US5346767A - Abrasion resistant highly filled polyester compositions - Google Patents
Abrasion resistant highly filled polyester compositions Download PDFInfo
- Publication number
- US5346767A US5346767A US07/994,795 US99479592A US5346767A US 5346767 A US5346767 A US 5346767A US 99479592 A US99479592 A US 99479592A US 5346767 A US5346767 A US 5346767A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/043—Improving the adhesiveness of the coatings per se, e.g. forming primers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/046—Forming abrasion-resistant coatings; Forming surface-hardening coatings
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2367/00—Characterised by the use of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Derivatives of such polymers
- C08J2367/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2433/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L51/00—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L51/04—Compositions of graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers grafted on to rubbers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L53/02—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers of vinyl-aromatic monomers and conjugated dienes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
- C08L67/025—Polyesters derived from dicarboxylic acids and dihydroxy compounds containing polyether sequences
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L69/00—Compositions of polycarbonates; Compositions of derivatives of polycarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
- C08L79/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
- C08L79/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31507—Of polycarbonate
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31786—Of polyester [e.g., alkyd, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31942—Of aldehyde or ketone condensation product
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
Description
M.sup.z.sub.x H.sub.y P.sub.n O.sub.3n+1
______________________________________ polybutylene terephthalate 7-25 wt. % polyethylene terephthalate 3-10 wt. % aromatic polycarbonate 10-25 wt. % stabilizer 0.01-10 wt. % impact modifier 0-15 wt. % barium sulfate 40-79.99 wt. % ______________________________________
______________________________________ polybutylene terephthalate 15-30 wt. % polyethylene terephthalate 5-15 wt. % branched arom. polycarbonate 20-30 wt. % stabilizer 0.05-2 wt. % barium sulfate 30-59.95 wt. % polybutylene terephthalate 6-10 wt. % polyethylene terephthalate 5-10 wt. % polycarbonate 12-20 wt. % stabilizer 0.01-5 wt. % impact modifier 1-10 wt. % barium sulfate 59-72.99 wt. % polybutylene terephthalate 15-50 wt. % polyethylene terephthalate 5-15 wt. % polyetherimide ester 5-15 wt. % barium sulfate 50-75 wt. % ______________________________________
______________________________________ 1 2 ______________________________________ PBT.sup.a 26.3 17.1 PET.sup.b -- 10.0 BaSO.sub.4 63.5 37.0 Polycarbonate.sup.c -- 28.0 Impact -- 7.5 Modifier.sup.d Polyetherimide 10 -- ester.sup.e Antioxidant.sup.f 0.2 0.1 Diphenyl -- 0.1 isodecyl- phosphite Mold Release.sup.g -- 0.2 ______________________________________ .sup.a polybutylene terephthalate, Valox ® 315, having a melt viscosity of 7250-9000 poise; .sup.b polyethylene terephthalate having an IV of 0.57 dl/g as measured i a 60:40 mixture of phenol:tetrachloroethane at 25° C.; .sup.c polycarbonate derived from bisphenolA and 0.4 weight percent trimellitic trichloride and phosgene, said polycarbonate having an IV of 0.58 dl/g as measured in chloroform at 25° C.; .sup.d Kraton G 1651, Shell Chemical Co. an styreneethylene butylenestyrene copolymer; .sup.e polyetherimide ester of butane diol, hexane diol, (65:35 wt. %) dimethylterephthalate and poly(tetramethylene ether)glycol 2000 wt. average mol. wt. (33% by weight); .sup.f tetrakis(methylene(3,5-di-tert-butyl-4-hydroxyhydro cinnamate)methane; and .sup.g pentaerythritol tetrastearate.
