US8871277B2 - Particulate wood preservative and method for producing the same - Google Patents
Particulate wood preservative and method for producing the same Download PDFInfo
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- US8871277B2 US8871277B2 US13/777,649 US201313777649A US8871277B2 US 8871277 B2 US8871277 B2 US 8871277B2 US 201313777649 A US201313777649 A US 201313777649A US 8871277 B2 US8871277 B2 US 8871277B2
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D15/00—Woodstains
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N2300/00—Combinations or mixtures of active ingredients covered by classes A01N27/00 - A01N65/48 with other active or formulation relevant ingredients, e.g. specific carrier materials or surfactants, covered by classes A01N25/00 - A01N65/48
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/005—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising microparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/007—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process employing compositions comprising nanoparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/22—Compounds of zinc or copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/32—Mixtures of different inorganic impregnating agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/52—Impregnating agents containing mixtures of inorganic and organic compounds
Abstract
Description
TABLE I |
Exemplary Formulations To Precipitate |
Mg/Zn-Stabilized Copper Hydroxide |
Formulation | Parts Zinc | Parts Magnesium | Parts Copper | ||
1 | 0.5 | 0.5 | 22.5 | ||
2 | 0.75 | 0.75 | 22.5 | ||
3 | 1.5 | 1.5 | 22.5 | ||
4 | 2.5 | 1.0 | 22.5 | ||
5 | 2.5 | 2.5 | 22.5 | ||
TABLE 2 |
Average Particle size (from Stokes Law Settling) Before |
and After Milling With 0.5 mm Zirconium Silicate |
Median | Particle Size Distribution Data |
PS | % <10 | % <1 | % <0.4 | % <0.2 |
Description | (microns) | um | um | um | um | Ref: |
Copper Hydroxide, | After | <0.2 | 99.0 | 96.7 | 94.6 | 84.9 | V.216.69 |
Dettwiler | Treat | ||||||
Copper Hydroxide, | Before | <0.2 | 99.7 | 84.0 | 63.9 | 57.1 | V.216.69 |
Dettwiler | |||||||
Copper Hydroxide, | After | 0.30 | 99.7 | 95.4 | 21.7 | — | V.216.74 |
Furness | Treat | ||||||
Copper Hydroxide, | Before | 2.5 | 99.6 | 8.7 | — | — | V.216.74 |
Furness | |||||||
Copper Carbonate | After | <0.2 | 99.1 | 97.2 | 96.9 | 87.3 | V.216.77 |
Treat | |||||||
Copper Carbonate | Before | 3.4 | 98.0 | 1.2 | — | — | V.216.77 |
Tribasic Copper Sulfate | After | <0.2 | 99.5 | 96.4 | 90.5 | 55.1 | V.216.85 |
Treat | |||||||
Tribasic Copper Sulfate | Before | 6.2 | 69.5 | 16.5 | — | — | V.216.85 |
Copper Oxychloride | After | 0.38 | 99.4 | 93.9 | 63.2 | — | V.218.7 |
Treat | |||||||
Copper Oxychloride | Before | 3.3 | 98.5 | 2.8 | — | — | V.218.7 |
Description of | 96 hr. | 240 hr. | |
Ex. | Preservative System | ration to CCA | ration to CCA |
A | 3% TEB and basic copper | 0.67:1 | 0.51:1 |
| |||
C | |||
3% TEB and copper MEA | 5.2:1 | 3.85:1 | |
carbonate (comparative) | |||
|
3% TEB and basic copper | 0.54:1 | 0.46:1 |
carbonate particulates | |||
with sodium bicarbonate | |||
buffer | |||
E | basic copper carbonate | 0.77:1 | 0.63:1 |
| |||
F | |||
3% TEB and copper hydroxide | 0.2:1 | 0.19:1 | |
with Zn and Mg particulates | |||
G | 5% TEB and copper hydroxide | 1.0:1 | 0.88:1 |
particulates modified with | |||
| |||
H | |||
3% TEB and tribasic copper | 0.96:1 | 0.88:1 | |
sulfate particulates | |||
I | 3% TEB and copper oxy | 1.4:1 | 1.17:1 |
chloride particulates | |||
Claims (28)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US13/777,649 US8871277B2 (en) | 2003-06-17 | 2013-02-26 | Particulate wood preservative and method for producing the same |
US14/447,338 US20150144027A1 (en) | 2003-06-17 | 2014-07-30 | Particulate wood preservative and method for producing the same |
Applications Claiming Priority (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US47882503P | 2003-06-17 | 2003-06-17 | |
US47882703P | 2003-06-17 | 2003-06-17 | |
US47882203P | 2003-06-17 | 2003-06-17 | |
US47882003P | 2003-06-17 | 2003-06-17 | |
US57153504P | 2004-05-17 | 2004-05-17 | |
US10/868,967 US20040258768A1 (en) | 2003-06-17 | 2004-06-17 | Particulate wood preservative and method for producing same |
US12/458,522 US8409627B2 (en) | 2003-06-17 | 2009-07-15 | Particulate wood preservative and method for producing the same |
US13/777,649 US8871277B2 (en) | 2003-06-17 | 2013-02-26 | Particulate wood preservative and method for producing the same |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US12/458,522 Continuation US8409627B2 (en) | 2003-06-17 | 2009-07-15 | Particulate wood preservative and method for producing the same |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US14/447,338 Continuation US20150144027A1 (en) | 2003-06-17 | 2014-07-30 | Particulate wood preservative and method for producing the same |
Publications (2)
Publication Number | Publication Date |
---|---|
US20130230575A1 US20130230575A1 (en) | 2013-09-05 |
US8871277B2 true US8871277B2 (en) | 2014-10-28 |
Family
ID=34084833
Family Applications (4)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/868,967 Abandoned US20040258768A1 (en) | 2003-06-17 | 2004-06-17 | Particulate wood preservative and method for producing same |
US12/458,522 Active 2025-08-07 US8409627B2 (en) | 2003-06-17 | 2009-07-15 | Particulate wood preservative and method for producing the same |
US13/777,649 Active US8871277B2 (en) | 2003-06-17 | 2013-02-26 | Particulate wood preservative and method for producing the same |
US14/447,338 Abandoned US20150144027A1 (en) | 2003-06-17 | 2014-07-30 | Particulate wood preservative and method for producing the same |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US10/868,967 Abandoned US20040258768A1 (en) | 2003-06-17 | 2004-06-17 | Particulate wood preservative and method for producing same |
US12/458,522 Active 2025-08-07 US8409627B2 (en) | 2003-06-17 | 2009-07-15 | Particulate wood preservative and method for producing the same |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US14/447,338 Abandoned US20150144027A1 (en) | 2003-06-17 | 2014-07-30 | Particulate wood preservative and method for producing the same |
Country Status (15)
Country | Link |
---|---|
US (4) | US20040258768A1 (en) |
EP (1) | EP1651401B1 (en) |
JP (1) | JP4971790B2 (en) |
CN (1) | CN1835830A (en) |
AU (2) | AU2004257148A1 (en) |
BR (1) | BRPI0411340B1 (en) |
CA (1) | CA2530044C (en) |
DE (1) | DE602004022171D1 (en) |
DK (1) | DK1651401T3 (en) |
ES (1) | ES2329044T3 (en) |
HK (1) | HK1088862A1 (en) |
MX (1) | MXPA05013850A (en) |
NZ (1) | NZ544699A (en) |
PL (1) | PL1651401T3 (en) |
WO (1) | WO2005007368A2 (en) |
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US20040258768A1 (en) | 2004-12-23 |
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