US3079663A - Method and apparatus for producing tobacco smoke filters - Google Patents

Method and apparatus for producing tobacco smoke filters Download PDF

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Publication number
US3079663A
US3079663A US736900A US73690058A US3079663A US 3079663 A US3079663 A US 3079663A US 736900 A US736900 A US 736900A US 73690058 A US73690058 A US 73690058A US 3079663 A US3079663 A US 3079663A
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Prior art keywords
tow
jet
rolls
air
filaments
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US736900A
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Richard F Dyer
Gallagher Paul
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Eastman Kodak Co
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Eastman Kodak Co
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Priority to NL239385D priority Critical patent/NL239385A/xx
Priority to GB918598D priority patent/GB918598A/en
Priority to NL113839D priority patent/NL113839C/xx
Priority to US736900A priority patent/US3079663A/en
Application filed by Eastman Kodak Co filed Critical Eastman Kodak Co
Priority to ES0249365A priority patent/ES249365A1/en
Priority to DE1959E0017650 priority patent/DE1188998C2/en
Priority to FR795127A priority patent/FR1226046A/en
Priority to CH356705D priority patent/CH356705A/en
Application granted granted Critical
Publication of US3079663A publication Critical patent/US3079663A/en
Priority to MY196412A priority patent/MY6400012A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02GCRIMPING OR CURLING FIBRES, FILAMENTS, THREADS, OR YARNS; YARNS OR THREADS
    • D02G1/00Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics
    • D02G1/16Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics using jets or streams of turbulent gases, e.g. air, steam
    • D02G1/161Producing crimped or curled fibres, filaments, yarns, or threads, giving them latent characteristics using jets or streams of turbulent gases, e.g. air, steam yarn crimping air jets
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • A24D3/0229Filter rod forming processes
    • A24D3/0233Filter rod forming processes by means of a garniture
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D39/00Filtering material for liquid or gaseous fluids
    • B01D39/14Other self-supporting filtering material ; Other filtering material
    • B01D39/16Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres
    • B01D39/18Other self-supporting filtering material ; Other filtering material of organic material, e.g. synthetic fibres the material being cellulose or derivatives thereof
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01GPRELIMINARY TREATMENT OF FIBRES, e.g. FOR SPINNING
    • D01G99/00Subject matter not provided for in other groups of this subclass
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2922Nonlinear [e.g., crimped, coiled, etc.]

Definitions

  • This invention relates to the production of tobacco smoke filters suitable for cigarettes, pipes, and cigarette
  • this invention is concerned with an apparatus and process for treating a continuous filament crimped tow to substantially increase the filtration efiiciency thereof for the removal of nicotine, tars and aerosol particles from the tobacco smoke while at the same time elfecting a reduction in weight of filter material required and materially improving the processing of the tow into filter plugs.
  • One object of this invention is to provide an apparatus and means for processing a continuous filament crimped tow into a filter plug having a randomized filament arrangement, said filaments retaining a high .degree of their original crimp so that a filter may be obtained which has an eificiency that is relatively high to the weight of the filter material. Another object is to obtain a well opened up tow suitable for filters without substantially impairing the strength or the degree of crimp in the individual filaments.
  • a particular object is to provide a simple and efiective apparatus arrangement for converting a dense continuous filament crimped tow into a well opened up filter tow readily susceptible to treatment with plasticizer and the like.
  • Still another object is to make a filter from continuous filament crimped tow, which filter for a specific filament size and resistance to air flow, is more efiicient in removing tars and nicotine than prior art filament filters.
  • a still further object is to utilize tows which have a higher crimp than heretofore tolerated with the prior art processes used in making filters from such tow.
  • FIG. 1 is a schematic flow diagram of the processing of the continuous filament tow into a filter plug for tobacco smoke filters.
  • FIG. 2 is a schematic diagram of the overall apparatus arrangement of apparatus which would be used in carrying out the process of the present invention.
  • FIG. 3 is a detailed cross-sectional view of the finding jet of the present invention.
  • FIG. 4 is a part semi-diagrammatic front end view of the jet shown in H6. 3.
  • one object of the tow conditioning of filter tow is to convert the densely packed crimped tow from the supply package into a relatively fiufiy resilient flat sheet of filaments which are in a randomized state, then to establish an adhesive condition on the filaments by suitto 50 p.s.i. gauge. .high velocity gas how is produced which is evenly disjet and the rolls 6. the exit zone of the jet the filaments can thus be violentbly 7 described above.
  • tow feed No. 1 may be at the rate of 50 y.p.m.
  • tow feed No. 2 at the rate of 49 y.p.m.
  • tow .feedNo 3 at the rate of 48 y.p.m.
  • the ifilamen-ts are given a strong thrust by the air flow such that tension is generated in the tow between the rolls 4and the jet 5.
  • the tow then passes to roll pair 6 which is driven 'atsnch a speed relative to roll pair 4 as to allow the tow to'be in arelaxed state between-the In this area and particularly in 1y agitated and vibrated such that each filament is separated from the other and the crimp knees assume completely random position relative to each other.
  • This cycle of blooming or debundlizing is then repeated with roll pairs 6 and 9 and jet 7.
  • tension is again present between rolls 6 and jet 7 due to the in- :tiuence of the high velocity jet air on the tow.
  • Roll pair 9 however is driven at a speed relative to roll pair 4S so that betweenjet 7 and rolls 9 therevis substantially no tension other than that required to prevent excessive sag in the tow.
  • spray booth 8 which applies plasticizer or other material to the tow. Since the tow is relaxed and the filaments wellseparated at this point excellent distribution and even application of the plasticizer or the like on each filament is possible.
  • a common drive motorll drivesall the individual rolls and the cigarette machine 10 by chain, cog belt or other positive drive means.
  • variable speed transmissions 12 and 13 Interposed between the motor 11 and roll pairs '4 and 6 there are variable speed transmissions 12 and 13 such that the relative speeds of roll ;pairs 4, 6 and9' can be adjusted to establish the desired degree of relaxation in each blooming stage.
  • roll pair 4 and blooming jet 5 may be omitted with the tow passing directly from guide 3a to roll pair 6.
  • This arrangement may not bloom the 'tow as etiectivelyas the two-jet assem-
  • the one jet assembly of the present invention will process the tow better than prior art procedures. Thereare other'alternatives.
