WO1992019698A3 - Combination magnetic separation, classification and attrition process for renewing and recovering particulates - Google Patents

Combination magnetic separation, classification and attrition process for renewing and recovering particulates Download PDF

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Publication number
WO1992019698A3
WO1992019698A3 PCT/US1992/003251 US9203251W WO9219698A3 WO 1992019698 A3 WO1992019698 A3 WO 1992019698A3 US 9203251 W US9203251 W US 9203251W WO 9219698 A3 WO9219698 A3 WO 9219698A3
Authority
WO
WIPO (PCT)
Prior art keywords
catalyst
renewing
classification
magnetic separation
attrition process
Prior art date
Application number
PCT/US1992/003251
Other languages
French (fr)
Other versions
WO1992019698A2 (en
Inventor
William P Hettinger Jr
Original Assignee
Ashland Oil Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ashland Oil Inc filed Critical Ashland Oil Inc
Priority to EP92914638A priority Critical patent/EP0583422B1/en
Publication of WO1992019698A2 publication Critical patent/WO1992019698A2/en
Publication of WO1992019698A3 publication Critical patent/WO1992019698A3/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/14Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
    • C10G11/18Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
    • C10G11/182Regeneration

Abstract

Optimized utilization of combinations of fluid catalyst magnetic separator, classifier, and/or attriter can be used to achieve lower catalyst cost, and better catalyst activity and selectivity through control of metal-on-catalyst, particle size and particle size distribution. This process is especially useful when processing high metal-containing feedstocks. This provides a catalyst recovery unit (RCUTM) ancillary to an FCC or similar unit.
PCT/US1992/003251 1991-05-03 1992-04-20 Combination magnetic separation, classification and attrition process for renewing and recovering particulates WO1992019698A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
EP92914638A EP0583422B1 (en) 1991-05-03 1992-04-20 Combination magnetic separation, classification and attrition process for renewing and recovering particulates

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US695,188 1991-05-03
US07/695,188 US5393412A (en) 1991-05-03 1991-05-03 Combination magnetic separation, classification and attrition process for renewing and recovering particulates

Publications (2)

Publication Number Publication Date
WO1992019698A2 WO1992019698A2 (en) 1992-11-12
WO1992019698A3 true WO1992019698A3 (en) 1993-01-07

Family

ID=24791995

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US1992/003251 WO1992019698A2 (en) 1991-05-03 1992-04-20 Combination magnetic separation, classification and attrition process for renewing and recovering particulates

Country Status (5)

