USRE35007E - Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures - Google Patents
Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures Download PDFInfo
- Publication number
- USRE35007E USRE35007E US08/180,609 US18060994A USRE35007E US RE35007 E USRE35007 E US RE35007E US 18060994 A US18060994 A US 18060994A US RE35007 E USRE35007 E US RE35007E
- Authority
- US
- United States
- Prior art keywords
- oxalate
- bis
- solution
- parts
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/06—Luminescent, e.g. electroluminescent, chemiluminescent materials containing organic luminescent materials
- C09K11/07—Luminescent, e.g. electroluminescent, chemiluminescent materials containing organic luminescent materials having chemically interreactive components, e.g. reactive chemiluminescent compositions
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F21—LIGHTING
- F21K—NON-ELECTRIC LIGHT SOURCES USING LUMINESCENCE; LIGHT SOURCES USING ELECTROCHEMILUMINESCENCE; LIGHT SOURCES USING CHARGES OF COMBUSTIBLE MATERIAL; LIGHT SOURCES USING SEMICONDUCTOR DEVICES AS LIGHT-GENERATING ELEMENTS; LIGHT SOURCES NOT OTHERWISE PROVIDED FOR
- F21K2/00—Non-electric light sources using luminescence; Light sources using electrochemiluminescence
- F21K2/06—Non-electric light sources using luminescence; Light sources using electrochemiluminescence using chemiluminescence
Abstract
Description
______________________________________ Color Formulations ______________________________________ Blue 12 wt % CPPO. 0.2 wt % BPEN Green 12 wt % CPPO. 0.15 wt % BPEA Yellow 12 wt % CPPO. 0.25 wt % CBPEA ______________________________________
TABLE I ______________________________________ COLOR FLUORESCER (WT %) TLOP (FT-L-HR) ______________________________________ YELLOW 0.25 71.1 YELLOW 0.30 67.9 YELLOW 0.35 73.5 GREEN 0.15 47.9 GREEN 0.20 46.3 BLUE 0.07 7.09 BLUE 0.11 8.87 BLUE 0.14 9.40 BLUE 0.20 10.08 BLUE 0.25 13.51 ______________________________________
TABLE II ______________________________________ COLOR CPPO (WT %) TLOP (FT-L-HR) ______________________________________ YELLOW 8 39.6 YELLOW 11 46.2 YELLOW 15* 71.1 YELLOW 17 66.8 GREEN 4 8.98 GREEN 7.8 15.2 GREEN 12 27.4 GREEN 15* 26.2 BLUE 3.7 2.35 BLUE 7.7 6.47 BLUE 11.7 8.87 BLUE 14.2* 7.80 ______________________________________ *The CPPO slowly precipitates out of this oxalate solution.
TABLE III ______________________________________ OXALATE/PVC TLOP ACTIVATOR (PARTS) RATIO (WT:WT) (FT-L-HR) ______________________________________ 9 0.9:1 28.2 10 1.0:0 29.2 11 1.1:1 31.1 12 1.2:1 30.8 13 1.3:1 34.8 14 1.4:1 40.7 15 1.5:1 38.6 17 1.7:1 38.9 ______________________________________
TABLE IV ______________________________________ SLURRY WEIGHT (PARTS) MOLD THICKNESS (MM) ______________________________________ 10 90 mm dish 1.3 45 5 × 8 inch 1.9 15 90 mm dish 2.3 67.5 5 × 8 inch 2.9 20 90 mm dish 3.4 90 5 × 8 inch 3.7 25 90 mm dish 4.2 35 90 mm dish 5.1 40 90 mm dish 7.0 ______________________________________
TABLE V ______________________________________ STL PAD BRIGHTNESS THICKNESS (MM) (FT-L) TLOP (FT-L-HR) ______________________________________ 1.9 57.5 36.0 2.9 68.1 41.4 3.4 59.0 44.4 3.7 -- 56.0 4.2 62.6 51.9 5.1 69.6 66.6 7.0 93.3 78.8 ______________________________________
TABLE VI ______________________________________ WITH OR THICKNESS WITHOUT BRIGHTNESS TLOP (MM) FOIL BACKING (FT-L) (FT-L-HR) ______________________________________ 1.9 with 70.2 46.1 1.9 without 57.5 36.0 2.9 with 96.7 61.6 2.9 without 68.1 41.4 3.4 with 62.1 57.1 3.4 without 59.0 44.4 3.7 with -- 63.7 3.7 without -- 56.0 ______________________________________
