US6762013B2 - Thermally developable materials containing fluorochemical conductive layers - Google Patents
Thermally developable materials containing fluorochemical conductive layers Download PDFInfo
- Publication number
- US6762013B2 US6762013B2 US10/265,058 US26505802A US6762013B2 US 6762013 B2 US6762013 B2 US 6762013B2 US 26505802 A US26505802 A US 26505802A US 6762013 B2 US6762013 B2 US 6762013B2
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- US
- United States
- Prior art keywords
- silver
- pat
- materials
- photothermographic
- thermally developable
- Prior art date
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- 239000002356 single layer Substances 0.000 description 1
- 235000010378 sodium ascorbate Nutrition 0.000 description 1
- PPASLZSBLFJQEF-RKJRWTFHSA-M sodium ascorbate Substances [Na+].OC[C@@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RKJRWTFHSA-M 0.000 description 1
- 229960005055 sodium ascorbate Drugs 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 229960002920 sorbitol Drugs 0.000 description 1
- 125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000005504 styryl group Chemical group 0.000 description 1
- SEEPANYCNGTZFQ-UHFFFAOYSA-N sulfadiazine Chemical compound C1=CC(N)=CC=C1S(=O)(=O)NC1=NC=CC=N1 SEEPANYCNGTZFQ-UHFFFAOYSA-N 0.000 description 1
- 125000004964 sulfoalkyl group Chemical group 0.000 description 1
- 150000003871 sulfonates Chemical class 0.000 description 1
- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 description 1
- 125000004434 sulfur atom Chemical group 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229910002029 synthetic silica gel Inorganic materials 0.000 description 1
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 1
- 235000015523 tannic acid Nutrition 0.000 description 1
- 229920002258 tannic acid Polymers 0.000 description 1
- 229940033123 tannic acid Drugs 0.000 description 1
- 238000010345 tape casting Methods 0.000 description 1
- 229920001897 terpolymer Polymers 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- AUHHYELHRWCWEZ-UHFFFAOYSA-N tetrachlorophthalic anhydride Chemical compound ClC1=C(Cl)C(Cl)=C2C(=O)OC(=O)C2=C1Cl AUHHYELHRWCWEZ-UHFFFAOYSA-N 0.000 description 1
- 150000003536 tetrazoles Chemical class 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- VLLMWSRANPNYQX-UHFFFAOYSA-N thiadiazole Chemical compound C1=CSN=N1.C1=CSN=N1 VLLMWSRANPNYQX-UHFFFAOYSA-N 0.000 description 1
- 150000004897 thiazines Chemical class 0.000 description 1
- 150000003549 thiazolines Chemical class 0.000 description 1
- 125000005309 thioalkoxy group Chemical group 0.000 description 1
- 125000004001 thioalkyl group Chemical group 0.000 description 1
- 125000005000 thioaryl group Chemical group 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- NZFNXWQNBYZDAQ-UHFFFAOYSA-N thioridazine hydrochloride Chemical compound Cl.C12=CC(SC)=CC=C2SC2=CC=CC=C2N1CCC1CCCCN1C NZFNXWQNBYZDAQ-UHFFFAOYSA-N 0.000 description 1
- 210000000115 thoracic cavity Anatomy 0.000 description 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 150000003918 triazines Chemical class 0.000 description 1