Country Link
US (3) US5393412A (en)
EP (1) EP0583422B1 (en)
AU (1) AU2265392A (en)
MX (1) MX9202040A (en)
WO (1) WO1992019698A2 (en)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5393412A (en) * 1991-05-03 1995-02-28 Ashland Oil, Inc. Combination magnetic separation, classification and attrition process for renewing and recovering particulates
US6059959A (en) * 1996-02-08 2000-05-09 Kellogg Brown & Root, Inc. Varying carbon on catalyst to magnetically separate high metals catalyst
US5985134A (en) * 1997-01-12 1999-11-16 M.W. Kellogg Company Startup of magnetic separation process in an FCC unit
US5958219A (en) * 1997-01-12 1999-09-28 The M. W. Kellogg Company Metals passivation by magnetic treatment to permit higher metals levels on FCC catalyst
US6041942A (en) * 1997-01-12 2000-03-28 Kellogg Brown & Root, Inc. Magnetic catalyst separation using stacked magnets
US5972208A (en) * 1997-07-11 1999-10-26 The M. W. Kellogg Company FCC metals passivation additives applied to catalyst
US5985133A (en) * 1997-07-11 1999-11-16 Marathon Ashland Petroleum Llc Control of particle size distribution in an FCC unit
US6099721A (en) * 1998-02-12 2000-08-08 The M.W. Kellogg Company Use of magnetic separation to remove non-magnetic, particles from FCC catalyst
CN1089642C (en) * 1998-06-24 2002-08-28 中国石化集团洛阳石油化工总厂 Magnetic separating machine, separating process and corollary equipment for separating waste catalytic cracking catalyst
US6361749B1 (en) * 1998-08-18 2002-03-26 Immunivest Corporation Apparatus and methods for magnetic separation
WO2000062034A2 (en) * 1999-04-09 2000-10-19 Shot, Inc. Multistage electromagnetic separator for purifying cells, chemicals and protein structures
US7223896B2 (en) * 2004-04-29 2007-05-29 Exxonmobil Chemical Patents Inc. Fines co-feed for maintaining efficient reactor hydrodynamics
US7090081B2 (en) * 2003-09-05 2006-08-15 Exxonmobil Chemical Patents Inc. Selectively removing undesirably sized catalyst particles from a reaction system
CA2453005A1 (en) * 2003-12-17 2005-06-17 Fermag Inc. Hydrometallurgical process for separating steel mill dust using an arc furnace and pigments obtained by the process
WO2005065267A2 (en) * 2003-12-24 2005-07-21 Massachusetts Institute Of Technology Magnetophoretic cell clarification
US7431826B2 (en) * 2004-02-26 2008-10-07 Metal Alloy Reclaimers, Inc. Ii. Discarded FCC equilibrium catalyst through reclamation
US7829750B2 (en) * 2004-12-30 2010-11-09 Exxonmobil Chemical Patents Inc. Fluidizing a population of catalyst particles having a low catalyst fines content
US7829030B2 (en) * 2004-12-30 2010-11-09 Exxonmobil Chemical Patents Inc. Fluidizing a population of catalyst particles having a low catalyst fines content
US8016935B2 (en) * 2005-06-17 2011-09-13 Ferrinov Inc. Anti-corrosion pigments coming from dust of an electric arc furnace and containing sacrificial calcium
US20070012597A1 (en) * 2005-07-13 2007-01-18 Crystal Filtration Company Process and apparatus for filtering metal working fluid containing metal fines
US8262902B2 (en) * 2009-02-19 2012-09-11 Phillips 66 Company Magnetic removal of material from a mixture based on sulfided diluent in the mixture
US9242235B2 (en) * 2009-05-18 2016-01-26 Integrated & Proven Catalyst Technologies Corp. Separation of fluid catalytic cracking equilibrium catalysts to improve value and reduce waste
AU2012231256A1 (en) * 2011-03-19 2013-10-03 Quanta Technologies, Llc Process to improve formulations of hydrocarbon conversion catalysts through removal and modification of detrimental particles and reuse of modified fractions
CN103509596B (en) * 2013-09-29 2015-08-26 中国石油大学(北京) A kind of method of processing inferior heavy oil
JP6719980B2 (en) * 2016-05-17 2020-07-08 日揮触媒化成株式会社 Method for reactivating catalyst for fluidized catalytic cracking of iron deposit, reactivating device, fluid catalytic cracking method
CN111764850B (en) * 2020-06-22 2022-02-25 中国石油大学(北京) Hollow ball filtering and separating device and drilling string
CN111921459B (en) * 2020-07-31 2022-04-08 宁波巨化化工科技有限公司 Reactor capable of simultaneously producing trichloroethylene and tetrachloroethylene
CN113048828B (en) * 2021-02-23 2022-09-23 山西文龙中美环能科技股份有限公司 Multistage waste heat recovery device convenient to handle usefulness to cinder processing

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2067217A (en) * 1979-12-21 1981-07-22 Nippon Oil Co Ltd Treatment of fluid cracking catalyst
EP0072394A1 (en) * 1981-05-13 1983-02-23 Ashland Oil, Inc. Magnetic separation of high activity catalyst from low activity catalyst
WO1990012075A1 (en) * 1989-04-03 1990-10-18 Ashland Oil, Inc. Magnetic separation into low, intermediate and high metals and activity catalyst
WO1991012298A1 (en) * 1990-02-09 1991-08-22 Ashland Oil, Inc. Addition of magnetic moieties in fluid bed hydrocarbon processing

