USH1949H1 - Hydrogenated elastomer primed polyolefin film - Google Patents
Hydrogenated elastomer primed polyolefin film Download PDFInfo
- Publication number
- USH1949H1 USH1949H1 US08/595,094 US59509496A USH1949H US H1949 H1 USH1949 H1 US H1949H1 US 59509496 A US59509496 A US 59509496A US H1949 H USH1949 H US H1949H
- Authority
- US
- United States
- Prior art keywords
- block copolymer
- styrene
- process according
- weight percent
- film
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/50—Adhesives in the form of films or foils characterised by a primer layer between the carrier and the adhesive
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/043—Improving the adhesiveness of the coatings per se, e.g. forming primers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2323/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
- C08J2323/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2453/00—Characterised by the use of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2423/00—Presence of polyolefin
- C09J2423/006—Presence of polyolefin in the substrate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2453/00—Presence of block copolymer
- C09J2453/003—Presence of block copolymer in the primer coating
Abstract
Description
TABLE 1 | ||||||||
Materials | A | B | C | D | E | F | G | H |
G16521 | 7 | 7 | 0 | 0 | 0 | 0 | 0 | 0 |
FG19012 | 0 | 0 | 7 | 7 | 0 | 0 | 0 | 0 |
B52-53 | 0 | 0 | 0 | 0 | 7 | 7 | 0 | 0 |
Bayprene4 | 0 | 0 | 0 | 0 | 0 | 0 | 3.5 | 3.5 |
Nipol5 | 0 | 0 | 0 | 0 | 0 | 0 | 3.5 | 3.5 |
Toluene6 | 93 | 0 | 93 | 0 | 93 | 0 | 93 | 0 |
XPS68477 | 0 | 93 | 0 | 93 | 0 | 93 | 0 | 93 |
1KRATON ® R G1652 elastomeric ABA block copolymer; 7,200 MW polymerized styrene end-blocks; mid-block hydrogenated 1-2 addition polymerization butadiene; 28 weight % styrene SEBS | ||||||||
2KRATON ® G1652 maleated to give about 2 weight percent functional component. | ||||||||
3KRATON ® G1652 maleated to give about 5 weight percent functional component. | ||||||||
4Neoprene rubber. | ||||||||
5Neoprene rubber. | ||||||||
6Aromatic solvent. | ||||||||
7Developmental non-aromatic hydrocarbon containing predominantly methylcyclohexane and other aliphatic hydrocarbons. |
TABLE 2 | ||||||
avg1 | ||||||
I.D. | (pli) | solvent | primer | % primer fail4 | ||
A(tsu)2 | 4.36 | TOL | G1652 | 3 | ||
A(tsd)3 | 4.18 | TOL | G1652 | 30 | ||
B(tsu) | 4.34 | XPS | G1652 | |||
B(tsd) | 4.06 | XPS | G1652 | |||
C(tsu) | 5.12 | TOL | FG1901 | 0 | ||
C(tsd) | 5.12 | TOL | FG1901 | 0 | ||
D(tsu) | 4.34 | XPS | FG1901 | 1 | ||
D(tsd) | 4.12 | XPS | FG1901 | 0 | ||
E(tsu) | 4.2 | TOL | B52-5 | 0 | ||
E(tsd) | 4.9 | TOL | B52-5 | |||
F(tsu) | 4.7 | XPS | B52-5 | |||
F(tsd) | 5 | XPS | B52-5 | |||
G(tsu) | 2.04 | TOL | NEOPR | 70 | ||
G(tsd) | 2.28 | TOL | NEOPR | 38 | ||
H5 | XP | NEOPR | ||||
1An average of the five “T” peel Instron readings (pli). A high reading indicates good adhesion of the primer to the biaxially-oriented polypropylene backing, and a low number indicates poor adhesion. The actual reading on the ½-inch wide film was multiplied by 2 to give the number reported. | ||||||
2Indicates treated side up, i.e. this tests the adhesion of the primer to the 30 micron corona discharge-treated surface. | ||||||
3Treated side down; this tests the adhesion of the primer to the side of the biaxially oriented polypropylene film not corona discharge treated. | ||||||
4Against polypropylene film | ||||||
5Could not be run since material would not dissolve in non-aromatic solvent. |
D1107 | 100 | parts | ||
Wingtack ® 95 | 100 | parts | ||
IRGANOX ® 1010 | 1 | part | ||
TABLE 3 | |||||||||
Materials | A | B | C | D | E | F | G8 | ||
G16521 | 7 | 7 | |||||||
FG19012 | 7 | 7 | |||||||
B52-53 | 7 | ||||||||
Bayprene4 | 3.5 | ||||||||
Nipol5 | 3.5 | ||||||||
Toluene6 | 93 | — | 93 | — | 93 | 93 | |||
XPS 68477 | — | 93 | — | 93 | — | — | |||
