WO1990006046A3 - Method for purifying a crude dimethyl naphthalene dicarboxylate - Google Patents

Method for purifying a crude dimethyl naphthalene dicarboxylate Download PDF

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Publication number
WO1990006046A3
WO1990006046A3 PCT/US1989/005282 US8905282W WO9006046A3 WO 1990006046 A3 WO1990006046 A3 WO 1990006046A3 US 8905282 W US8905282 W US 8905282W WO 9006046 A3 WO9006046 A3 WO 9006046A3
Authority
WO
WIPO (PCT)
Prior art keywords
purifying
naphthalene dicarboxylate
dimethyl naphthalene
crude dimethyl
containing component
Prior art date
Application number
PCT/US1989/005282
Other languages
French (fr)
Other versions
WO1990006046A2 (en
Inventor
Juergen Klaus Holzhauer
Robert David Oltrogge
Dennis James Michalak
Original Assignee
Amoco Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Amoco Corp filed Critical Amoco Corp
Priority to KR1019900701556A priority Critical patent/KR0137646B1/en
Priority to DE68926574T priority patent/DE68926574T2/en
Priority to EP90900473A priority patent/EP0444132B1/en
Publication of WO1990006046A2 publication Critical patent/WO1990006046A2/en
Publication of WO1990006046A3 publication Critical patent/WO1990006046A3/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
    • C07C69/84—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring
    • C07C69/88—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring of monocyclic hydroxy carboxylic acids, the hydroxy groups and the carboxyl groups of which are bound to carbon atoms of a six-membered aromatic ring with esterified carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/39—Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/56—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption

Abstract

A method for purifying a dimethyl naphthalene dicarboxylate produced from a naphthalene dicarboxylic acid which is in turn produced by the liquid phase oxidation of a dialkylnaphthalene or partially oxidized derivative thereof in the presence of a catalyst comprising a bromine-containing component and at least one of a cobalt- or manganese-containing component.
PCT/US1989/005282 1988-11-21 1989-11-17 Method for purifying a crude dimethyl naphthalene dicarboxylate WO1990006046A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
KR1019900701556A KR0137646B1 (en) 1988-11-21 1989-11-17 Method for purifying a crude dimethyl naphthalene dicarboxylate
DE68926574T DE68926574T2 (en) 1988-11-21 1989-11-17 METHOD FOR PURIFYING A RAW DIMETHYL-NAPHTHALINE DIKARBOXYLATE
EP90900473A EP0444132B1 (en) 1988-11-21 1989-11-17 Method for purifying a crude dimethyl naphthalene dicarboxylate

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US274,238 1988-11-21
US07/274,238 US4886901A (en) 1988-11-21 1988-11-21 Method for purifying a crude dimethyl naphthalene dicarboxylate

Publications (2)

Publication Number Publication Date
WO1990006046A2 WO1990006046A2 (en) 1990-06-14
WO1990006046A3 true WO1990006046A3 (en) 1990-08-09

Family

ID=23047381

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1989/005282 WO1990006046A2 (en) 1988-11-21 1989-11-17 Method for purifying a crude dimethyl naphthalene dicarboxylate

Country Status (7)

Country Link
US (1) US4886901A (en)
EP (1) EP0444132B1 (en)
JP (1) JP2808185B2 (en)
KR (1) KR0137646B1 (en)
AT (1) ATE138636T1 (en)
DE (1) DE68926574T2 (en)
WO (1) WO1990006046A2 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5101050A (en) * 1989-11-29 1992-03-31 Amoco Corporation Process for the production of aromatic anhydrides and aromatic esters with superior color properties
US5169977A (en) * 1990-03-15 1992-12-08 Mitsubishi Gas Chemical Company, Inc. Process for purifying dimethyl-2,6-naphthalene dicarboxylate
US5095135A (en) * 1990-04-05 1992-03-10 Sumikin Chemical Co., Ltd. Process for the preparation of high-purity naphthalenecarboxylic acid esters
US5194572A (en) * 1990-08-30 1993-03-16 Amoco Corporation Stabilized naphthalenedicarboxylic acid diesters
US5138025A (en) * 1990-08-30 1992-08-11 Amoco Corporation Stabilized naphthalenedicarboxylic acid diesters
US5328927A (en) * 1992-03-03 1994-07-12 Merck Sharpe & Dohme, Ltd. Hetercyclic compounds, processes for their preparation and pharmaceutical compositions containing them
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
US6054610A (en) * 1995-06-07 2000-04-25 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes
US6013835A (en) * 1995-06-07 2000-01-11 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid
US5767311A (en) * 1995-06-07 1998-06-16 Glitsch International, Inc. Method and apparatus for preparing purified terephtalic acid
US6013831A (en) * 1997-05-08 2000-01-11 Mitsubishi Gas Chemical Company, Inc. Processes for the production of high-purity dimethyl 2, 6-naphthalenedicarboxylate and naphthalenedicarboxylic acid
ES2216953T3 (en) 1999-08-30 2004-11-01 MOSSI & GHISOLFI INTERNATIONAL S.A. AN INTEGRATED PROCESS FOR THE PRODUCTION OF ACID 2,6-NAFTALEN DICARBOXILICO.
KR100417058B1 (en) * 2001-06-01 2004-02-05 한국화학연구원 Purification Method and Equipment for Polyethylene Wax