TABLE VII ______________________________________ Parts NaSal TLOP (FT-L-HR) GLOW TIME ______________________________________ YELLOW STL 0.009 57.3 436 0.019 64.6 267 0.029 63.1 158 0.043 57.3 95 0.050 57.3 85 0.062 48.1 65 0.071 41.4 57 0.082 40.1 44 0.087 39.6 39 GREEN STL 0.009 43.0 330 0.019 47.4 217 0.029 43.3 119 0.043 42.3 80 0.050 41.6 90 0.062 39.4 74 0.071 38.9 62 0.082 35.5 44 0.087 34.4 42 BLUE STL 0.009 8.6 412 0.019 10.0 324 0.029 9.4 209 0.043 9.3 111 0.050 9.1 108 0.062 8.2 79 0.071 9.5 52 0.082 8.6 38 0.087 7.6 36 ______________________________________
______________________________________ PVC Particle Size FORMULATION FINE MEDIUM LARGE ______________________________________ No. 1 2.6 wt % 75 wt % 22.4 wt % No. 2 3.8 wt % 75 wt % 21.2 wt % No. 3 5.7 wt % 75 wt % 19.3 wt % ______________________________________
TABLE VIII ______________________________________ ACTIVATOR ABSORPTION No. 1 No. 2 No. 3 2.6% Fine PVC 3.8% Fine PVC 5.7% Fine PVC Time Wt. Time Wt. Time Wt. Min. Gain Min. Gain Min. Gain ______________________________________ 1 0.13 1 0.007 1 0.025 2 0.21 2 0.09 2 0.025 3 0.24 3 0.10 3 0.027 5 0.25 5 0.11 5 0.030 ______________________________________
TABLE IX ______________________________________ EXPOSURE TLOP LIGHTSTICK TLOP STRUCTURE (WEEKS) (FT-L-HR) (FT-L-HR) ______________________________________ 0 111.3 43.2 1 100.1 44.3 2 92.7 41.7 3 71.6 40.1 4 77.4 41.3 5 70.1 37.4 6 69.2 38.0 8 54.9 34.9 10 14.4 -- 12 9.7 18.7 ______________________________________
TABLE X ______________________________________ EXPOSURE TIME (HR) TLOP (FT-L-HR) ______________________________________ YELLOW 0 68.0 6 47.6 22 40.3 47 33.4 77 27.9 144 25.4 GREEN 0 44.7 6 39.8 24 36.7 48 32.9 72 30.1 168 26.4 BLUE 0 8.19 6 8.42 24 7.34 48 7.29 ______________________________________
TABLE XI __________________________________________________________________________ PARTS OF AVERAGE ACTIVATOR APPEARANCE PARTICLE MOLECULAR PER PART OF SIZE WEIGHT OF STRUCTURE STRUCTURES __________________________________________________________________________ 0.2-1.5 303,000 0.05 tough, highly microns (A) plasticized 70-75 98,000 0.28 smooth sur- microns (B) face, friable 120 104,000 0.45 rough surface, microns (C) fragile 150 205,000 0.62 bumpy surface, microns (D) very fragile __________________________________________________________________________
TABLE XII ______________________________________ PARTS OF ACTIVATOR PER PART OF APPEARANCE FORMULATION NO. STRUCTURE OF SHEET ______________________________________ 1 0.22 smooth surface, good strength .sup. 2C 0.25 slurry settles quickly, slightly flaky surface 3 0.33 smooth surface, good strength, can be folded without breaking, slightly stretchy 4 0.35 appearance similar to sheet from for- mulation No. 3 .sup. 5C 0.68 poor strength, very flaky surface ______________________________________ C = Comparative
TABLE XIII ______________________________________ PARTS OF ACTIVATOR PER PART OF APPEARANCE FORMULATION NO. STRUCTURE OF STRUCTURE ______________________________________ 6C 0.33 textured (orange peel) surface, strong, stretchy, can be folded double, flaky when cut 7C 0.37 smooth surface, breaks when folded double, strong, stretchy, flaky around edges 8C 0.33 same as formula- tion No. 7 ______________________________________ C = Comparative
______________________________________ FORMULATION NO. TLOP (FT-L-HR) ______________________________________ 6 31.6663 7 30.3903 8 36.4072 ______________________________________
TABLE XIV ______________________________________ TEMP TIME APPEARANCE OF SHEET ______________________________________ 90° C. 10 min smooth surface, reasonable strength 90° C. 15 min smooth surface, good strength 120° C. 30 min smooth surface, strong 150° C. 5 min very strong, tough, flex- ible, slightly over plasticized 150° C. 10 min slightly translucent, very strong tough, over plast- icized* 150° C. 20 min translucent, very strong and strong and tough, highly plasticized* ______________________________________ *Comparative