1KRATON ® R G1652 elastomeric ABA block copolymer; 28% styrene SEBS; mid-block hydrogenated 1-2 addition polymerization butadiene | |||||||||
2KRATON ® G1652 maleated to give about 2 weight percent functional component. | |||||||||
3KRATON ® G1652 maleated to give about 5 weight percent functional component. | |||||||||
4Neoprene rubber. | |||||||||
5Neoprene rubber. | |||||||||
6Aromatic solvent. | |||||||||
7Commercial non-aromatic hydrocarbon containing predominantly methyl-cyclohexane. | |||||||||
8No primer. |
TABLE 4 |
“T” Peel Results |
avg1 | ||||
(pli) | solvent | primer | ||
A (treated, 40 dynes) | 3.9 | TOL | G1652 | ||
A (treated, 56 dynes) | 2.9 | TOL | G1652 | ||
A (not treated) | 4.3 | TOL | G1652 | ||
B (treated, 40 dynes) | 4.1 | XPS | G1652 | ||
B (treated, 56 dynes) | 3.8 | XPS | G1652 | ||
B (not treated) | 5.6 | XPS | G1652 | ||
C (treated, 40 dynes) | 5.8 | TOL | FG1901 | ||
C (treated, 56 dynes) | 5.4 | TOL | FG1901 | ||
C (not treated) | 5.7 | TOL | FG1901 | ||
D (treated, 40 dynes) | 5.4 | XPS | FG1901 | ||
D (treated, 56 dynes) | 5.7 | XPS | FG1901 | ||
D (not treated) | 4.3 | XPS | FG1901 | ||
E (treated, 40 dynes) | 5.5 | TOL | B52-5 | ||
E (treated, 56 dynes) | 5.8 | TOL | B52-5 | ||
E (not treated) | 3.3 | TOL | B52-5 | ||
F (treated, 40 dynes) | 3 | TOL | neopr | ||
F (treated, 56 dynes) | 3 | TOL | neopr | ||
F (not treated) | 2.9 | TOL | neopr | ||
G (treated, 40 dynes) | 5.6 | NA | None | ||
1An average of the five “T” peel Instron readings as in Example 1. A high reading indicates good adhesion of the primer to the biaxially-oriented polypropylene backing chemical and a low number indicates poor adhesion. |
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/595,094 USH1949H1 (en) | 1996-02-01 | 1996-02-01 | Hydrogenated elastomer primed polyolefin film |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/595,094 USH1949H1 (en) | 1996-02-01 | 1996-02-01 | Hydrogenated elastomer primed polyolefin film |
Publications (1)
Publication Number | Publication Date |
---|---|
USH1949H1 true USH1949H1 (en) | 2001-03-06 |
Family
ID=24381706
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US08/595,094 Abandoned USH1949H1 (en) | 1996-02-01 | 1996-02-01 | Hydrogenated elastomer primed polyolefin film |
Country Status (1)
Country | Link |
---|---|
US (1) | USH1949H1 (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050016675A1 (en) * | 1999-06-02 | 2005-01-27 | Bain Peter Stewart | Adhesive composition comprising thermoexpandable microcapsules |
Citations (31)
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---|---|---|---|---|
US3239478A (en) * | 1963-06-26 | 1966-03-08 | Shell Oil Co | Block copolymer adhesive compositions and articles prepared therefrom |
US3565247A (en) * | 1968-10-21 | 1971-02-23 | Minnesota Mining & Mfg | Pressure-sensitive adhesive tape product |
US3577398A (en) | 1966-06-09 | 1971-05-04 | Goodyear Tire & Rubber | Synthetic resin |
USRE27145E (en) | 1969-05-20 | 1971-06-22 | Side-chain | |
US3753936A (en) * | 1970-02-18 | 1973-08-21 | Phillips Petroleum Co | Branched rubbery block copolymer adhesive |
US3879248A (en) * | 1971-05-17 | 1975-04-22 | Donald O Kest | Method of bonding using urethane base pressure sensitive adhesives |
US3917607A (en) * | 1971-09-22 | 1975-11-04 | Shell Oil Co | Block copolymer adhesive compositions |
US3932327A (en) * | 1973-02-05 | 1976-01-13 | Phillips Petroleum Company | Adhesive compositions |
US3984369A (en) * | 1975-05-15 | 1976-10-05 | Shell Oil Company | Sealant |
US4062995A (en) * | 1976-06-23 | 1977-12-13 | Johnson & Johnson | Reticular web |
US4332858A (en) | 1978-12-27 | 1982-06-01 | Asahi Kasei Kogyo Kabushiki Kaisha | Multi-layer laminate comprising a modified styrene-butadiene block copolymer |
US4360568A (en) | 1980-05-12 | 1982-11-23 | Phillips Petroleum Company | Hot melt adhesive and additive therefor |