  • Another alternative is to utilize one flufiing jet 7 and do some tension blooming between rolls 4 and 6 with or without the aid of a beater between the two sets of rolls. This method requires a larger tow to provide a specified filter efiiciency and firmness.
  • The-two nozzle plates 16 and 17 are assembled to venturi body plates Hand 14 respectively by cap screws as indicated at 25 and 26. These nozzle plates coact with each other to form a slot-like yarn entrance passage 27 which convengesat 28.
  • the nozzle plate 16 also co acts with venturi plate 15 to form a wedge-shaped chamber .29 which is in communication with the circular air chamber 20 via'slot passage 21. At the down stream side of this chamber 29 it converges at an angle of about fifteen degrees so that air passing through is accelerated to a high velocity at the transition between the venturi entrance 22and the venturi throat 23.
  • Nozzle plate 17 and venturi plate 14 coact in a similar manner. As apparent from FIG. 3 that although only slot 22, airchamber 20, etc. have been referred to specifically, that on the otherside of part17 there are comparable slots, chambers and the like. Hence, further description thereof appearsto be unnecessary.
  • the tow enters the jet through passageway 27 and atthe tipof the nozzle 2 8, it is subjected to the impingement-ofthe high velocity sheets of air emerging from the venturi entrances. It maybe observed from inspection of these'ctional v'iew shown in FIGURE 3 of the drawings that there is a low-included angle of incidence. Also the tow is subjected to the impingement "of two'thin intersecting fiat sheets of air emerging from "the passages tormed by the mating plates 15, 16 and 14, 17 so that there are two high velocity sheets of air In the throat 23 air and emer ing from the entrances.
  • tow are intermixed and parallelized in their direction of flow and the velocityeflect of the air generates a tension in' the tow'and a suction in'the nozzle entrance 27.
  • This suction is strong enough to make the jet self 'threading, i;e. it will suck the tow into the jet.
  • the air begins to lose velocity and expand. This action has the effect of exploding the tow and causing the filaments of the 'tow to diverge also, thus separating the filaments one from another. 'Also the filaments tend to vibrate muchin the manner of ribbons attached to the front of an electric fan. This :action further assists This will bloom the tow pressure spot.
  • divergence of the venturi should be from four to ten seven times the length.
  • the filaments Recalling that between the jet and the downstream feed roll the tow is allowed to relax and Contact, the filaments also move longitudinally relative to each other so that knees of crimp in adjaccnt filaments are thrown out of phase in a completely random manner. Thus as the tow emerges from the jet the filaments are completely rearranged relative to each other as compared with their relative positions on entering the area of high velocity gas flow.
  • FIG. 4 The principal purpose of FIG. 4 is to illustrate that the jet shown in FIG. 3 is not the usual round or cylindrical type of jet known in the prior art but is an elongated slot type of jet. In FIG. 4 the jet has been shown broken away on one corner to show the air chamber. The width of the jet may be, for example, 4-20 inches.
  • the air inlet pipe is shown at 20 as are the nozzle plate parts 16 and 17.
  • the opening indicated at 27 is the entrance passageway for the tow being fed to the jet.
  • PEG. 4 also shows parts 18 and 13:: which are the end plates.
  • An end plate is merely a metal plate bolted onto the side of the parts discussed in the description of FIG. 3 to provide an end closure for the jet. Also, the construction of the end plate is such that the spacing of the parts may be accomplished to the desired degree.
  • the length i the diverging portion 24 should be about four to ten times the length of the throat 23 and preferably about
  • the nozzle throat length 23 should be about three times its width.
  • the total area of the entrance slots as 22 should be about .10 times the area of the venturi throat. This latter ratio, however, is adjustable depending on the amount of suction or back pressure desired in the entrance nozzle 2. A low ratio tends to increase the suction while too high a ratio causes back pressure or blow back in the nozzle entrance 27.
  • the width of the jet is largely determined by the width to which it is desired to spread the tow.
  • the proportion of the area of the venturi throat to the denier of the tow is not unduly critical but values in the order of one square inch per 50,000 denier are esirable.
  • the included angle of the venturi throat entrance formed by plates 14 and 15 is preferably 90 but may vary from 4-5 to 135.
  • the manner in which the tow enters and leaves the jet can be arranged to improve the blooming. In general a straight line pass is less desirable. Bringing the tow in parallel to the jet axis and removing it at about a right angle produces improved results. Also about a right angle bend in the tow as it enters the jet and 21 second approximate right angle bend as it leaves with the tow either reversing its general direction of flow or ending up proceeding in the same direction are also bene- EXAMPLE I Filter rods were made by the air blooming process of this invention using a 54,000 denier tow containing approximately 20,300 filament-s having an average size of 2.6 denier.
  • filter rods were made by the prior art proce lures using a 72,000 denier tow containing approximately 27,700 filaments having an average size of 2.6 denier.
  • the physical characteristics and filtering eiiiciency of both rods are shown in the following table.
  • Filter rods were made by the air blooming process of the present invention using 5 d./f.70,000 denier tow. Filter rods were made by the prior art tensioning process using 5 d./f.-70,000 denier tow and also 5 d./f.- 80,000 denier tow. The comparative tests are tabulated below.
  • the tow was under no tension between jet 5 and roll "set 6 and between jet 7 and roll set 9.
  • the speed of the roll sets 4 and -6 in this case were equal with the .jet 5 being used to flex-the tow much in the manner of a spring, but this flexing-opened up the tow, randomized the filament arrangement and the locations of the crimp x-knees.
  • the roll speeds of the various rolls may be as follows: Input teed roll set '4, 200 y.p.-m.; rolls 4 to 6 speed ratio, 1.20/1 to .7/ 1; rolls 6 to 9speed'ratio, 1.20/1 to .8/ 1.0.
  • the total denier (T.D.) of the tow may vary bet-ween 15,000 to 100,000 and the denier per filament (D.F.')' may be .1 to 8. As pointed out above, this invention works well on highly crimped filaments.
  • the crimp in the tow would generally not be less than 7 crimps' per inch, and may be l7 or 18 per inch. In cer- --tain filaments the crimp may be higher, say up to per inch.
  • plasticizer glycerol triacetate weus'ed the plasticizer glycerol triacetate to the extent of 812% on the filaments
  • other plasticizers as dimethoxycthyl phthalate'or triethyl citrate may be used.
  • other materials such as dextrin or gum arabic in aqueouss'olution may be applied.