- 125000002221 trityl group Chemical group [H]C1=C([H])C([H])=C([H])C([H])=C1C([*])(C1=C(C(=C(C(=C1[H])[H])[H])[H])[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
- INDZTCRIYSRWOH-UHFFFAOYSA-N undec-10-enyl carbamimidothioate;hydroiodide Chemical compound I.NC(=N)SCCCCCCCCCC=C INDZTCRIYSRWOH-UHFFFAOYSA-N 0.000 description 1
- 229920006163 vinyl copolymer Polymers 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229910052724 xenon Inorganic materials 0.000 description 1
- FHNFHKCVQCLJFQ-UHFFFAOYSA-N xenon atom Chemical compound [Xe] FHNFHKCVQCLJFQ-UHFFFAOYSA-N 0.000 description 1
- 229940102001 zinc bromide Drugs 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/494—Silver salt compositions other than silver halide emulsions; Photothermographic systems ; Thermographic systems using noble metal compounds
- G03C1/498—Photothermographic systems, e.g. dry silver
- G03C1/49872—Aspects relating to non-photosensitive layers, e.g. intermediate protective layers
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C1/00—Photosensitive materials
- G03C1/76—Photosensitive materials characterised by the base or auxiliary layers
- G03C1/85—Photosensitive materials characterised by the base or auxiliary layers characterised by antistatic additives or coatings
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S430/00—Radiation imagery chemistry: process, composition, or product thereof
- Y10S430/166—Toner containing
Abstract
Description
MEK | 88 g | ||
CAB 381-20 | 10.98 g | ||
Syloid 74X6000 | 0.14 g | ||
Antistatic Candidate Compound | amount indicated below | ||
TABLE I | ||||
Amount of | Keithley SER | |||
Antistatic Agent | Decay Time | Resitivity | ||
Experiment | Antistatic Agent | (g/100 g of Topcoat) | (Seconds) | (Ohms/sq) |
1-1 | ZONYL ® FSD | 0.87 | 0.01 | 3 × 109 |
1-2 | ZONYL ® FSD | 1.74 | 0.01 | 2 × 109 |
1-3 | ZONYL ® FSD | 3.48 | 0.01 | 1 × 108 |
1-4 | LODYNE ® S106A | 0.261 | 22 | 4.6 × 1014 |
1-5 | LODYNE ® S106A | 0.348 | 3.8 | 8.9 × 1011 |
1-6 | LODYNE ® S106A | 0.435 | 0.09 | 2.6 × 1010 |
1-7 | LODYNE ® S106A | 0.58 | 0.03 | 4 × 1010 |
1-8 | LODYNE ® S106A | 0.696 | 0.02 | 4 × 1010 |
C-1-9 | L-9342 | 0.435 | not conductive | 1.3 × 1014 |
C-1-10 | L-9342 | 0.87 | 1.06 | 6.7 × 1012 |
C-1-11 | L-9342 | 1.74 | 0.52 | 1.2 × 1012 |
C-1-12 | L-9342 | 2.61 | 0.68 | 6.2 × 1011 |
C-1-13 | L-9342 | 3.48 | 0.24 | 4.2 × 1011 |
C-1-14 | L-9342 | 3.48 | 0.01 | |
C-1-15 | L-9342 | 8.7 | 0.01 | |
C-1-16 | ASA-11 | 0.87 | not conductive | |
C-1-17 | ASA-11 | 1.74 | not conductive | |
C-1-18 | ASA-11 | 3.48 | 10.97 | |
C-1-19 | ASA-12 | 0.87 | not conductive | |
C-1-20 | ASA-12 | 1.74 | not conductive | |
C-1-21 | ASA-12 | 3.48 | 16.36 | |
C-1-22 | ASA-13 | 0.87 | not conductive | |
C-1-23 | ASA-13 | 1.74 | not conductive | |
C-1-24 | ASA-13 | 3.48 | 3.85 | |
C-1-25 | AVITEX DN100 | 0.87 | not conductive | |
C-1-26 | AVITEX DN100 | 1.74 | not conductive | |
C-1-27 | AVITEX DN100 | 3.48 | 7 | 1 × 1013 |
C-1-28 | AVITEX DN100 | 8.7 | 0.01 | 5 × 109 |