US4578429A (en) | 1984-08-31 | 1986-03-25 | Shell Oil Company | Selectively hydrogenated block copolymers modified with acid compounds or derivatives |
US4692357A (en) | 1985-02-21 | 1987-09-08 | Mitsubishi Petrochemical Co., Ltd. | Primer composition for olefin resin |
US4820568A (en) * | 1987-08-03 | 1989-04-11 | Allied-Signal Inc. | Composite and article using short length fibers |
US4833193A (en) * | 1987-08-14 | 1989-05-23 | Sieverding David L | Novel pressure sensitive adhesives |
US4835200A (en) | 1986-12-19 | 1989-05-30 | Shell Oil Company | Color stable hot melt adhesive |
US4898784A (en) | 1987-12-30 | 1990-02-06 | Shell Oil Company | Tie layer composition and laminated structures containing same |
US5021113A (en) | 1987-12-30 | 1991-06-04 | Shell Oil Company | Tie layer composition and laminated structures containing same |
USH1022H (en) * | 1991-01-09 | 1992-02-04 | Shell Oil Company | Soft paintable polymer composition |
US5112882A (en) | 1989-09-06 | 1992-05-12 | Minnesota Mining And Manufacturing Company | Radiation curable polyolefin pressure sensitive adhesive |
US5149741A (en) | 1989-07-21 | 1992-09-22 | Findley Adhesives, Inc. | Hot melt construction adhesives for disposable soft goods |
US5180766A (en) | 1990-05-14 | 1993-01-19 | Mitsubishi Petrochemical Co., Ltd. | Resin composition for primer use and primer composition employing the same |
US5194530A (en) | 1991-04-15 | 1993-03-16 | Shell Oil Company | Termination of anionic polymerization using hydrocarbon terminating agents |
US5209971A (en) | 1989-09-06 | 1993-05-11 | Minnesota Mining And Manufacturing Company | Radiation curable polyolefin pressure sensitive adhesive |
US5229464A (en) | 1991-04-29 | 1993-07-20 | Shell Oil Company | Epoxidized viscous conjugated diene block copolymers |
US5234524A (en) | 1990-10-25 | 1993-08-10 | Mitsubishi Petrochemical Co., Ltd. | Process for the preparation of laminate |
US5559165A (en) * | 1995-08-08 | 1996-09-24 | National Starch And Chemical Investment Holding Corporation | Hot melt adhesives for bonding to sensitive areas of the human body |
US5591792A (en) * | 1994-01-25 | 1997-01-07 | Mitsubishi Chemical Corporation | Adhesive resin composition |
US5633286A (en) * | 1977-03-17 | 1997-05-27 | Applied Elastomerics, Inc. | Gelatinous elastomer articles |
US5710206A (en) * | 1986-07-18 | 1998-01-20 | Raychem Limited | Gels comprising block copolymers |
-
1996
- 1996-02-01 US US08/595,094 patent/USH1949H1/en not_active Abandoned
Patent Citations (32)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3239478A (en) * | 1963-06-26 | 1966-03-08 | Shell Oil Co | Block copolymer adhesive compositions and articles prepared therefrom |
US3577398A (en) | 1966-06-09 | 1971-05-04 | Goodyear Tire & Rubber | Synthetic resin |
US3565247A (en) * | 1968-10-21 | 1971-02-23 | Minnesota Mining & Mfg | Pressure-sensitive adhesive tape product |
USRE27145E (en) | 1969-05-20 | 1971-06-22 | Side-chain | |
US3753936A (en) * | 1970-02-18 | 1973-08-21 | Phillips Petroleum Co | Branched rubbery block copolymer adhesive |
US3879248A (en) * | 1971-05-17 | 1975-04-22 | Donald O Kest | Method of bonding using urethane base pressure sensitive adhesives |
US3917607A (en) * | 1971-09-22 | 1975-11-04 | Shell Oil Co | Block copolymer adhesive compositions |
US3932327A (en) * | 1973-02-05 | 1976-01-13 | Phillips Petroleum Company | Adhesive compositions |
US3984369A (en) * | 1975-05-15 | 1976-10-05 | Shell Oil Company | Sealant |
US4062995A (en) * | 1976-06-23 | 1977-12-13 | Johnson & Johnson | Reticular web |
US5633286B1 (en) * | 1977-03-17 | 2000-10-10 | Applied Elastomerics Inc | Gelatinous elastomer articles |
US5633286A (en) * | 1977-03-17 | 1997-05-27 | Applied Elastomerics, Inc. | Gelatinous elastomer articles |
US4332858A (en) | 1978-12-27 | 1982-06-01 | Asahi Kasei Kogyo Kabushiki Kaisha | Multi-layer laminate comprising a modified styrene-butadiene block copolymer |