  • the term psi. gauge means pounds per square inch above atmospheric pressure as measured by any standard pressure recording instrument.
  • the tow is opened up and the crimp put out of registry; said air flow being distinctly in the direction of movement of the tow thereby advancing the tow, withdrawing the tow from the jet by further rolls at a speed such that'thetow is not put under tension, passing this withdrawn tow through a further jet where the tow is subjected to further air treatment,'then passing the'proc- 'essed tow through a spray booth and further rolls, said last-mentioned rolls also operating at a speed so that the tow is not put under tension and conducting the processed tow from the last-mentioned rolls to filter formation; and throughout the process avoiding tensions in the tow greater than those required to support and transport the tow.
  • tow through a high velocity slot venturi jet having a rectangular divergent exit section supplied with air including contacting the compact ribbon-like crimped tow with two intersecting fiat thin streams of high velocity air at a low angle of incidence, passing both the tow and air stream through a venturi throat to further accelerate the air velocity, then causing the air to expand and lose velocity in the divergent exit portion of the venturi such that the compact crimped tow is caused to expand and bloom in width and thickness and the filaments are longitudinally displaced relative to each other whereby the crimp is put out of registry without breaking the filaments.
  • a method of manufacturing tobacco smoke filters from crimped tow in a package form the steps which comprise withdrawing said tow from said package through the nip of a pair of feed rolls, passing the tow from said rolls through a high velocity rectangular cross section venturi jet supplied with a gas, said jet being positioned in close proximity to said rolls and the jet being of a construction whereby the gas flows from the jet in two sheets of gas in a direction relatively parallel to the direction of movement of the tow so that the tow is advanced by the gas, and conducting said tow after it passes through such slot jet to further steps for forming a filter therefrom and throughout the process avoiding tensions in the tow greater than those required to support and transport the tow.
  • An apparatus arrangement for carrying out processes for advancing and opening tow in the manufacture of filters which comprises three pairs of feed rolls in series, said feed rolls being adapted to receive and pass through the nip of the rolls a continuous filament crimped tow, a high velocity rectangular cross section venturi jet positioned between the first and second roll pair, said jet when supplied with gas being adapted to advance and open said tow, a further jet and spray booth positioned between the second and third roll pair, and means for forming in series with the third roll pair for forming tow processed in said jets into filter elements.
  • a high velocity rectangular cross section venturi jet having a divergent exit section adapted to be supplied with a gas positioned between the two pairs of rolls and in close proximity to the first pair of rolls, said jet being of a construction having an inlet for tow as it is received from the first pair of rolls and an exit from the jet, the internal construction of the jet being such that the gas supplied to the jet is caused to contact the tow and then is accelerated in the same direction as the movement of the tow to a high velocity, and is then caused to expand as it is discharged from the jet in the divergent exit section so as to exert both a longitudinal and divergent transverse thrusting force on the individual crimped filament of the tow.

Description

March 5, 1963 R. F. DYER Ei AL 3,079,663
METHOD AND APPARATUS FOR PRODUCING TOBACCO SMOKE FILTERS Filed May 21, 1958 2Sheets-Sheet 1 {D m k E i u l: -w -8 0 a E l E si k 2 5 w Q s g l 0 F 3E SUPPLY TOW Riclu zrdE .Dger Paul Gallagher INVENTORS moteum METHOD AND APPARATUS FOR PRODUCING TOBACCO SMOKE FILTERS 2 Sheets-Sheet 2 R. F. DYER ETAL March 5, 1963 Filed May 21, 1958 RichardRDger Paul Gallagher INVENTORS' BY APTORNm and cigar holders.
ilnited rates hatent 3,079,663 Miififill) ANB APPARATUS FGR PRQDUCING TGRAQCO SMGKE PETERS Richard F. Dyer and Paul Gallagher, Kingsport, Tenn,
assignors to Eastman Kodak Company, Rochester, N31,
a corporation of New Jersey Filed May 21, 1958, Ser. No. 735,900 11 Claims. (Cl. 28-4) This invention relates to the production of tobacco smoke filters suitable for cigarettes, pipes, and cigarette In particular this invention is concerned with an apparatus and process for treating a continuous filament crimped tow to substantially increase the filtration efiiciency thereof for the removal of nicotine, tars and aerosol particles from the tobacco smoke while at the same time elfecting a reduction in weight of filter material required and materially improving the processing of the tow into filter plugs.
In the industry at the present time a large number of tobacco smoke filters are made from continuous crimped filament tow. Such tow material is very useful for making such filter element constructions for a number of reasons. The continuous filament tow works well in automatic filter making machinery. The filaments due to their longitudinal arrangement contain elongated aligned parallel type passageways for the smoke. However, while in making filters from such tow although it has been desired to preserve to some extent the longitudinal align- -ent, it has also been desired to alter the crimp arrangement in a manner that the cn'mps are out of registry, thereby producing shoulders in the filter upon which the smoke may impinge. lso the putting of the crimps out of registry enables the obtaining of a firmer filter with lower quantities of material.
In the art prior to the instant invention, various means have been used to try and alter the filament parallelism and to randomize the location of the knees of the crimp to some extent. Such means have included mechanical vibrators or strikers, pinch rolls and the like. However, such procedures as inducing a high static electrical charge on the tow by means of rubber rollers or the alternate application of high and then low tension by passing the tow from slow speed to high speed and then to low speed rolls or the beating of the tow by mechanical heaters have certain disadvantages. The generation of a high charge of static electricity on the tow may present a hazard if any volatil matter is present or if at a later step in the process it is desired to treat the tow with certain liquids or powdered additives. The application of high tensions or the beating of the tow with vibrators not only weakens the tow and may cause breaks therein but such prior art type of treatment has destroyed to a substantial extent the effectiveness of the crimp. In other words, in the prior art one must choose between a good crimp that remains in the treated tow or a deficiency of crimp that is randomized and, therefore, in each instance the most efiicient and economical filter plug is not obtained.
Another and perhaps more serious problem encountered in the prior art type of operation is that it has not been possible to utilize tow having a particularly high degree of crimp. That is, highly crimped tow may have certain weak points at the point of crimp. Consequently, when it has been attempted to process highly cn'mped "ice tow in accordance with prior art procedures with rolls or vibrators, such attempts have not been too satisfactory because of the breaking of the highly crimped tow. Furthermore, as already briefiy mentioned, the prior art processes of beating and tensioning the tow in an elfort to break up the registry of the knees of the crimp often causes the filaments to be strained beyond the yield point. Thus the sharp angular crimp originally in the filaments is often removed because the stresses of blooming the tow are great enough to permanently remove a substantial amount of the crimp.
