeration of the raw sewage and addition of an adsorptive material, if utilized, should preferably precede rather than follow the concentration process to be described. Other adsorptive materials may be employed instead of powdered coke, such as lfullers earth, silica gel, diatomaceous earth or the like. Coke is, however, preferred. The proportion of finely dividedv adsorptiveV material, such as coke, that is added is suitably inthe order of`0.5 to 2.5 parts per parts of sludge, Yby weight, and preferably, in the case of coke, is about 1- part per 100 parts of sludge by weight.
it should oe noted that although the preliminary aeration of the raw sludge to undergo digestion is preferred, such aeration may be omitted. The primary operation to 'oe performedv in the digestion process of the present invention is one. of anaerobic digestion which does not require the presence of oxygen to effect digestion.
Promply after the aeration of the sludge and its intermixture with the coke or other adsorptive material, the sludge is` introduced into the concentration tank 32. The sludge may suitably bewithdrawn from the aeration and mixing tank 29 through line 33 by pump 34. The raw sludge entering concentration tank 32 is heated in a suitable heater 34 which may, for example, be similar to the heater. disclosed in copending application Serial No. 290,848, on` a Method and Apparatus for Treating Sewage Sludge, filedr May` 3l, 1952, by Milton Spiegel and MilesH. Lamb. The temperature to which the raw sludge is` heated is not critical, but the sludge is preferably heated to a temperature of from 80 to 100 F.
Although it is preferred to heat the sludge externally of the concentration tank 32 to avoid unnecessary obstructionfrom-heatingcoils within the concentration tank, such heating may be carried on, if desired, Within the concentrationtank. 1n either case, the concentration tank should'. beinsulated to prevent. the escape of heat therefrom..
The sludgel enteringthe concentration tank may, for example, consist of? from about 3 to 8% by weight of solids out-of which 40% to 70% may bevolatile solids.
The aerated raw sludge (or the raw sludge, if the aeration step` is omitted) in sludge concentration tank 32 isrcorncentrated bybeing floated to the surface of the mixture therein in amanner to be described. A relatively clarified liquor (subnantant) forms in the bottom of concentration tank 32 as a result of the concentration process, which is drawn off from the lower level of the concentration tank through one or more withdrawal pipes indicated generally by numeral 36. The subnatant may then be discharged into primary settling tank l1 as by pump 39 via lines 38 and 37. The concentrated sludge tloating in the upper portion of concentration tank 32 may be suitably withdrawn from this tank through line 40 by pump 41 and discharged through line 42 to a digester tank 43. This concentrated sludge may include as much as 8% to 12% solids by weight.
Concentration tank 32 is preferably of square or circular cross section and includes a cover 32' of the tixed or floating variety, a fixed one being shown, to isolate the contents therein from the atmosphere.
The raw sludge is concentrated in concentration tank 32 as by digester gas fed from a digester tank, such as tank 43, by means of a blower 44 from a gas draw-ott line 45 communicating with the gas collecting dome 45 of digester tank 43. The gas passes through line 48 and through a gas ditusing device 47, similar to difiusers 16, located preferably near the bottom and center of the concentration tank 32. The dilfusing device 47 should produce a slowly rising column of gas extendingover a considerable area. This slowly rising column of gas should not agitate the sewage sludge or impart thereto a circulatory movement.
Diffusing device 47 preferably would include a series of diffusing elements or tubes arranged near the center of the bottom of concentration tank 32.
Figure 2 shows an exemplary arrangement ofv diffuser tubes which may be used in concentration tank 32. Thus a plurality of dituser tubes 100 extend radially from an enlarged end portion of gas feed line 48. A relatively large cylindrical column of gas is thereby produced. Other di'user tube arrangements may be used, if desired. For example, the various arrangements described and illustrated in said copending application Serial No. 360,282 may be used for ditfusing device 4,7.
The dituser tubes may take any one of a variety of forms, as for example the diffuser tank elements described in U. S. Patent No. 2,555,201 to Nordell granted December 5, 1950, or those disclosed in application Serial No. 206,237, tiled by Miles A. Lamb on January l6, 1951, and in application Serial No. 246,854, tiled by Joseph J. Klein on September 15, 1951. These tubes direct gas upward along their upper surfaces. Diiusing device 47 should preferably be located in the center and bottom third of the concentration tank and at least a few feet above the bottom of the tank. In order to generate a column of gas over a considerable area, the diffuser tube elements should be equally dispersed about a region extending no less than about 7% of the diameter of the tank, in the case of a tank of circular cross section, or about 7% of the diagonal of a rectangular tank. Circular or square tanks are preferred for use as concentration tanks.