US4360568A (en) | 1980-05-12 | 1982-11-23 | Phillips Petroleum Company | Hot melt adhesive and additive therefor |
US4578429A (en) | 1984-08-31 | 1986-03-25 | Shell Oil Company | Selectively hydrogenated block copolymers modified with acid compounds or derivatives |
US4692357A (en) | 1985-02-21 | 1987-09-08 | Mitsubishi Petrochemical Co., Ltd. | Primer composition for olefin resin |
US5710206A (en) * | 1986-07-18 | 1998-01-20 | Raychem Limited | Gels comprising block copolymers |
US4835200A (en) | 1986-12-19 | 1989-05-30 | Shell Oil Company | Color stable hot melt adhesive |
US4820568A (en) * | 1987-08-03 | 1989-04-11 | Allied-Signal Inc. | Composite and article using short length fibers |
US4833193A (en) * | 1987-08-14 | 1989-05-23 | Sieverding David L | Novel pressure sensitive adhesives |
US5021113A (en) | 1987-12-30 | 1991-06-04 | Shell Oil Company | Tie layer composition and laminated structures containing same |
US4898784A (en) | 1987-12-30 | 1990-02-06 | Shell Oil Company | Tie layer composition and laminated structures containing same |
US5149741A (en) | 1989-07-21 | 1992-09-22 | Findley Adhesives, Inc. | Hot melt construction adhesives for disposable soft goods |
US5209971A (en) | 1989-09-06 | 1993-05-11 | Minnesota Mining And Manufacturing Company | Radiation curable polyolefin pressure sensitive adhesive |
US5112882A (en) | 1989-09-06 | 1992-05-12 | Minnesota Mining And Manufacturing Company | Radiation curable polyolefin pressure sensitive adhesive |
US5180766A (en) | 1990-05-14 | 1993-01-19 | Mitsubishi Petrochemical Co., Ltd. | Resin composition for primer use and primer composition employing the same |
US5234524A (en) | 1990-10-25 | 1993-08-10 | Mitsubishi Petrochemical Co., Ltd. | Process for the preparation of laminate |
USH1022H (en) * | 1991-01-09 | 1992-02-04 | Shell Oil Company | Soft paintable polymer composition |
US5194530A (en) | 1991-04-15 | 1993-03-16 | Shell Oil Company | Termination of anionic polymerization using hydrocarbon terminating agents |
US5229464A (en) | 1991-04-29 | 1993-07-20 | Shell Oil Company | Epoxidized viscous conjugated diene block copolymers |
US5591792A (en) * | 1994-01-25 | 1997-01-07 | Mitsubishi Chemical Corporation | Adhesive resin composition |
US5559165A (en) * | 1995-08-08 | 1996-09-24 | National Starch And Chemical Investment Holding Corporation | Hot melt adhesives for bonding to sensitive areas of the human body |
Non-Patent Citations (3)
Title |
---|
Crosslinking KRATON(R) FG1901X Rubber with CYMEL* 303, pp. 16-17, Technical Bulletin, SC:1048-88 (Oct. 1990). |
Crosslinking KRATON® FG1901X Rubber with CYMEL* 303, pp. 16-17, Technical Bulletin, SC:1048-88 (Oct. 1990). |
Robert A. Tait et al., "A Pragmatic Approach to the Manufacture of Solventborne Adhesives", Solvents, SC:2304-95 (Apr. 1995). |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050016675A1 (en) * | 1999-06-02 | 2005-01-27 | Bain Peter Stewart | Adhesive composition comprising thermoexpandable microcapsules |
US7371300B2 (en) * | 1999-06-02 | 2008-05-13 | De-Bonding Limited | Adhesive composition comprising thermoexpandable microcapsules |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
AS | Assignment |
Owner name: SHELL OIL COMPANY, TEXAS Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:HANSEN, DAVID R.;TAIT, ROBERT A.;SALAZAR, LYDIA A.;REEL/FRAME:010743/0010 Effective date: 19960131 |
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Free format text: PATENTED CASE |
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Owner name: CHASE MANHATTAN BANK, AS COLLATERAL AGENT, THE, NE Free format text: SECURITY AGREEMENT;ASSIGNOR:KRATON, POLYMERS U.S. LLC, FORMERLY KNOWN AS SHELL ELASTOMERS LLC;REEL/FRAME:011571/0342 Effective date: 20010228 |
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