It is, theerfore, believed apparent that the developent of a simpler more efiective method for treating continuous filament crimped tow for use in the manufacture of tobacco smoke filters whereby the tow may be opened up, the crimps placed out of registry and yet the crimp not removed from the tow as well as filament breakage avoided represents a highly desirable result. After extended investigation we have found an improved apparatus and method whereby prior art difiiculties as above discussed may be eliminated or materially reduced.
One object of this invention is to provide an apparatus and means for processing a continuous filament crimped tow into a filter plug having a randomized filament arrangement, said filaments retaining a high .degree of their original crimp so that a filter may be obtained which has an eificiency that is relatively high to the weight of the filter material. Another object is to obtain a well opened up tow suitable for filters without substantially impairing the strength or the degree of crimp in the individual filaments. A particular object is to provide a simple and efiective apparatus arrangement for converting a dense continuous filament crimped tow into a well opened up filter tow readily susceptible to treatment with plasticizer and the like. Still another object is to make a filter from continuous filament crimped tow, which filter for a specific filament size and resistance to air flow, is more efiicient in removing tars and nicotine than prior art filament filters. A still further object is to utilize tows which have a higher crimp than heretofore tolerated with the prior art processes used in making filters from such tow. Other objects will appear hereinafter.
For a more complete understanding of our invention reference will be made to the attached drawings forming a part of the present application.
In these drawings FIG. 1 is a schematic flow diagram of the processing of the continuous filament tow into a filter plug for tobacco smoke filters.
FIG. 2 is a schematic diagram of the overall apparatus arrangement of apparatus which would be used in carrying out the process of the present invention.
FIG. 3 is a detailed cross-sectional view of the finding jet of the present invention.
FIG. 4 is a part semi-diagrammatic front end view of the jet shown in H6. 3.
Referring now to FIG. 1, as indicated above the general overall arrangement for making filters in accordance with the present invention is shown. As mentioned above, one object of the tow conditioning of filter tow is to convert the densely packed crimped tow from the supply package into a relatively fiufiy resilient flat sheet of filaments which are in a randomized state, then to establish an adhesive condition on the filaments by suitto 50 p.s.i. gauge. .high velocity gas how is produced which is evenly disjet and the rolls 6. the exit zone of the jet the filaments can thus be violentbly 7 described above.
be seen that where opening and banding and fiutfing were formerly separate steps, these steps are combined in our newprocess. The preferred system now involves feeding the towat a constant rate to a blooming jet, taking up the bloomed tow at an equal or reduced speed relative to the feed rate and then subjecting it to the action of a second blooming jet, then to the adhesive spray, and finally removing it from the tow conditioning zone at a reduced rate relative to the rate of the initial tow feed. For example, tow feed No. 1 may be at the rate of 50 y.p.m., tow feed No. 2 at the rate of 49 y.p.m. and tow .feedNo 3 at the rate of 48 y.p.m. Thus duringeach blooming process the tow isuiider conditions which promote its relaxation v 7 I v In FIG. 2. the overall'apparatus arrangement is shown in more detail. (Srimped and compacted tow 1 is with drawn from bale 2 over guides 3 and 3a by the first pair of tow feed rolls 4. The tow then passes through blooming jet 5 which is supplied with-gas at a pressure of The design of the jet is such that a tributed over the width of the rectangular-shaped jet. The action of this high velocity gas separates the individual filaments from each other and spreads the tow out into'a band or sheet of filaments. At the same time the ifilamen-ts are given a strong thrust by the air flow such that tension is generated in the tow between the rolls 4and the jet 5. The tow then passes to roll pair 6 which is driven 'atsnch a speed relative to roll pair 4 as to allow the tow to'be in arelaxed state between-the In this area and particularly in 1y agitated and vibrated such that each filament is separated from the other and the crimp knees assume completely random position relative to each other.
This cycle of blooming or debundlizing is then repeated with roll pairs 6 and 9 and jet 7. Here tension is again present between rolls 6 and jet 7 due to the in- :tiuence of the high velocity jet air on the tow. Roll pair 9 however is driven at a speed relative to roll pair 4S so that betweenjet 7 and rolls 9 therevis substantially no tension other than that required to prevent excessive sag in the tow. Also in the slack tension zone between -je't 7 and rolls 9 there is located .spray booth 8 which applies plasticizer or other material to the tow. Since the tow is relaxed and the filaments wellseparated at this point excellent distribution and even application of the plasticizer or the like on each filament is possible.
After leaving roll pair 9 the tow passes to the garniture of the cigarette making imachine'sh'own overall at 10. To insure good control over the process a common drive motorll drivesall the individual rolls and the cigarette machine 10 by chain, cog belt or other positive drive means. Interposed between the motor 11 and roll pairs '4 and 6 there are variable speed transmissions 12 and 13 such that the relative speeds of roll ;pairs 4, 6 and9' can be adjusted to establish the desired degree of relaxation in each blooming stage.
In some cases it may be desired to eliminate one blooming stageand in this case, roll pair 4 and blooming jet 5 may be omitted with the tow passing directly from guide 3a to roll pair 6. This arrangement may not bloom the 'tow as etiectivelyas the two-jet assem- However, the one jet assembly of the present invention will process the tow better than prior art procedures. Thereare other'alternatives. One
is to retain maximum crimp in the bloomed tow which may leave a few groups of unopened filaments in the tow. The other is to use somewhat higher air pressure than is required with two jets. well but may remove some slight amount of crimp from the opened filaments.
Another alternative is to utilize one flufiing jet 7 and do some tension blooming between rolls 4 and 6 with or without the aid of a beater between the two sets of rolls. This method requires a larger tow to provide a specified filter efiiciency and firmness.