C-1-29 | DUPONT BA | 1.74 | 40 | 2.7 × 1013 |
C-1-30 | FLOUROLINK | 0.87 | not conductive | |
XPH613 | ||||
C-1-31 | FLOUROLINK | 1.74 | not conductive | |
XPH613 | ||||
C-1-32 | FLOUROLINK | 3.48 | not conductive | |
XPH613 | ||||
C-1-33 | FLOUROLINK | 0.87 | not conductive | |
XPH614 | ||||
C-1-34 | FLOUROLINK | 1.74 | not conductive | |
XPH614 | ||||
C-1-35 | FLOUROLINK | 3.48 | not conductive | |
XPH614 | ||||
C-1-36 | FLOUROLINK | 0.87 | not conductive | |
XPH615 | ||||
C-1-37 | FLOUROLINK | 1.74 | not conductive | |
XPH615 | ||||
C-1-38 | FLOUROLINK | 3.48 | not conductive | |
XPH615 | ||||
C-1-39 | FLOUROLINK | 0.87 | not conductive | |
XPH616 | ||||
C-1-40 | FLOUROLINK | 1.74 | not conductive | |
PH616 | ||||
C-1-41 | FLOUROLINK | 3.48 | not conductive | |
XPH616 | ||||
C-1-42 | FLOWET NMQ | 0.87 | 19.88 | 4 × 1014(a) |
C-1-43 | FLOWET NMQ | 1.74 | 0.81 | 9 × 1011(a) |
C-1-44 | FLOWET NMQ | 3.48 | 0.23 | 4 × 1011(a) |
C-1-45 | SURFONIC ® | 0.87 | not conductive | |
PE-BP2 | ||||
C-1-46 | SURFONIC ® | 1.74 | not conductive | |
PE-BP2 | ||||
C-1-47 | LODYNE ® S100 | 26.1 | not conductive | |
C-1-48 | LODYNE ® S100 | 52.2 | not conductive | |
C-1-49 | LODYNE ® S103A | 26.1 | not conductive | |
C-1-50 | LODYNE ® S103A | 52.2 | not conductive | |
C-1-51 | MODIPER ® F600 | 0.87 | not conductive | |
C-1-52 | MODIPER ® F600 | 1.74 | not conductive | |
C-1-53 | MODIPER ® F600 | 3.48 | not conductive | |
C-1-54 | MODIPER ® F600 | 8.7 | not conductive | |
C-1-55 | MODIPER ® F600 | 1.74 | not conductive | |
C-1-56 | MODIPER ® F600 | 3.48 | not conductive | |
C-1-57 | MODIPER ® F600 | 8.7 | not conductive | |
C-1-58 | MODIPER ® FS700 | 0.87 | not conductive | |
C-1-59 | POLYFOX | 0.87 | not conductive | |
C-1-60 | POLYFOX | 1.74 | not conductive | |
C-1-61 | POLYFOX | 3.48 | not conductive | |
C-1-62 | SURFLON ® S393 | 0.87 | not conductive | |
C-1-63 | SURFLON ® S393 | 3.48 | not conductive | |
C-1-64 | SURFLON ® S393 | 8.7 | not conductive | |
C-1-65 | SURFLON ® S393 | 21.75 | 22.45 | |
C-1-66 | SURFLON ® S8405 | 0.87 | not conductive | |
C-1-67 | SURFLON ® S8405 | 3.48 | not conductive | |
C-1-68 | SURFLON ® S8405 | 8.7 | not conductive | |
C-1-69 | SURFLON ® S8405 | 43.5 | 60 | |
C-1-70 | ZONYL ® 8740 | 0.87 | not conductive | |
C-1-71 | ZONYL ® 8740 | 8.7 | not conductive | |
C-1-72 | ZONYL ® 8740 | 87.0 | not conductive | |
C-1-73 | ZONYL ® FS-62 | 1.74 | not conductive | |
C-1-74 | ZONYL ® FS-62 | 3.48 | 59 | |
C-1-75 | ZONYL ® FS-62 | 8.7 | 0.01 | |
C-1-76 | ZONYL ® FS-62 | 17.4 | 0.01 | |
C-1-77 | ZONYL ® FSA | 0.87 | not conductive | |
C-1-78 | ZONYL ® FSA | 8.7 | not conductive | |
C-1-79 | ZONYL ® FSA | 87.0 | not conductive | |
C-1-80 | ZONYL ® FSG | 0.87 | not conductive | |
C-1-81 | ZONYL ® FSG | 3.48 | not conductive | |
C-1-82 | ZONYL ® FSG | 8.7 | not conductive | |
C-1-83 | ZONYL ® FSJ | 0.87 | 43.6 | |
C-1-84 | ZONYL ® FSJ | 1.74 | 5.08 | |
C-1-85 | ZONYL ® FSJ | 1.74 | 4.92 | |
C-1-86 | ZONYL ® FSJ | 3.48 | 1.06 | |
C-1-87 | ZONYL ® FSJ | 8.7 | 0.25 | |
C-1-88 | ZONYL ® FSJ | 17.4 | 0.02 | |