TABLE XV ______________________________________ PARTS OF ACTIVATOR PER PART OF TLOP TEMP (°C.) TIME (MIN) STRUCTURES (FT-L-HR) ______________________________________ 90 10 0.27 36.3930 90 15 0.30 34.5938 90 30 0.32 34.8413 120 10 0.35 37.8190 150 5 0.17 22.8411 150 10 0.02 6.4400 150 20 0.02 1.6309 ______________________________________
Claims (12)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/180,609 USRE35007E (en) | 1990-12-24 | 1994-01-13 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/632,844 US5173218A (en) | 1990-12-24 | 1990-12-24 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
US08/180,609 USRE35007E (en) | 1990-12-24 | 1994-01-13 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US07/632,844 Reissue US5173218A (en) | 1990-12-24 | 1990-12-24 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
Publications (1)
Publication Number | Publication Date |
---|---|
USRE35007E true USRE35007E (en) | 1995-08-01 |
Family
ID=24537184
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US07/632,844 Ceased US5173218A (en) | 1990-12-24 | 1990-12-24 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
US07/944,572 Expired - Lifetime US5348690A (en) | 1990-12-24 | 1992-09-14 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
US08/180,609 Expired - Lifetime USRE35007E (en) | 1990-12-24 | 1994-01-13 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US07/632,844 Ceased US5173218A (en) | 1990-12-24 | 1990-12-24 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
US07/944,572 Expired - Lifetime US5348690A (en) | 1990-12-24 | 1992-09-14 | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
Country Status (1)
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US (3) | US5173218A (en) |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5705103A (en) * | 1996-11-22 | 1998-01-06 | Jame Fine Chemicals, Inc. | Composition for producing chemiluminescent light of controllable duration |
US5824242A (en) * | 1995-03-31 | 1998-10-20 | Prolufab S.A.R.L. | Chemiluminescent solution |
US6523778B2 (en) | 2000-06-29 | 2003-02-25 | The Night Fun Co., Llc | Illuminated emergency signaling device and flying balloon |
US6647688B1 (en) | 2001-09-01 | 2003-11-18 | Brenda S. Gaitan | Thermoset fluorescent pigmentary vinyl |
US20050090878A1 (en) * | 2003-10-24 | 2005-04-28 | Solsberg Murray D. | Disposable chemiluminescent infrared therapy device |
US20050198879A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Emergency information sign |
US20050201079A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Emergency information lighting system |
US20050201078A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Lighting system with a passive phosphorescent light source |
US20050254227A1 (en) * | 2004-05-13 | 2005-11-17 | Bilodeau Wayne L | Chemiluminescent light article |
US7028687B1 (en) | 1999-08-26 | 2006-04-18 | Precious Life, Llc | Escape hood |
US20070134513A1 (en) * | 2005-12-13 | 2007-06-14 | Binney & Smith | Chemiluminescent system |
US20080128666A1 (en) * | 2005-12-13 | 2008-06-05 | Crayola, Llc | Chemiluminescent system |
US8647579B2 (en) | 2007-03-19 | 2014-02-11 | Nomadics, Inc. | Hydrogen peroxide detector comprising light-blocking tip with air deflector |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5173218A (en) * | 1990-12-24 | 1992-12-22 | American Cyanamid Company | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
US6336729B1 (en) | 1999-05-20 | 2002-01-08 | Richard Pavelle | Emergency light device |
MXPA04007835A (en) * | 2002-02-12 | 2005-09-30 | Omniglow Corp | Formable, porous, chemiluminescent reactant compositions and device therefor. |
US7622060B2 (en) * | 2002-02-12 | 2009-11-24 | Cyalume Technologies, Inc. | Formable, porous, chemiluminescent reactant composition and device therefor |
CN1299044C (en) * | 2002-03-20 | 2007-02-07 | 奥美尼发光有限公司 | Thixotropic, porous, chemiluminescent reactant composition |