These several alternatives illustrate the flexibility of the new method. The arrangement shown in FIG. 2 will give'the most efiicient filter, will require the lowest total denier, and will make the fir'mest rod using fine filaments.- However, other considerations, such as the type of filter making equipment the manufacturer already has on hand, maymake it desirable to utilize one of the above alternatives and these are included in the venturi bodyparts when assembled to the end plates 18 and 18a coact-to form elongated slot venturi entrance 22, a venturi throat 23 and a diverging venturi exit 24.-
The-two nozzle plates 16 and 17 are assembled to venturi body plates Hand 14 respectively by cap screws as indicated at 25 and 26. These nozzle plates coact with each other to form a slot-like yarn entrance passage 27 which convengesat 28. The nozzle plate 16 also co acts with venturi plate 15 to form a wedge-shaped chamber .29 which is in communication with the circular air chamber 20 via'slot passage 21. At the down stream side of this chamber 29 it converges at an angle of about fifteen degrees so that air passing through is accelerated to a high velocity at the transition between the venturi entrance 22and the venturi throat 23. Nozzle plate 17 and venturi plate 14 coact in a similar manner. As apparent from FIG. 3 that although only slot 22, airchamber 20, etc. have been referred to specifically, that on the otherside of part17 there are comparable slots, chambers and the like. Hence, further description thereof appearsto be unnecessary.
The tow enters the jet through passageway 27 and atthe tipof the nozzle 2 8, it is subjected to the impingement-ofthe high velocity sheets of air emerging from the venturi entrances. It maybe observed from inspection of these'ctional v'iew shown in FIGURE 3 of the drawings that there is a low-included angle of incidence. Also the tow is subjected to the impingement "of two'thin intersecting fiat sheets of air emerging from "the passages tormed by the mating plates 15, 16 and 14, 17 so that there are two high velocity sheets of air In the throat 23 air and emer ing from the entrances. tow are intermixed and parallelized in their direction of flow and the velocityeflect of the air generates a tension in' the tow'and a suction in'the nozzle entrance 27. This suction is strong enough to make the jet self 'threading, i;e. it will suck the tow into the jet. As the high velocity gas and tow mixture leaves the venturi throat 23 and enters the diverging throat 24, the air begins to lose velocity and expand. This action has the effect of exploding the tow and causing the filaments of the 'tow to diverge also, thus separating the filaments one from another. 'Also the filaments tend to vibrate muchin the manner of ribbons attached to the front of an electric fan. This :action further assists This will bloom the tow pressure spot.
-tions have been found to be desirable. divergence of the venturi should be from four to ten seven times the length.
ao'zaeea in separating the filaments. Recalling that between the jet and the downstream feed roll the tow is allowed to relax and Contact, the filaments also move longitudinally relative to each other so that knees of crimp in adjaccnt filaments are thrown out of phase in a completely random manner. Thus as the tow emerges from the jet the filaments are completely rearranged relative to each other as compared with their relative positions on entering the area of high velocity gas flow.
So far we have considered only the cross section of the jet. We will now consider FIG. '4. The principal purpose of FIG. 4 is to illustrate that the jet shown in FIG. 3 is not the usual round or cylindrical type of jet known in the prior art but is an elongated slot type of jet. In FIG. 4 the jet has been shown broken away on one corner to show the air chamber. The width of the jet may be, for example, 4-20 inches.
Referring in more detail to FIG. 4, it will be observed that the air inlet pipe is shown at 20 as are the nozzle plate parts 16 and 17. The opening indicated at 27 is the entrance passageway for the tow being fed to the jet. PEG. 4 also shows parts 18 and 13:: which are the end plates. An end plate is merely a metal plate bolted onto the side of the parts discussed in the description of FIG. 3 to provide an end closure for the jet. Also, the construction of the end plate is such that the spacing of the parts may be accomplished to the desired degree.
if we look in the transverse plane i.e., along the width of the jet, it will be seen that an even sheet of air flow is generated in the venturi throat from side to side of the jet. This is because air very quickly will equalize variations in pressure or velocity in a given zone or enclosure. Thus if high pressure was present in the middle of the jet it would quickly level out by transfer of air from the high pressure spot to the adjacent low Furthermore, the jet is so proportioned that the supply of air in circular chamber 20, and in the converging chamber 29 is large relative to the amount that can pass into and through the venturi.
.tinual leveling of air velocities and pressures tend to expand the tow width not only in the jet entrance but also in the venturi throat 23 and exit 24.
To obtain the most efficient use of air compatible with the most eiiective blooming of the tow certain propor- The angle of degrees with eight degrees being preferred. The length i the diverging portion 24 should be about four to ten times the length of the throat 23 and preferably about The nozzle throat length 23 should be about three times its width. The total area of the entrance slots as 22 should be about .10 times the area of the venturi throat. This latter ratio, however, is adjustable depending on the amount of suction or back pressure desired in the entrance nozzle 2. A low ratio tends to increase the suction while too high a ratio causes back pressure or blow back in the nozzle entrance 27. The width of the jet is largely determined by the width to which it is desired to spread the tow. The proportion of the area of the venturi throat to the denier of the tow is not unduly critical but values in the order of one square inch per 50,000 denier are esirable. The included angle of the venturi throat entrance formed by plates 14 and 15 is preferably 90 but may vary from 4-5 to 135.
The manner in which the tow enters and leaves the jet can be arranged to improve the blooming. In general a straight line pass is less desirable. Bringing the tow in parallel to the jet axis and removing it at about a right angle produces improved results. Also about a right angle bend in the tow as it enters the jet and 21 second approximate right angle bend as it leaves with the tow either reversing its general direction of flow or ending up proceeding in the same direction are also bene- EXAMPLE I Filter rods were made by the air blooming process of this invention using a 54,000 denier tow containing approximately 20,300 filament-s having an average size of 2.6 denier. For comparison, filter rods were made by the prior art proce lures using a 72,000 denier tow containing approximately 27,700 filaments having an average size of 2.6 denier. The physical characteristics and filtering eiiiciency of both rods are shown in the following table.
Present Prior artinvent-iontension air bloomed, bloomed, Total Denier 54, 000 72, 000
Denier per Filament. 2.6 2. 6 Crlrnps per Inch 18 16 Weight of mm, Rod, gm 74 8 Pressure Drop 90 mm. Rod, inches 1 l 11.2 11.3 Hardness of Rod 5. 7 7.8 Pressure Drop 15 mm. Tip, inches H2O. 2. 1 2. 1 Ta: Removed, percent 34 30 Tests of pressure drop, hardness, removal and weight were conducted under standard conditions using procedures and apparatus which are accepted in the cigarette industry. The hardness value is a measure of rod deformation under a specified load and a low number indicates greater firmness. It will be seen that the air blooming process requires less material, makes a firmer rod, and results in more effective filtration.