Family Cites Families (37)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1339300A (en) * 1920-05-04 Process for the magnetic sizing and grading oe ore
US1390688A (en) * 1915-12-30 1921-09-13 Ellis Carleton Removing catalyzer from oil
US2348418A (en) * 1940-11-20 1944-05-09 Standard Oil Co Catalytic process
US2430015A (en) * 1945-08-21 1947-11-04 Shell Dev Utilization of powdered catalysts
US2471078A (en) * 1946-06-12 1949-05-24 Standard Oil Dev Co Catalyst quality by magnetic separation
US2635749A (en) * 1949-09-29 1953-04-21 Standard Oil Co Catalyst separation
US2786047A (en) * 1952-02-11 1957-03-19 Phillips Petroleum Co Process for removing nickel catalyst from hydrogenated polybutadiene
US3595391A (en) * 1969-02-24 1971-07-27 Byron C Schmid Magnetic separator
US3945915A (en) * 1973-02-09 1976-03-23 Fmc Corporation Method of and apparatus for assorting particles according to the physical characteristics thereof
US4021367A (en) * 1973-05-08 1977-05-03 Budapesti Muszaki Egyetem Process for recovering suspended metal catalyst from their suspension
JPS5198399A (en) * 1975-02-26 1976-08-30
US4051023A (en) * 1975-04-11 1977-09-27 Eriez Magnetics Combination electromagnet and permanent magnet separator
LU75716A1 (en) * 1975-09-05 1977-04-28
US4057512A (en) * 1975-09-29 1977-11-08 Exxon Research & Engineering Co. Alkali metal catalyst recovery system
GB1592779A (en) * 1976-12-15 1981-07-08 English Clays Lovering Pochin Magnetic separation
US4200520A (en) * 1978-01-30 1980-04-29 Exxon Research & Engineering Co. Catalytic cracking process
GB2064377B (en) * 1979-10-12 1984-03-21 Imperial College Magnetic separators
US4280839A (en) * 1979-11-01 1981-07-28 Uop Inc. Recovery of metal values from a metal bearing source of nickel and vanadium
US4252672A (en) * 1979-12-04 1981-02-24 Xerox Corporation Preparation of colloidal iron dispersions by the polymer-catalyzed decomposition of iron carbonyl and iron organocarbonyl compounds
US4280896A (en) * 1979-12-31 1981-07-28 Exxon Research & Engineering Co. Passivation of cracking catalysts
JPS5730786A (en) * 1980-07-31 1982-02-19 Nippon Oil Co Ltd Method for catalytic reaction of heavy petroleum oil
US4394281A (en) * 1980-12-19 1983-07-19 Exxon Research And Engineering Co. Composition for use in a magnetically fluidized bed
JPS57159884A (en) * 1981-03-30 1982-10-02 Nippon Oil Co Ltd Fluidized catalytic cracking of heavy oils
JPS57209642A (en) * 1981-06-19 1982-12-23 Res Assoc Residual Oil Process<Rarop> Treatment of waste catalyst
FR2577235B1 (en) * 1985-02-13 1987-02-20 Omnium Traitement Valorisa SOLID WASTE TREATMENT PLANT FOR PRODUCING FUEL
US4667832A (en) * 1985-04-08 1987-05-26 Reinfeld Nyles V Apparatus for processing and recovery of the metal containers from trash
US4720473A (en) * 1986-03-10 1988-01-19 Cri International, Inc. Production of improved catalyst-type particles using length and density grading
US4669397A (en) * 1986-08-21 1987-06-02 Smith & Mahoney, P.C. Recovery of useful materials from refuse fuel ash
DE3637200A1 (en) * 1986-10-31 1988-05-05 Kloeckner Humboldt Deutz Ag MAGNETIC BLOCK ARRANGEMENT WITH OUTSIDE FIELD
US4835128A (en) * 1986-12-04 1989-05-30 Mobil Oil Corporation Method for reducing the effects of metals on FCC catalysts
US4834870A (en) * 1987-09-04 1989-05-30 Huron Valley Steel Corporation Method and apparatus for sorting non-ferrous metal pieces
ZA886696B (en) * 1987-09-11 1989-04-26 Alcan Int Ltd Method of separating metal alloy particles
WO1992003251A1 (en) * 1990-08-20 1992-03-05 Welding Industries Limited Welding electrodes and method
US5198098A (en) * 1990-10-19 1993-03-30 Ashland Oil, Inc. Magnetic separation of old from new equilibrium particles by means of manganese addition
US5116486A (en) * 1991-02-01 1992-05-26 Pederson Dennis A Apparatus and method for separating recyclable waste
US5393412A (en) * 1991-05-03 1995-02-28 Ashland Oil, Inc. Combination magnetic separation, classification and attrition process for renewing and recovering particulates
US5516420A (en) * 1994-05-10 1996-05-14 Ashland Inc. Magnetically separated equilibrium catalyst for specialized cracking

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2067217A (en) * 1979-12-21 1981-07-22 Nippon Oil Co Ltd Treatment of fluid cracking catalyst
EP0072394A1 (en) * 1981-05-13 1983-02-23 Ashland Oil, Inc. Magnetic separation of high activity catalyst from low activity catalyst
WO1990012075A1 (en) * 1989-04-03 1990-10-18 Ashland Oil, Inc. Magnetic separation into low, intermediate and high metals and activity catalyst
WO1991012298A1 (en) * 1990-02-09 1991-08-22 Ashland Oil, Inc. Addition of magnetic moieties in fluid bed hydrocarbon processing

Also Published As

Publication number Publication date
AU2265392A (en) 1992-12-21
US5393412A (en) 1995-02-28
EP0583422A1 (en) 1994-02-23
MX9202040A (en) 1992-11-01
EP0583422B1 (en) 1996-12-18
US5746321A (en) 1998-05-05
US5636747A (en) 1997-06-10
WO1992019698A2 (en) 1992-11-12

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