TABLE 1 ______________________________________ Test Results: Abrasion Initial Water Loss (wt. 60° Adhesion Soak loss) Gloss ______________________________________ A Good >100 h 2.2 mg 15.0 A (with Good >100 h 14.1 mg 16 primer) C-1 Good >100 h 3.6 mg 45 C-2 Good >100 h 19.6 mg 13 C-3 Good >100 h 13.9 mg 49 Uncoated -- -- 56.0 mg 4 Control ______________________________________
TABLE 2 ______________________________________ Initial Water Abrasion 60° C. Coating Adhesion Soak Wt. Loss Gloss YI ______________________________________ A Good >100 h 2 mg -- -- B Fair -- -- 42 -- B (with Good >100 h 2 mg 46 10 primer) (850 h)** D Good >100 h 3 mg*** 61 31 (850 h)** Control -- -- 15 mg 7 34-49* (Uncoat- ed) ______________________________________ *range of color measured on the sample **equals hours of radiation **measured at 100 cycles
Claims (44)
M.sub.x.sup.z H.sub.y P.sub.n O.sub.3n+1
M.sub.x.sup.z H.sub.y P.sub.n O.sub.3n+1
Priority Applications (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/994,795 US5346767A (en) | 1992-12-22 | 1992-12-22 | Abrasion resistant highly filled polyester compositions |
DE1993617533 DE69317533T2 (en) | 1992-12-22 | 1993-12-10 | Process for the production of abrasion-resistant coatings for highly filled polyester compositions |
ES93309977T ES2113501T3 (en) | 1992-12-22 | 1993-12-10 | PROCEDURE FOR THE MANUFACTURE OF COMPOSITIONS OF VERY LOADED POLYESTER RESISTANT TO ABRASION. |
EP19930309977 EP0604079B1 (en) | 1992-12-22 | 1993-12-10 | Process for manufacture of abrasion resistant coatings for highly filled polyester compositions |
JP32073093A JP2634763B2 (en) | 1992-12-22 | 1993-12-21 | Abrasion resistant highly filled polyester composition |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/994,795 US5346767A (en) | 1992-12-22 | 1992-12-22 | Abrasion resistant highly filled polyester compositions |
Publications (1)
Publication Number | Publication Date |
---|---|
US5346767A true US5346767A (en) | 1994-09-13 |
Family
ID=25541055
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US07/994,795 Expired - Lifetime US5346767A (en) | 1992-12-22 | 1992-12-22 | Abrasion resistant highly filled polyester compositions |
Country Status (5)
Country | Link |
---|---|
US (1) | US5346767A (en) |
EP (1) | EP0604079B1 (en) |
JP (1) | JP2634763B2 (en) |
DE (1) | DE69317533T2 (en) |
ES (1) | ES2113501T3 (en) |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5554674A (en) * | 1995-04-07 | 1996-09-10 | General Electric Company | Flame retardant molding thermoplastics |
US5601641A (en) * | 1992-07-21 | 1997-02-11 | Tse Industries, Inc. | Mold release composition with polybutadiene and method of coating a mold core |
US5674928A (en) * | 1995-09-21 | 1997-10-07 | General Electric Company | Thermoplastic resin compositions containing a high hydroxyl polyester and a polycarbonate, and articles made therefrom |
US5979932A (en) * | 1996-08-13 | 1999-11-09 | Saint-Gobain Vitrage | Protection for the occupants of a vehicle in the event of a side impact |
US6028127A (en) * | 1994-10-14 | 2000-02-22 | Mitsubishi Rayon Co., Ltd. | Artificial marble and method for preparing it |
US6187848B1 (en) * | 1998-02-20 | 2001-02-13 | General Electric Company | Glass filled polyester compositions with improved color stability |
US20040062932A1 (en) * | 2002-08-23 | 2004-04-01 | Gallucci Robert R. | Reflective article and method for the preparation thereof |
US20040063031A1 (en) * | 2002-08-23 | 2004-04-01 | Gallucci Robert R. | Data storage medium and method for the preparation thereof |