EXAMPLE II Filter rods were made by the air blooming process of the present invention using 5 d./f.70,000 denier tow. Filter rods were made by the prior art tensioning process using 5 d./f.-70,000 denier tow and also 5 d./f.- 80,000 denier tow. The comparative tests are tabulated below.
Air Tension Tension bloomed, bloomed, bloomed, Total Denier 70, 000 70, 000 80, 000
Denier per Filament 5 5 5 Crimps per Inch 7. 5 7. 5 8.0 Weight of 90 mm. Rod, gm" .37 .80 92 Pressure Drop of 90 mm. Rod, inches 1. 16 9 1. 2 Tar Removal, percent" 20 12 17 The improvement obtained by the air blooming process of the present invention is again clearly evident. The present invention gives improved crimp retention and a more inter-twined condition of the tow.
In Table A which follows there is summarized the results of tests made on a range of denier/filament sizes tow size-s, comparing filter plugs made by the jetblooming process of the present invention and filter plugs made by prior art processes. In general it will be noted that where rod weights are equal the percent tar removal or the jet bloomed yarn of the present invention is higher; or if the percent tar removal and pressure drops are equal then the weight of the jet bloomed filter plug is less.
p rases Table A I Air Jet Control Tow Plug Crimps Weight Hard- Pressure Percent rod made Example No. D./f. denier code per inch of 20 rods ness drop tar reby tenmoval No. No. 7 slon pressure pressure blooming III 2.0 54, 000 403 X7 14. 5 6. 3 11.9 33
'2. 0 54, 000 IAXP 17 13. 3 8. 1 8. 6 24 Yes. 7 2.0 72,000 lAXM 17 17. 5 8. 9 13. 3 Yes.
IV 2. 5 54, 000 40E 17 14. 9 5. 7 ll. 2
2. 5 54, 000 lAWX 17 13. 1 11.7 7.0 Yes. 2. 5 72, 000 lAW'l 17 16. 4 7.8 11.0 Yes. V 3.0 70, 000 40K 11 16. 9 5. 8 10. 8
3. 0 84, 600 lAXU ll 19. 4 6.8 11.3 Yes. VI 5. 0 000 40J 7. 5 17. 4 6. 7 6. 5
5.0 80, 000 lBAE .8. 0 l8. 5 5. 5 6. 9 Yes.
In making these plugs of Table A the filter plug making ,apparatus of FIG. 2'was operated typically in a manner as will be described in the example which follows:
EXAMPLE VII In this example the followilig pressures,
speeds and the like conditions were used.
Tow denier 57,000 Denier/filament 3 Crimps/Inch 18 Speed of roll set 4 '.:m v 54.4 pressure to jet 5 p.s.i. gauge Speed of roll set 6 y.p'.m 54.5 Air pressure to jet 7 p.s.i. gauge;. 25 Speed of roll set 9 y.p.m.. 53.4
"The tow was under no tension between jet 5 and roll "set 6 and between jet 7 and roll set 9. The speed of the roll sets 4 and -6 in this case were equal with the .jet 5 being used to flex-the tow much in the manner of a spring, but this flexing-opened up the tow, randomized the filament arrangement and the locations of the crimp x-knees.
traction oi the tow was-allowed to take place. Since crimped tow is highly elastic it is possible to have two Between roll set 6 and 9, an actual slight con pairs of rolls at equal speeds but still have the tow relaxed slightly between the jet and the output rolls since this slack or relaxed condition represents recovery of the stretching done between the input rolls and the jet input due to tension generated by the jet air flow.
While the exactmechanism by which the air jets of the present invention bloom the tow is not fully known,
pressures within the range of 5 to 100 p.-s.-i.g. may be used. The roll speeds of the various rolls may be as follows: Input teed roll set '4, 200 y.p.-m.; rolls 4 to 6 speed ratio, 1.20/1 to .7/ 1; rolls 6 to 9speed'ratio, 1.20/1 to .8/ 1.0. The total denier (T.D.) of the tow may vary bet-ween 15,000 to 100,000 and the denier per filament (D.F.')' may be .1 to 8. As pointed out above, this invention works well on highly crimped filaments. Hence, the crimp in the tow would generally not be less than 7 crimps' per inch, and may be l7 or 18 per inch. In cer- --tain filaments the crimp may be higher, say up to per inch. Whereas, in spray booth 8 for cellulose ester filaments weus'ed the plasticizer glycerol triacetate to the extent of 812% on the filaments, other plasticizers as dimethoxycthyl phthalate'or triethyl citrate may be used. Or other materials such as dextrin or gum arabic in aqueouss'olution may be applied.
and is the. measured roll surface speed. The term psi. gauge means pounds per square inch above atmospheric pressure as measured by any standard pressure recording instrument.
Although the examples given relate particulary to cellulose acetate fiber, other textile fiber tows may also ;be successfully bloomed by the method of this invention. Such materials as cellulose acetate butyrate'cellulose acetate propionate, cellulose triacetate, acrylamide polymers and copolymers', polyolefins'and polyester-fibers could also be used although the method of producing an ad- -he'sive state in the tow may be varied to use other plasticizers, adhesives,-solvents or the like which are'com patible with the particular filaments being treated.
The invention has been described in detail with particular reference to preferred embodiments thereof, but 7 from said package through the nip of a pair of feed rolls,
passing the tow from the rolls through a blooming jet having a rectangular 'divergentexit section whereby the individual filaments of the tow are violently agitated, vi-
brated, and separated by the expansion of the air in the rectangular divergent exit section-of a blooming jet so:
that the tow is opened up and the crimp put out of registry; said air flow being distinctly in the direction of movement of the tow thereby advancing the tow, withdrawing the tow from the jet by further rolls at a speed such that'thetow is not put under tension, passing this withdrawn tow through a further jet where the tow is subjected to further air treatment,'then passing the'proc- 'essed tow through a spray booth and further rolls, said last-mentioned rolls also operating at a speed so that the tow is not put under tension and conducting the processed tow from the last-mentioned rolls to filter formation; and throughout the process avoiding tensions in the tow greater than those required to support and transport the tow.
2. A process in accordance with claim 1 wherein the speed of feed to the first jetis between 30250 y.p.m.
3. The process in accordance with claim 1 wherein a the tow enters'the jets at an angle and exits at an angle.
4. The process in accordance with claim l wherein the tow fed through the process is made up of continuous cellulose acetate filaments of .1-8 denier per filament and 15,000100,000 total denier crimped to at least 17 crimps per inch.