Gas in the form of bubbles rises to the surface of the contents in concentration tank 32. The solid particles in the raw sludge undergoing concentration are thereby gasilied to reduce the density thereof and cause the solid particles to lloat to the top of the sludge mixture.
Excessive motion of the mixture caused by the tlow of digester gas through the sludge in the concentration tank must be prevented or else the solid sludge particles will not remain concentrated at the top of the sludge mixture. The digester gas must therefore be gently circulated through the contents of the concentration tank. To elect this end, the rate f ow of gas through gas diffusing device 47 is kept within the limits of from lo to 3A0 of a cubic foot per minute per foot of internal diameter of concentration tank 32, assuming that the concentration tank 32 has a substantially constant circular cross section. With this limited gas flow, sludge particles will be oated to the top of the raw sludge mixture until substantially all of the solid particles in the concentration tank are concentrated as a floating mass on the top of the mixture. A clarified subnatant then remains below the concentrated sludge. If the rate of gas diffusion were increased above about /o of a cubic foot per minute per foot ofk tank diameter there would be excessive turbulence andthe solids concentration would not build up. A valve 51 in gas line 48 is provided to control the amount of digester gas fed to concentration tank 32.
Cover 32 of the concentration tank includes a gas collecting dome 37 which communicates with a line 38 leading to the gas-drawotf line 45 of digester tank 43. The gas fed to concentration tank 32 is thus recirculated through the system, resulting in an economical utilization of the gaseous products of digestion.
The vabove specified concentration process is applicable to concentration tanks having other than circular cross sections if the basis for the desirable gas tiow rate is taken, for example, on the basis of the longest diagonal of the horizontal cross section of the concentration tank, assuming that the tank has a constant rectangular cross section. This will be described in more detail hereinafter in connection with the description ofdigester tank 43, where the rate of flow of gas within the digester tank is also dependent on tank diameter or longest diagonal dimension.
lt has been found that the length of time required to completely concentrate sewage sludge in concentration tank 32 can be materially reduced by introducing digested sludge as seed sludge -from digester tank 43 into the concentration tank. Accordingly, a line 52 communicating with the bottom of digester tank 43 carries a portion of4 the digested sludge removed from digester tank 43 to the concentration tank 32 through branch lines 53 and 54, including pump 55 and heater 56. Heater 56 maintains the temperature of the sludge at approximately the same temperature as the concentration tank contents.v
The amount of seed sludge which is mixed with the raw sludge carried to concentration tank 32 should be about 2% to 20% of the raw sludge volume in concen-l tration tank 32 at the time of mixing. Accordingly, the Volume of raw sludge in concentration tank 32 to undergo concentration is determined by any suitable method' soon after it is pumped thereto, and the proper amount of seed sludge is metered to the concentration tank through valves 57 and 58 located, respectively, in lines'` 53 and 54 leading from the main draw-oft sludge line 52.
The combination of gas concentration and seeding of' the concentration tank above described materially reducesv the time required to complete concentration from aboutY two days, more or less, to as little as one day. The seeding feature has the further advantage that it increases the volume of subnatant produced by as much as' The use of seed sludge to improve the concentration' of raw sewage has also been found to shorten the time for concentration, when used with other concentrationy processes such as a flotation process utilizing only heat and` time to effect concentration. This is more fully described and is claimed in the copending application of Philip F. Morgan, Serial No. 361,019, tiled June ll, 1953.
As previously stated, the concentrated sludge from concentra-tion tank 32 is pumped to the digester tank 43 through lines 40 and 42 by a suitable pump 41. If desired, gravity feed may be utilized to carry the concentrated sludge to the digester tank. This may be done by locating the inlet to the digester tank below the outlet of concentration tank 32.
In ordinary operation, the digester tank will be filled to its normal operating level with sludge undergoing digestion. lust prior to the introduction of the sludge from the concentration tank, the supernatant digested sludge liquor in amount corresponding to the amount of concentrated sludge to be introduced will be drawn olf from an upper level in the digestion tank through one or more of provided with a floating roof 60 having a gas collecting dome 45', which is well known in the art. A fixed roof many be used, if d-esired. The contents of the digester tank are thereby isolated from the atmosphere.