WO2006113175A2 (en) * | 2005-04-13 | 2006-10-26 | INVISTA TECHNOLOGIES, S.à r.l. | Oxygen scavenging compositions and method of preparation |
US20080119617A1 (en) * | 2006-11-16 | 2008-05-22 | General Electric Company | Polycarbonate-polyester blends, methods of manufacture, and methods of use |
WO2008124344A1 (en) * | 2007-04-02 | 2008-10-16 | Certainteed Corporation | Photocatalytic colored roofing granules |
US7504156B2 (en) | 2004-04-15 | 2009-03-17 | Avery Dennison Corporation | Dew resistant coatings |
US20100099792A1 (en) * | 2008-10-20 | 2010-04-22 | Gallucci Robert R | Medical device using sulfonated neutralized polymers with reduced adhesion of biological fluids |
US20120246873A1 (en) * | 2011-04-01 | 2012-10-04 | Rama Konduri | Hollow articles comprising fiber-filled polyester compositions, methods of manufacture, and uses thereof |
US9200451B2 (en) | 2003-10-06 | 2015-12-01 | Certainteed Corporation | Colored roofing granules with increased solar heat reflectance, solar heat-reflective shingles, and process for producing same |
CN110734629A (en) * | 2019-10-11 | 2020-01-31 | 金旸(厦门)新材料科技有限公司 | high-impact-strength ceramic-like PET and preparation method thereof |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5674931A (en) * | 1995-04-07 | 1997-10-07 | General Electric Company | Flame retardant heavily filled thermoplastic composition |
GB9919922D0 (en) * | 1999-08-24 | 1999-10-27 | Univ Loughborough | Acoustic device |
GB0602678D0 (en) | 2006-02-09 | 2006-03-22 | Dupont Teijin Films Us Ltd | Polyester film and manufacturing process |
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US5554674A (en) * | 1995-04-07 | 1996-09-10 | General Electric Company | Flame retardant molding thermoplastics |
US5674928A (en) * | 1995-09-21 | 1997-10-07 | General Electric Company | Thermoplastic resin compositions containing a high hydroxyl polyester and a polycarbonate, and articles made therefrom |
US5979932A (en) * | 1996-08-13 | 1999-11-09 | Saint-Gobain Vitrage | Protection for the occupants of a vehicle in the event of a side impact |
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US7504156B2 (en) | 2004-04-15 | 2009-03-17 | Avery Dennison Corporation | Dew resistant coatings |
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WO2006113175A2 (en) * | 2005-04-13 | 2006-10-26 | INVISTA TECHNOLOGIES, S.à r.l. | Oxygen scavenging compositions and method of preparation |
US20080171169A1 (en) * | 2005-04-13 | 2008-07-17 | Invista North America S.A.R.L. | Oxygen Scavenging Compositions and Method of Preparation |
US20080119617A1 (en) * | 2006-11-16 | 2008-05-22 | General Electric Company | Polycarbonate-polyester blends, methods of manufacture, and methods of use |
US7655737B2 (en) | 2006-11-16 | 2010-02-02 | Sabic Innovative Plastics Ip B.V. | Polycarbonate-polyester blends, methods of manufacture, and methods of use |
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US20100099792A1 (en) * | 2008-10-20 | 2010-04-22 | Gallucci Robert R | Medical device using sulfonated neutralized polymers with reduced adhesion of biological fluids |
US9539370B2 (en) | 2008-10-20 | 2017-01-10 | Sabic Global Technologies, B.V. | Medical device using sulfonated neutralized polymers with reduced adhesion of biological fluids |
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Also Published As
Publication number | Publication date |
---|---|
EP0604079A1 (en) | 1994-06-29 |
DE69317533T2 (en) | 1998-10-15 |
DE69317533D1 (en) | 1998-04-23 |
EP0604079B1 (en) | 1998-03-18 |
JPH06279661A (en) | 1994-10-04 |
JP2634763B2 (en) | 1997-07-30 |
ES2113501T3 (en) | 1998-05-01 |
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