5. A process in accordance with claim 1 wherein'the tow fed to the process is 2-5 inches wide and in the process is spread out to at least 10 inches in width.
6. In a process 'for the manufacture of tobacco smoke filter elements from continuous'crimped compacted tow the improvement step which comprises opening up the tow and putting the crimp out of registry by a substantially tensionless process comprising the passage of .the
tow .through a high velocity slot venturi jet having a rectangular divergent exit section supplied with air including contacting the compact ribbon-like crimped tow with two intersecting fiat thin streams of high velocity air at a low angle of incidence, passing both the tow and air stream through a venturi throat to further accelerate the air velocity, then causing the air to expand and lose velocity in the divergent exit portion of the venturi such that the compact crimped tow is caused to expand and bloom in width and thickness and the filaments are longitudinally displaced relative to each other whereby the crimp is put out of registry without breaking the filaments.
7. In a method of manufacturing tobacco smoke filters from crimped tow in a package form, the steps which comprise withdrawing said tow from said package through the nip of a pair of feed rolls, passing the tow from said rolls through a high velocity rectangular cross section venturi jet supplied with a gas, said jet being positioned in close proximity to said rolls and the jet being of a construction whereby the gas flows from the jet in two sheets of gas in a direction relatively parallel to the direction of movement of the tow so that the tow is advanced by the gas, and conducting said tow after it passes through such slot jet to further steps for forming a filter therefrom and throughout the process avoiding tensions in the tow greater than those required to support and transport the tow.
8. An apparatus arrangement for carrying out processes for advancing and opening tow in the manufacture of filters which comprises three pairs of feed rolls in series, said feed rolls being adapted to receive and pass through the nip of the rolls a continuous filament crimped tow, a high velocity rectangular cross section venturi jet positioned between the first and second roll pair, said jet when supplied with gas being adapted to advance and open said tow, a further jet and spray booth positioned between the second and third roll pair, and means for forming in series with the third roll pair for forming tow processed in said jets into filter elements.
9. In an apparatus for opening tow in the manufacture of filters two pairs of rolls in series, said rolls being adapted to receive and pass through the nip of the rolls a crimped tow, a high velocity rectangular cross section venturi jet having a divergent exit section adapted to be supplied with a gas positioned between the two pairs of rolls and in close proximity to the first pair of rolls, said jet being of a construction having an inlet for tow as it is received from the first pair of rolls and an exit from the jet, the internal construction of the jet being such that the gas supplied to the jet is caused to contact the tow and then is accelerated in the same direction as the movement of the tow to a high velocity, and is then caused to expand as it is discharged from the jet in the divergent exit section so as to exert both a longitudinal and divergent transverse thrusting force on the individual crimped filament of the tow.
10. An apparatus construction in accordance with claim 9 wherein the high velocity rectangular cross section venturi jet is positioned above and at an angle to the path of the .tow between the two pairs of rolls.
11. An apparatus in accordance with claim 9 wherein the high velocity rectangular cross section venturi jet is 4-20 inches wide.
References ited in the file of this patent UNITED STATES PATENTS 2,435,891 Lodge Feb. 10, 1948 2,476,582 Browne et a1 July 19, 1949 2,657,433 Merrirnan Nov. 3, 1953 2,737,688 Jackson Mar. 13, 1956 2,750,653 White June 19, 1956 2,774,680 Hackney et al Dec. 18, 1956 2,783,609 Breen Mar. 5, 1957 2,793,418 Pfau May 28, 1957 2,794,239 Crawford et a1 June 4, 1957 2,794,480 Crawford et a1 June 4, 1957 2,805,671 Hackney et al Sept. 10, 1957 2,807,862 Griset Oct. 1, 1957 2,812,569 Lawson et al Nov. 12, 1957 2,815,761 Shearer Dec. 10, 1957 2,828,752 Jackson Apr. 1, 1958 2,908,045 Stevens Oct. 13, 1959 2,914,835 Slayter et al Dec. 1, 1959 2,966,198 Wylde Dec. 27, 1960

Claims (1)

  1. 8. AN APPARATUS ARRANGEMENT FOR CARRYING OUT PROCESSES FOR ADVANCING AND OPENING TOW IN THE MANUFACTURE OF FILTERS, WHICH COMPRISES THREE PAIRS OF FEED ROLLS IN SERIES, SAID FEED ROLLS BEING ADAPTED TO RECEIVE AND PASS THROUGH THE NIP OF THE ROLLS A CONTINUOUS FILAMENT CRIMPED TOW, A HIGH VELOCITY RECTANGULAR CROSS SECTION VENTURI JET POSITIONED BETWEEN THE FIRST AND SECOND ROLL PAIR, SAID JET WHEN SUPPLIED WITH GAS BEING ADAPTED TO ADVANCE AND OPEN SAID TOW, A FURTHER JET AND SPRAY BOOTH POSITIONED BETWEEN THE SECOND AND THIRD ROLL PAIR, AND MEANS FOR FORMING IN SERIES WITH THE THIRD ROLL PAIR FOR FORMING TOW PROCESSED IN SAID JETS INTO FILTER ELEMENTS.
US736900A 1958-05-21 1958-05-21 Method and apparatus for producing tobacco smoke filters Expired - Lifetime US3079663A (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
NL239385D NL239385A (en) 1958-05-21
GB918598D GB918598A (en) 1958-05-21
NL113839D NL113839C (en) 1958-05-21
US736900A US3079663A (en) 1958-05-21 1958-05-21 Method and apparatus for producing tobacco smoke filters
ES0249365A ES249365A1 (en) 1958-05-21 1959-05-13 Method and apparatus for producing tobacco smoke filters
DE1959E0017650 DE1188998C2 (en) 1958-05-21 1959-05-16 Method and device for producing a filter material strand for tobacco smoke filters or the like.