Gas drawotf line 4S communicates with gas collecting downe, 45 and carries the gaseous products of the digestion. processV to any one of a plurality of locations, Thus, drawoff line 45'may communicate with a line 61 leading lto suitable equipment for utilizing such gas, such as gas engines or burners, or to a gas holder. A valve 62 ccntrols the amount of `gas carried by line 6l. Gas drawor' line 45, as previously state-communicates with valved line 48 leading to gas-diffusing device 47 in concentration tank 32. A branch line 63 extending from-line 4S ahead of valve 51 into the digester tank, isprovided to recirculate digester gas, .by means of blower 44,- to the digester tank 43 to effect an accelerated digestion of the sewage sludge inaccordance with the present invention. Branch line 63 communicates with a gas diifusing device 63 which is similar to gas diffusing device 47 in concentration tank 32.
The rate at which digester gas-is introduced into the digester tank and the desired velocity of movement of the contents of the digester tank desired should fall within well defined limits in order to aid the digestion process. Valve 70 in line 63 controls the quantityot' gas circulated in the digester tank. These limits are described in our copending application, Serial No. 360,282, tiled June 8, i953.- f an insufficient amount of gas is circulated in the `digester tank, the sewage solids tend to accumulate as a floatingmass uponthe top of the sewage liquid, thereby seriously inhibiting the normal anaerobic digestion of the sewage solids. lf the amount of digester gas circulated is too great, excessive turbulence takes place Within the tank with the result that frothing `takes place and thereby interferes with the normal separation of the digester gas from the material undergoing digestion.
In addition to the function of heating the seed sludge fed from digester tank 43 to concentration tank 32, heater 56 also performs the function of maintaining the temperature of the sludge in the digester tank 43 at a desired level, for example, from 90 to 95 F. Pump 55 `is thus periodically put into operation to circulate the contents of digester tank 43 through heater S6 vin line.53, through valve 66 and line 65 Where the heated sludge is discharged into the digester tank.
After digestion is complete, the recirculation of gas within the digestertank is stopped to allow the liquid and solid particles in the digested sludge to separate. The digested sludge then settles to the bottom of the digester tank where it is discharged through Vline 66 and line 6% to sludge drying beds and/or is directed to some other location such as to concentration tank 32 or to another' digester tank where the sludge is utilized as seed sludge, as above described.
The digestion process is considered complete when judged yby either one of the following standards. Digestion is complete when 71/2 to l0 cubic ft. of gas per pound of volatile solids in the sludge added to the digester is evolved or when the volatile solids are reduced 40% to 50% by weight. On either of these standards, sewage sludge may be digested by the process of the present invention in about ten days. On the same standards, the digestion of sewage sludge as it is generally being carried out commercially, takes about thirty days.
The elfectiveness of the digestion process of the present invention may be maintained indefinitely by saturating the gas` which iscirculated within concentration tank 32 and digester tank 43 with moisture. A humidifier or steam diifuser tubes making up diffusing devices 47 and 63, re-
spectively, so that these devices can operate for long periods of time Without loss of efficiency and without the need for frequent cleaning.` The humiditication of a gaseous body used in conjunction with diffuser tube elements for this lpurpose isV disclosed andY claimed in copending application SerialNo. 243,702, John A. Tapleshav and Carl H. Nordell, tiled August 25, 1951, now Pate No. 2,694,042, issued November 9, 1954.
One exemplary Vembodirrient of a digester tank installation is as follows:
Tank diameter (inner diam. of circular tank) ft 70 Tank depth ft 25 Depth of sludge ft-- 25 Depth of diffusing device from top of sludge ft 23 Diameter of diffusing device (circular arrangement of Fig. 2) ft 5% Total rate of gas flow cu. ft;/min 5 The re-introduction or recirculation of the digester gas in the concentration tank 32 and digester tank 43 appears to provide a more favorable medium for the propagation and activity of the anaerobic bacteria which effects the concentration of raw sewage sludge and also the decomposition of the sludge.
In consequence thereof, a more etective digestion is secured ina given time and the digestion process is itself` materially accelerated. Thus, it'has been found that, by the use o'f the present process, the time required to eifect a given extent ofdig'estion or decomposition may be decreased by approximately.' 50% or more. in this way, the capacity of a given system may be materially increased.
While reference in the preceding description has been made to the recirculation' of digester gas, it has been found that similar results may be secured by the introduction into the digester or concentration tanks of substantially pure methane in amounts corresponding to 50 to 75% of the amounts'of digester gas hereinbefore referred to. Other methan'elcontaining gases, such as natural gas, for example, may also be employed 'in amounts sufficient to'provide'equivalent quantities of methane gas. in such case, the proportionsof sulfur'compounds, aromatic hydrocarbons, carbonr monoxide and other undesirable constituents inthe gas used should be controlled to such an extent as not toimpa'ir the effective action of the active organisms in thefdig'estion process.v Thus, natural 'gas which has been treated withv the customary reagents for sulfur removal so as to make the gas suitable for use for synthesis gas may be employed in the present process.