US6798956B2 (en) * | 2002-07-16 | 2004-09-28 | Sun Microsystems, Inc. | Optical cable with indicator |
US7052456B2 (en) * | 2003-04-16 | 2006-05-30 | Simon James S | Airway products having LEDs |
US7799573B2 (en) | 2005-08-31 | 2010-09-21 | Normadics, Inc. | Detection of explosives and other species |
US20070111321A1 (en) * | 2005-08-31 | 2007-05-17 | Nomadics, Inc. | Detection of explosives and other species |
US7674406B2 (en) * | 2007-06-14 | 2010-03-09 | Bindra Perminder S | Chemiluminescent compositions and methods of making and using thereof |
US7777208B2 (en) * | 2007-09-13 | 2010-08-17 | Cyalume Technologies, Inc. | Infra-red lighting system and device |
US8658066B2 (en) | 2009-05-12 | 2014-02-25 | Mega Glow, Llc | Chemiluminescent powders and methods of making and using thereof |
US7964119B2 (en) * | 2009-05-12 | 2011-06-21 | Mega Glow, LLC. | Chemiluminescent powders and methods of making and using thereof |
SG177773A1 (en) * | 2009-07-27 | 2012-03-29 | Cyalume Technologies Inc | Combined thermal and chemiluminescent reaction system |
WO2011019695A1 (en) | 2009-08-11 | 2011-02-17 | Kms Consulting, Llc | Projectile with a multi-spectral marking plume |
KR101883660B1 (en) * | 2010-10-24 | 2018-07-31 | 사이륨 테크놀로지즈 인코포레이티드 | Combined thermal and chemiluminescent reaction system |
WO2013008106A1 (en) | 2011-07-11 | 2013-01-17 | Etview Ltd. | Endobronchial tube |
EP2754384B1 (en) | 2013-01-10 | 2018-07-11 | Ambu A/S | Endobronchial tube with integrated image sensor and cleaning nozzle arrangement |
US9217627B2 (en) | 2013-03-21 | 2015-12-22 | Kms Consulting, Llc | Training ammunition cartridge with reactive liquid materials for marking a point of impact |
Citations (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3350553A (en) * | 1965-08-05 | 1967-10-31 | Du Pont | Oxyluminescent light sources and processes of making same |
US3362378A (en) * | 1964-10-28 | 1968-01-09 | Navy Usa | Light extending product and process |
US3539794A (en) * | 1967-09-12 | 1970-11-10 | American Cyanamid Co | Self-contained chemiluminescent lighting device |
US3729425A (en) * | 1969-04-29 | 1973-04-24 | Us Navy | Porous chemiluminescent material and method of manufacture |
US3774022A (en) * | 1965-06-30 | 1973-11-20 | Trw Inc | Packaged chemiluminescent material |
US3808414A (en) * | 1972-12-21 | 1974-04-30 | American Cyanamid Co | Device for the packaging of a three or more component chemiluminescent system |
US3816325A (en) * | 1970-04-15 | 1974-06-11 | American Cyanamid Co | Chemical lighting system comprising a polymeric chemiluminescent composition and an activating liquid comprising hydrogen peroxide |
US3893938A (en) * | 1971-07-14 | 1975-07-08 | American Cyanamid Co | Chemiluminescent article of bis-ester of oxalic acid and method of providing chemiluminescent light |
US3994820A (en) * | 1972-06-19 | 1976-11-30 | American Cyanamid Company | Polymers in oxalate chemiluminescent systems |
US4635166A (en) * | 1985-08-28 | 1987-01-06 | Cameron Robert W | Chemical emergency light |
US4814949A (en) * | 1987-11-13 | 1989-03-21 | American Cyanamid Company | Chemiluminescent device |
US4859369A (en) * | 1984-09-24 | 1989-08-22 | American Cyanamid Company | Use of water-soluble polymers in aqueous chemical light formulations |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5121302A (en) * | 1990-12-24 | 1992-06-09 | American Cyanamid Company | Solid, thin chemiluminescent device |
US5173218A (en) * | 1990-12-24 | 1992-12-22 | American Cyanamid Company | Preparation of chemiluminescent vinyl halide or vinylidene halide polymer structures |
-
1990
- 1990-12-24 US US07/632,844 patent/US5173218A/en not_active Ceased
-
1992
- 1992-09-14 US US07/944,572 patent/US5348690A/en not_active Expired - Lifetime
-
1994
- 1994-01-13 US US08/180,609 patent/USRE35007E/en not_active Expired - Lifetime