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3334131A (en) * 1962-03-09 1967-08-01 Chemische Werke Witten Process for the preparation of methyl esters of aromatic polyhalogen carboxylic acids
US3425915A (en) * 1967-02-09 1969-02-04 Edward S Roberts Purification of high boiling aromatic compounds by codistillation with a chlorinated diphenyl solvent
US3962315A (en) * 1973-05-09 1976-06-08 Hoechst Aktiengesellschaft Process for the purification of terephthalic acid dimethyl ester
US4048021A (en) * 1974-02-12 1977-09-13 Teijin Limited Method of purifying crude 2,6-naphthalenedicarboxylic acid dimethyl ester
US4126755A (en) * 1972-09-12 1978-11-21 Dynamit Nobel Aktiengesellschaft Process for the preparation of dimethyl terephthalate
US4402195A (en) * 1982-02-02 1983-09-06 Campbell Loyal E Drinking mug

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3402195A (en) * 1964-05-18 1968-09-17 Diamond Shamrock Corp Recovery of alkyl tetrahaloterephthalates from xylene
JPS4996467A (en) * 1973-01-24 1974-09-12
AR204838A1 (en) * 1973-08-20 1976-03-05 Amp Inc APPARATUS TO LOCATE IN A WORKING AREA IN A PREDETERMINED SPACED ARRANGEMENT THE FREE ENDS OF A PLURALITY OF ELECTRIC CONDUCTING WIRES
JPS522237U (en) * 1975-06-24 1977-01-08
JPS6119551A (en) * 1984-05-17 1986-01-28 Koyo Seiko Co Ltd Equipment for grinding outer peripheral surface of outer ring of rolling bearing with shaft
JPS6048814A (en) * 1984-07-19 1985-03-16 Yokota Kikai Kk Conveyor for loading electronic part

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3334131A (en) * 1962-03-09 1967-08-01 Chemische Werke Witten Process for the preparation of methyl esters of aromatic polyhalogen carboxylic acids
US3425915A (en) * 1967-02-09 1969-02-04 Edward S Roberts Purification of high boiling aromatic compounds by codistillation with a chlorinated diphenyl solvent
US4126755A (en) * 1972-09-12 1978-11-21 Dynamit Nobel Aktiengesellschaft Process for the preparation of dimethyl terephthalate
US3962315A (en) * 1973-05-09 1976-06-08 Hoechst Aktiengesellschaft Process for the purification of terephthalic acid dimethyl ester
US4048021A (en) * 1974-02-12 1977-09-13 Teijin Limited Method of purifying crude 2,6-naphthalenedicarboxylic acid dimethyl ester
US4402195A (en) * 1982-02-02 1983-09-06 Campbell Loyal E Drinking mug

Also Published As

Publication number Publication date
EP0444132B1 (en) 1996-05-29
KR900701727A (en) 1990-12-04
JPH03502334A (en) 1991-05-30
DE68926574T2 (en) 1996-09-26
EP0444132A4 (en) 1991-07-04
DE68926574D1 (en) 1996-07-04
ATE138636T1 (en) 1996-06-15
KR0137646B1 (en) 1998-04-30
WO1990006046A2 (en) 1990-06-14
US4886901A (en) 1989-12-12
EP0444132A1 (en) 1991-09-04
JP2808185B2 (en) 1998-10-08

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