By the term methane-containing gas or digester gas, as used herein, is meant gases including methane as the active constituent in proportions of from about 10% to 15% to 100% and preferably 50% to'70%, the remaining constituents being l inertl or in proportions innocuous tothe organisms active in the digestion process. T he remaining` constituentsof the gas may thus be carbon dioxide, nitrogen,`helurn, hydrogen, ethane, propane or mixtures thereof.
Numerous modifications may be made of the preferred process of the instant invention as above described without deviatingfrom the broader, generic aspects of the present invention.' For example, although the concentration process of the present invention is preferably utilized in a system including anaerobic digestion apparatus where methane-containing gas and digested sludge is readily available, the invention in its broader aspect does not require the presence `of anaerobic'digestion apparatusif methane-containing gas ordigested sludge is otherwise available.V
Additionally, the number and Vsize of the concentration and digester tanks may be varied to suit the particular needs of a situation.
The gas ow rate used in the concentration process of the present invention, being based on the cross sectional dimensions of the concentration tank, assumes a tank having a substantially constant cross section. If a concentration tank has a widely varying cross section, the figures given above for the desired range of gas ow rate may need to be adjusted somewhat. However, economical and other considerations favor the use of tanks having a substantially uniform cross section. Concentration tanks are generally of uniform cross section.
We claim:
1. In the anaerobic digestion of sewage sludge, wherein a body of such sludge is subjected to anaerobic digestion in an enclosed container with the production of methane-containing gas, the steps of removing such methane-containing gas from said container and introducing same into a second container containing sludge to be later digested in said rst mentioned container, as a rising column of gas, at a rate not to exceed 1/10 of a cubic foot per minute per foot of longest horizontal internal cross-sectional dimension of said second container, to gasify the solids in the sludge and to cause same to rise to the surface of the sludge mixture, and recirculating said gas produced in said trst mentioned container in the said container to eect circulation of sludge therein and thereby promote the anaerobic digestion of the sludge therein.
2. The method of claim 1 wherein the gas introduced into said second container to effect concentration is collected and re-introduced into said rst mentioned container.
3. The method of claim l wherein the said gas is introduced into said second container in an amount exceeding 1/20 of a cubic foot per minute per foot of longest horizontal internal cross-sectional dimension of said second container.
4. In the anaerobic digestion of sewage sludge, wherein a body of such sludge is subjected to anaerobic digestion in an enclosed container with the production of methanecontaining gas, the steps of removing such methanecontaining gas from said container and introducing same into a second container containing sludge to be later digested in said first mentioned container, as a rising column of gas, at a rate not to exceed 1/10 of a cubic foot per minute per foot of longest horizontal internal crosssectional dimension of said second container, to gasify the solids in the sludge and to cause same to rise to the surface of the sludge mixture, removing the gasied sludge solids from the said second container and introducing the same into said rst mentioned container, and recirculating said gas produced in said rst mentioned container in the said container to effect circulation of sludge therein and thereby promote the anaerobic digestion of the sludge therein.
References Cited in the tile of this patent UNITED STATES PATENTS 1,056,548 Imhoff Mar. 18, 1913 1,820,976 Imhot Sept. 1, 1931 2,190,598 Fischer Feb. 13, 1940 2,528,649 Genter et al Nov. 7, 1950 2,615,842 Kraus Oct. 28, 1952 2,638,444 Kapper May l2, 1953 2,640,027 McNamee et al May 26, 1953

Claims (1)

1. IN THE ANAEROBIC DIGESTION OF SEWAGE SLUDE, WHEREIN A BODY OF SUCH SLUDGE IN SUBJECTED TO ANAEROBIC DIGESTION IN AN ENCLOSED CONTAINER WITH THE PRODUCTION OF METHANE-CONTAINING GAS, THE STEPS OF REMOVING SUCH METHANE-CONTAINING GAS FROM SAID CONTAINER AND INTRODUCING SAME INTO A SECOND CONTAINER CONTAINING SLUDGE TO BE LATER DIGESTED IN SAID FIRST MENTIONED CONTAINER, AS A RISING COLUMN OF GAS, AT A RATE NOT TO EXCEED 1/10 OF A CUBIC FOOT PER MINUTE PER FOOT OF LONGEST HORIZONTAL INTERNAL CROSS-SECTIONAL DIMENSION OF SAID SECOND CONTAINER, TO GASIFY THE SOLIDS IN THE SLUDGE AND TO CAUSE SAID TO RISE TO THE SURFACE OF THE SLUDGE MIXTURE, AND
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