FR795127A FR1226046A (en) 1958-05-21 1959-05-20 Method and machine for the manufacture of filters for tobacco smoke and new product obtained
CH356705D CH356705A (en) 1958-05-21 1959-05-21 Process for manufacturing a filter element for tobacco smoke, apparatus for carrying out this process and filter element obtained by this process
MY196412A MY6400012A (en) 1958-05-21 1964-12-31 Method and apparatus for producing tobacco smoke filters

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US736900A US3079663A (en) 1958-05-21 1958-05-21 Method and apparatus for producing tobacco smoke filters

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CH (1) CH356705A (en)
DE (1) DE1188998C2 (en)
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US3111440A (en) * 1960-06-16 1963-11-19 Owens Corning Fiberglass Corp Devices and methods for applying strands
US3202747A (en) * 1961-04-26 1965-08-24 Celanese Corp Method for crimping wet spun cellulose triacetate
US3255506A (en) * 1963-02-20 1966-06-14 Eastman Kodak Co Tow treatment
US3273328A (en) * 1965-02-04 1966-09-20 Bloch Godfrey Process and apparatus for making bulked filament yarns
US3352735A (en) * 1966-10-25 1967-11-14 Eastman Kodak Co Method of preparing layered nonwoven products from continuous filamentary tow materials
US3804695A (en) * 1968-06-17 1974-04-16 Celanese Corp Apparatus for making tobacco smoke filters
WO1983003267A1 (en) * 1982-03-19 1983-09-29 Eastman Kodak Co Improved pneumatic tow blooming process and apparatus
US4468845A (en) * 1982-03-19 1984-09-04 Eastman Kodak Company Jet and bustle tow blooming apparatus for a tow blooming process
US5225277A (en) * 1989-11-17 1993-07-06 Daicel Chemical Industries, Ltd. Acetate tow having high crimp modulus and manufacturing method thereof
US6253431B1 (en) 1999-10-25 2001-07-03 Celanese Acetate Llc Air opening jet apparatus
US6543106B1 (en) 1999-10-25 2003-04-08 Celanese Acetate, Llc Apparatus, method and system for air opening of textile tow and opened textile tow web produced thereby
US20050066497A1 (en) * 2003-09-26 2005-03-31 Celanese Acetate, Llc Method and apparatus for making an absorbent composite
US20050066494A1 (en) * 2003-09-26 2005-03-31 Celanese Acetate, Llc Method and apparatus for making an absorbent composite
US8623248B2 (en) 2011-11-16 2014-01-07 Celanese Acetate Llc Methods for producing nonwoven materials from continuous tow bands
US20160333507A1 (en) * 2014-01-08 2016-11-17 Daicel Corporation Method of and apparatus for manufacturing bloomed fiber material

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GB1339496A (en) * 1971-03-12 1973-12-05 British American Tobacco Co Production of tobacco-smoke filters
US4507107A (en) * 1979-11-21 1985-03-26 American Filtrona Corporation Filter manufacturing technique
JPS6087778A (en) * 1983-02-01 1985-05-17 ハウニイ−ウエルケ・ケルベル・ウント・コンパニイ・コマンデイ−トゲゼルシヤフト Method and apparatus for preparing filter rod used in tobacco processing industry
US8967155B2 (en) 2011-11-03 2015-03-03 Celanese Acetate Llc Products of high denier per filament and low total denier tow bands
DE102013202182A1 (en) * 2013-02-11 2014-08-14 Hauni Maschinenbau Ag Device for producing filters with an additive for products of the tobacco processing industry
DE102015116564A1 (en) 2015-09-30 2017-03-30 Hauni Maschinenbau Gmbh Apparatus for loading a string-shaped, continuously supplied flavor carrier with a flavoring for products of the tobacco processing industry

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US3111440A (en) * 1960-06-16 1963-11-19 Owens Corning Fiberglass Corp Devices and methods for applying strands
US3202747A (en) * 1961-04-26 1965-08-24 Celanese Corp Method for crimping wet spun cellulose triacetate
US3255506A (en) * 1963-02-20 1966-06-14 Eastman Kodak Co Tow treatment
US3273328A (en) * 1965-02-04 1966-09-20 Bloch Godfrey Process and apparatus for making bulked filament yarns
US3352735A (en) * 1966-10-25 1967-11-14 Eastman Kodak Co Method of preparing layered nonwoven products from continuous filamentary tow materials
US3804695A (en) * 1968-06-17 1974-04-16 Celanese Corp Apparatus for making tobacco smoke filters
WO1983003267A1 (en) * 1982-03-19 1983-09-29 Eastman Kodak Co Improved pneumatic tow blooming process and apparatus
DE3337007T1 (en) * 1982-03-19 1984-02-23 Eastman Kodak Co. (n.d.Ges.d. Staates New Jersey), 14650 Rochester, N.Y. Method and device for the improved pneumatic loosening of fiber tows
US4468845A (en) * 1982-03-19 1984-09-04 Eastman Kodak Company Jet and bustle tow blooming apparatus for a tow blooming process
US5225277A (en) * 1989-11-17 1993-07-06 Daicel Chemical Industries, Ltd. Acetate tow having high crimp modulus and manufacturing method thereof
US5618620A (en) * 1989-11-17 1997-04-08 Daicel Chemical Industries, Ltd. Filter rod for filtering the smoke of a cigarette
US6253431B1 (en) 1999-10-25 2001-07-03 Celanese Acetate Llc Air opening jet apparatus
US6543106B1 (en) 1999-10-25 2003-04-08 Celanese Acetate, Llc Apparatus, method and system for air opening of textile tow and opened textile tow web produced thereby
US20050066497A1 (en) * 2003-09-26 2005-03-31 Celanese Acetate, Llc Method and apparatus for making an absorbent composite
US20050066494A1 (en) * 2003-09-26 2005-03-31 Celanese Acetate, Llc Method and apparatus for making an absorbent composite
US7103946B2 (en) * 2003-09-26 2006-09-12 Celanese Acetate Llc Method and apparatus for making an absorbent composite
US7181817B2 (en) * 2003-09-26 2007-02-27 Celanese Acetate Llc Method and apparatus for making an absorbent composite
US8623248B2 (en) 2011-11-16 2014-01-07 Celanese Acetate Llc Methods for producing nonwoven materials from continuous tow bands
US20160333507A1 (en) * 2014-01-08 2016-11-17 Daicel Corporation Method of and apparatus for manufacturing bloomed fiber material
US9968492B2 (en) * 2014-01-08 2018-05-15 Daicel Corporation Method of and apparatus for manufacturing bloomed fiber material

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DE1188998C2 (en) 1965-12-30
ES249365A1 (en) 1959-11-16
MY6400012A (en) 1964-12-31
DE1188998B (en) 1965-03-11
FR1226046A (en) 1960-07-06
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NL239385A (en)
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