C-1-89 | ZONYL ® FSK | 0.87 | not conductive | |
C-1-90 | ZONYL ® FSK | 1.74 | 41 | |
C-1-91 | ZONYL ® FSK | 3.48 | 8.1 | |
C-1-92 | ZONYL ® FSK | 8.7 | 3.4 | |
C-1-93 | ZONYL ® FSK | 17.4 | 0.71 | |
C-1-94 | ZONYL ® FSN100 | 0.87 | not conductive | |
C-1-95 | ZONYL ® FSN100 | 1.74 | not conductive | |
C-1-96 | ZONYL ® FSN100 | 3.48 | not conductive | |
C-1-97 | ZONYL ® FSO | 0.87 | not conductive | |
C-1-98 | ZONYL ® FSO | 8.7 | 2.65 | |
C-1-99 | ZONYL ® FSO | 17.4 | 0.05 | |
C-1-100 | ZONYL ® FSO | 3.48 | not conductive | |
C-1-101 | ZONYL ® FSP | 0.87 | not conductive | |
C-1-102 | ZONYL ® FSP | 8.7 | not conductive | |
C-1-103 | ZONYL ® TLF 9515 | 0.87 | 48 | 9 × 1014 |
C-1-104 | ZONYL ® TLF 9515 | 3.48 | 36 | 1 × 1013 |
C-1-105 | ZONYL ® TLF 9517 | 0.87 | 27 | 1 × 1013 |
C-1-106 | ZONYL ® TLF 9517 | 3.48 | 1.14 | 1.5 × 1012 |
C-1-107 | ZONYL ® TLF 9520 | 0.87 | 1.3 × 1016 | |
C-1-108 | ZONYL ® UR | 0.87 | 4.92 | 6 × 1012 |
C-1-109 | ZONYL ® UR | 1.74 | 2 | 3 × 1012 |
C-1-110 | ZONYL ® UR | 3.48 | 0.61 | 1 × 1012 |
(a)Experimental samples containing Flowet NMQ displayed severe surface smearing and developed a greasy soap-like deposit on their surface making them unusable in a thermally developable construction. |
MEK | 61.6 g | ||
Methanol | 26.4 g | ||
CAB 381-20 | 10.98 g | ||
Syloid 74X6000 | 0.14 g | ||
Active Antistatic Material | amount indicated below. | ||
TABLE II | ||||
Amount of | ||||
Antistatic | Keithley | |||
Agent | Decay | SER | ||
Experi- | (g/100 g of | Time | Resistivity | |
ment | Antistatic Agent | Topcoat) | (Seconds) | (Ohms/sq) |
2-1 | ZONYL ® FSD | 0.043 | not | >1 × 1016 |
conductive | ||||
2-2 | ZONYL ® FSD | 0.087 | not | >1 × 1016 |
conductive | ||||
2-3 | ZONYL ® FSD | 0.13 | not | >1 × 1016 |
conductive | ||||
2-4 | ZONYL ® FSD | 0.174 | 0.57 | 3 × 1014 |
2-5 | ZONYL ® FSD | 0.261 | 0.18 | 1 × 1011 |
2-6 | ZONYL ® FSD | 0.348 | 0.07 | 4 × 1010 |
2-7 | ZONYL ® FSD | 0.435 | 0.03 | 4 × 1010 |
2-8 | ZONYL ® FSD | 0.522 | 0.06 | 4 × 1010 |
2-9 | ZONYL ® FSD | 0.87 | 0.01 | 5 × 109 |
2-10 | LODYNE ® 106A | 0.261 | 0.03 | 7.6 × 1010 |
2-11 | LODYNE ® 106A | 0.348 | 0.03 | 4.4 × 1010 |
2-12 | LODYNE ® 106A | 0.435 | 0.03 | 2.4 × 1010 |
2-13 | LODYNE ® 106A | 0.522 | 0.02 | 2.0 × 1010 |
2-14 | LODYNE ® 106A | 0.609 | 0.01 | 1.6 × 1010 |
TABLE III | ||||||
Amount of | ||||||
Antistatic | Antistatic | Antistatic Agent | % Fade | % Fade | % Fade | |
Experiment | Formulation | Agent | (g/100 g of Topcoat) | 1 Day | 2 Days | 7 Day |
3-1 | I | ZONYL ® FSD | 0.405 | 6.29 | 10.18 | 25.1 |
Control A | I | None | 0 | 2.58 | 5.48 | 14.87 |
Control B | I | L-9342 | 0.87 | 41.18 | 71.7 | 98.5 |
3-2 | II | ZONYL ® FSD | 0.405 | 4.46 | 10.43 | 30.6 |
Control A | II | None | 0 | 2.58 | 1.32 | 8.5 |
Control B | II | L-9342 | 0.87 | 23.8 | 40.48 | 79.8 |
MEK | 86.10 weight % | ||
Vinyl sulfone | 0.35 weight % | ||
Benzotriazole | 0.27 weight % | ||
Silica | 0.21 weight % | ||
ACRYLOID ® A-21 | 0.47 weight % | ||
CAB 171-15S | 12.25 weight % | ||
Antihalation dye* | 0.21 weight % | ||
Ethyl-2-cyano-3-oxobutanoate | 0.23 weight % | ||