Patent Citations (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3362378A (en) * | 1964-10-28 | 1968-01-09 | Navy Usa | Light extending product and process |
US3774022A (en) * | 1965-06-30 | 1973-11-20 | Trw Inc | Packaged chemiluminescent material |
US3350553A (en) * | 1965-08-05 | 1967-10-31 | Du Pont | Oxyluminescent light sources and processes of making same |
US3539794A (en) * | 1967-09-12 | 1970-11-10 | American Cyanamid Co | Self-contained chemiluminescent lighting device |
US3729425A (en) * | 1969-04-29 | 1973-04-24 | Us Navy | Porous chemiluminescent material and method of manufacture |
US3816325A (en) * | 1970-04-15 | 1974-06-11 | American Cyanamid Co | Chemical lighting system comprising a polymeric chemiluminescent composition and an activating liquid comprising hydrogen peroxide |
US3893938A (en) * | 1971-07-14 | 1975-07-08 | American Cyanamid Co | Chemiluminescent article of bis-ester of oxalic acid and method of providing chemiluminescent light |
US3994820A (en) * | 1972-06-19 | 1976-11-30 | American Cyanamid Company | Polymers in oxalate chemiluminescent systems |
US3808414A (en) * | 1972-12-21 | 1974-04-30 | American Cyanamid Co | Device for the packaging of a three or more component chemiluminescent system |
US4859369A (en) * | 1984-09-24 | 1989-08-22 | American Cyanamid Company | Use of water-soluble polymers in aqueous chemical light formulations |
US4635166A (en) * | 1985-08-28 | 1987-01-06 | Cameron Robert W | Chemical emergency light |
US4814949A (en) * | 1987-11-13 | 1989-03-21 | American Cyanamid Company | Chemiluminescent device |
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5824242A (en) * | 1995-03-31 | 1998-10-20 | Prolufab S.A.R.L. | Chemiluminescent solution |
US5705103A (en) * | 1996-11-22 | 1998-01-06 | Jame Fine Chemicals, Inc. | Composition for producing chemiluminescent light of controllable duration |
US7028687B1 (en) | 1999-08-26 | 2006-04-18 | Precious Life, Llc | Escape hood |
US6523778B2 (en) | 2000-06-29 | 2003-02-25 | The Night Fun Co., Llc | Illuminated emergency signaling device and flying balloon |
US6647688B1 (en) | 2001-09-01 | 2003-11-18 | Brenda S. Gaitan | Thermoset fluorescent pigmentary vinyl |
US20050090878A1 (en) * | 2003-10-24 | 2005-04-28 | Solsberg Murray D. | Disposable chemiluminescent infrared therapy device |
US7628939B2 (en) | 2003-10-24 | 2009-12-08 | Murray David Solsberg | Disposable chemiluminescent infrared therapy device |
US7799247B2 (en) | 2003-10-24 | 2010-09-21 | Murray David Solsberg | Disposable chemiluminescent infrared therapy device |
US20080208250A1 (en) * | 2003-10-24 | 2008-08-28 | Murray David Solsberg | Disposable chemiluminescent infrared therapy device |
US20050198879A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Emergency information sign |
US20050201079A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Emergency information lighting system |
US20050201078A1 (en) * | 2004-03-12 | 2005-09-15 | Hannington Michael E. | Lighting system with a passive phosphorescent light source |
US8250794B2 (en) | 2004-03-12 | 2012-08-28 | Avery Dennison Corporation | Emergency information sign |
US7241021B2 (en) | 2004-03-12 | 2007-07-10 | Avery Dennison Corporation | Emergency information lighting system |
US20050254227A1 (en) * | 2004-05-13 | 2005-11-17 | Bilodeau Wayne L | Chemiluminescent light article |
US20080128666A1 (en) * | 2005-12-13 | 2008-06-05 | Crayola, Llc | Chemiluminescent system |
US20070134513A1 (en) * | 2005-12-13 | 2007-06-14 | Binney & Smith | Chemiluminescent system |
US8647579B2 (en) | 2007-03-19 | 2014-02-11 | Nomadics, Inc. | Hydrogen peroxide detector comprising light-blocking tip with air deflector |
Also Published As
Publication number | Publication date |
---|---|
US5173218A (en) | 1992-12-22 |
US5348690A (en) | 1994-09-20 |
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