*This compound is 1,3-bis[2,3-dihydro-2,2-bis[[(1-oxohexyl)-oxy]methyl]-1H-perimidin-6-yl]-2,4-dihydroxy-, bis (inner salt). |
TABLE IV | ||
Keithley SER Resistivity (Ohms/sq) |
70° F. | 70° F. | 70° F. | |||
Ex- | Antistatic | Days of | (52.2° C.) | (21.2° C.) | (52.2° C.) |
ample | Agent | Keeping | 20% RH | 50% RH | 80% RH |
1-1 | ZONYL ® | 0 | 4.70 × | 5.05 × 109 | 1.82 × 109 |
FSD | 1010 | ||||
1-2 | ZONYL ® | 9 | 5.15 × | 5.05 × 109 | 2.2 × 109 |
FSD | 1010 | ||||
1-3 | ZONYL ® | 65 | 3.83 × | 5.75 × 109 | 1.9 × 109 |
FSD | 1010 | ||||
1-4 | ZONYL ® | 160 | 3.23 × | 5.75 × 109 | 1.82 × 109 |
FSD | 1010 | ||||
C-1-5 | L-9342 | 0 | 5.62 × | 6.94 × 1011 | 1.49 × 1011 |
1012 | |||||
C-1-6 | L-9342 | 9 | 8.02 × | 2.49 × 1012 | 3.77 × 1011 |
1012 | |||||
C-1-7 | L-9342 | 65 | 1.02 × | 2.5 × 1012 | 8.86 × 1011 |
1013 | |||||
C-1-8 | L-9342 | 160 | 2.39 × | 8.42 × 1012 | 2.96 × 1012 |
1013 | |||||
TABLE V | ||
Decay Times (seconds) |
70° F. | 70° F. | 70° F. | |||
Ex- | Antistatic | Days of | (52.2° C.) | (21.2° C.) | (52.2° C.) |
ample | Agent | Keeping | 20% RH | 50% RH | 80% RH |
1-1 | ZONYL ® FSD | 0 | 0.03 | — | — |
1-2 | ZONYL ® FSD | 9 | 0.03 | .01 | .01 |
1-3 | ZONYL ® FSD | 65 | 0.02 | .01 | .01 |
1-4 | ZONYL ® FSD | 160 | 0.02 | .01 | .01 |
C-1-5 | L-9342 | 0 | 2.76 | — | — |
C-1-6 | L-9342 | 9 | 3.53 | .06 | .011 |
C-1-7 | L-9342 | 65 | 5.13 | 1.90 | 0.25 |
C-1-8 | L-9342 | 160 | 9.15 | 7.81 | 1.76 |
TABLE VI | ||||
Keithley SER | ||||
Antistatic | Days of | Decay Time | Resistivity | |
Example | Agent | Keeping | (Seconds) | (Ohms/sq) |
2-1 | ZONYL ® FSD | 0 day | 0.03 | 1 × 1011 |
2-2 | ZONYL ® FSD | 4 day | 0.11 | 2 × 1011 |
2-3 | ZONYL ® FSD | 8 day | 0.12 | 2 × 1011 |
2-4 | ZONYL ® FSD | 14 day | 0.15 | 2.5 × 1011 |
C-2-5 | L-9342 | 0 day | 3.05 | 8 × 1012 |
C-2-6 | L-9342 | 4 day | 12 | 2 × 1013 |
C-2-7 | L-9342 | 8 day | 32 | 7 × 1013 |
C-2-8 | L-9342 | 14 day | 83 | 1 × 1014 |
MEK | 75.5% | ||
Silver Behenate | 24.0% | ||
PIOLOFORM ® BL-16 | 0.5% | ||
MEK | 44.8 g | ||
CAB 171-15S | 51.10 g | ||
PARALOID A-21 | 1.36 g | ||
DC 550 | 1.65 g | ||
SERVOXYL ® VPAZ 100 | 0.22 g | ||
ALBACAR 5970 | 0.15 g | ||
TABLE VII | ||||
Keithley SER | ||||
Antistatic | Days of | Decay Time | Resistivity | |
Example | Agent | Keeping | (Seconds) | (Ohms/sq) |
3-1 | ZONYL ® FSD | 0 | 0.03 | 6.6 × 1010 |
3-2 | ZONYL ® FSD | 4 | 0.06 | 6.8 × 1010 |
3-3 | ZONYL ® FSD | 8 | 0.07 | 6.4 × 1010 |
3-4 | ZONYL ® FSD | 14 | 12.03 | 1.91 × 1013 |
TABLE VIII | ||||
Keithley SER | ||||
Antistatic | Days of | Decay Time | Resistivity | |
Example | Agent | Keeping | (Seconds) | (Ohms/sq) |
3-5 | ZONYL ® FSD | 0 | 0.03 | 3.3 × 1010 |
3-6 | ZONYL ® FSD | 4 | 0.07 | 6.4 × 1010 |
3-7 | ZONYL ® FSD | 8 | 0.09 | 8.6 × 1010 |
3-8 | ZONYL ® FSD | 14 | 0.54 | 8.9 × 1011 |
Claims (27)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/265,058 US6762013B2 (en) | 2002-10-04 | 2002-10-04 | Thermally developable materials containing fluorochemical conductive layers |
EP03077977A EP1406120A3 (en) | 2002-10-04 | 2003-09-22 | Thermally developable materials containing fluorochemical conductive layers |
JP2003347088A JP2004126599A (en) | 2002-10-04 | 2003-10-06 | Heat developable material, photothermographic material and method for forming image |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/265,058 US6762013B2 (en) | 2002-10-04 | 2002-10-04 | Thermally developable materials containing fluorochemical conductive layers |
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US20040067454A1 US20040067454A1 (en) | 2004-04-08 |
US6762013B2 true US6762013B2 (en) | 2004-07-13 |
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US10/265,058 Expired - Fee Related US6762013B2 (en) | 2002-10-04 | 2002-10-04 | Thermally developable materials containing fluorochemical conductive layers |
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EP (1) | EP1406120A3 (en) |
JP (1) | JP2004126599A (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050042553A1 (en) * | 2003-08-21 | 2005-02-24 | 3M Innovative Properties Company | Phototool coating |
US20050158528A1 (en) * | 2003-12-26 | 2005-07-21 | Hiroshi Sasaki | Wiring substrate |
US20050233270A1 (en) * | 2004-04-16 | 2005-10-20 | Eastman Kodak Company | Photothermographic materials with improved natural age keeping |
US7153636B1 (en) | 2005-08-01 | 2006-12-26 | Eastman Kodak Company | Thermally developable materials with abrasion-resistant backside coatings |
WO2017123444A1 (en) | 2016-01-15 | 2017-07-20 | Carestream Health, Inc. | Method of preparing silver carboxylate soaps |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7371709B2 (en) | 2005-09-28 | 2008-05-13 | Kumars Sakizadeh | Thermally developable materials with backside antistatic layer |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050042553A1 (en) * | 2003-08-21 | 2005-02-24 | 3M Innovative Properties Company | Phototool coating |
US7189479B2 (en) * | 2003-08-21 | 2007-03-13 | 3M Innovative Properties Company | Phototool coating |
US20070128557A1 (en) * | 2003-08-21 | 2007-06-07 | 3M Innovative Properties Company | Phototool coating |
US20050158528A1 (en) * | 2003-12-26 | 2005-07-21 | Hiroshi Sasaki | Wiring substrate |
US20050233270A1 (en) * | 2004-04-16 | 2005-10-20 | Eastman Kodak Company | Photothermographic materials with improved natural age keeping |
US7052819B2 (en) * | 2004-04-16 | 2006-05-30 | Eastman Kodak Company | Photothermographic materials with improved natural age keeping |
US7153636B1 (en) | 2005-08-01 | 2006-12-26 | Eastman Kodak Company | Thermally developable materials with abrasion-resistant backside coatings |
WO2017123444A1 (en) | 2016-01-15 | 2017-07-20 | Carestream Health, Inc. | Method of preparing silver carboxylate soaps |
Also Published As
Publication number | Publication date |
---|---|
EP1406120A3 (en) | 2004-08-18 |
EP1406120A2 (en) | 2004-04-07 |
US20040067454A1 (en) | 2004-04-08 |
JP2004126599A (en) | 2004-04-22 |
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CH | sented by Structure I-1 below wherein R, comprises 6 |
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