WO1998036826A1 - Multiautoclave for combinatorial synthesis of zeolites and other materials - Google Patents
Multiautoclave for combinatorial synthesis of zeolites and other materials Download PDFInfo
- Publication number
- WO1998036826A1 WO1998036826A1 PCT/NO1998/000051 NO9800051W WO9836826A1 WO 1998036826 A1 WO1998036826 A1 WO 1998036826A1 NO 9800051 W NO9800051 W NO 9800051W WO 9836826 A1 WO9836826 A1 WO 9836826A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- pressure
- perforations
- reactor vessel
- temperature reactor
- central block
- Prior art date
Links
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
- B01J3/04—Pressure vessels, e.g. autoclaves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00306—Reactor vessels in a multiple arrangement
- B01J2219/00313—Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00306—Reactor vessels in a multiple arrangement
- B01J2219/00313—Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks
- B01J2219/00319—Reactor vessels in a multiple arrangement the reactor vessels being formed by arrays of wells in blocks the blocks being mounted in stacked arrangements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00331—Details of the reactor vessels
- B01J2219/00333—Closures attached to the reactor vessels
- B01J2219/00335—Septa
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00279—Features relating to reactor vessels
- B01J2219/00331—Details of the reactor vessels
- B01J2219/00333—Closures attached to the reactor vessels
- B01J2219/00349—Spheres
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00277—Apparatus
- B01J2219/00477—Means for pressurising the reaction vessels
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00585—Parallel processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00596—Solid-phase processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00601—High-pressure processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
- B01J2219/00747—Catalysts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00718—Type of compounds synthesised
- B01J2219/00745—Inorganic compounds
- B01J2219/0075—Metal based compounds
- B01J2219/00754—Metal oxides
-
- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B30/00—Methods of screening libraries
- C40B30/08—Methods of screening libraries by measuring catalytic activity
-
- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B40/00—Libraries per se, e.g. arrays, mixtures
- C40B40/18—Libraries containing only inorganic compounds or inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B60/00—Apparatus specially adapted for use in combinatorial chemistry or with libraries
- C40B60/14—Apparatus specially adapted for use in combinatorial chemistry or with libraries for creating libraries
Abstract
Description
Claims
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE69801813T DE69801813T2 (en) | 1997-02-20 | 1998-02-20 | MULTI-AUTOCLAVE FOR COMBINED SYNTHESIS OF ZEOLITES AND OTHER SUBSTANCES |
AU62317/98A AU6231798A (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combinatorial synthesis of zeolites and other materials |
CA002281773A CA2281773C (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combinatorial synthesis of zeolites and other materials |
EP98904447A EP0968050B1 (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combinatorial synthesis of zeolites and other materials |
AT98904447T ATE206068T1 (en) | 1997-02-20 | 1998-02-20 | MULTIAUTOCLAVE FOR COMBINED SYNTHESIS OF ZEOLITES AND OTHER SUBSTANCES |
JP53652198A JP3372553B2 (en) | 1997-02-20 | 1998-02-20 | Multi-autoclave reaction vessel |
DK98904447T DK0968050T3 (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combined synthesis of zolites and other materials |
US09/308,562 US6821486B1 (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combinatorial synthesis of zeolites and other materials |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NO970788A NO304355B1 (en) | 1997-02-20 | 1997-02-20 | Multi-autoclave for methodical, automated synthesis of zeolites and other compounds |
NO970788 | 1997-02-20 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO1998036826A1 true WO1998036826A1 (en) | 1998-08-27 |
Family
ID=19900405
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/NO1998/000051 WO1998036826A1 (en) | 1997-02-20 | 1998-02-20 | Multiautoclave for combinatorial synthesis of zeolites and other materials |
Country Status (11)
Country | Link |
---|---|
US (1) | US6821486B1 (en) |
EP (1) | EP0968050B1 (en) |
JP (1) | JP3372553B2 (en) |
AT (1) | ATE206068T1 (en) |
AU (1) | AU6231798A (en) |
CA (1) | CA2281773C (en) |
DE (1) | DE69801813T2 (en) |
DK (1) | DK0968050T3 (en) |
ES (1) | ES2166143T3 (en) |
NO (1) | NO304355B1 (en) |
WO (1) | WO1998036826A1 (en) |
Cited By (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1999059716A2 (en) * | 1998-05-16 | 1999-11-25 | Studiengesellschaft Kohle Mbh | Combinational method for microgram-scale production and characterization of crystalline and amorphous libraries of materials |
WO2000036405A2 (en) * | 1998-12-18 | 2000-06-22 | Symyx Technologies, Inc. | Apparatus and method for characterizing libraries of different materials using x-ray scattering |
WO2001002089A1 (en) * | 1999-07-05 | 2001-01-11 | Sinvent As | Multi-test assembly for evaluating, detecting and monitoring processes at elevated pressure |
EP1172459A2 (en) * | 2000-06-29 | 2002-01-16 | Basf Aktiengesellschaft | Dosing of suspensions on a micro scale for preparation of material samples in combinatorial material research |
US6342185B1 (en) | 1999-12-15 | 2002-01-29 | Uop Llc | Combinatorial catalytic reactor |
WO2002007873A2 (en) * | 2000-07-19 | 2002-01-31 | Uop Llc | Multiautoclave with liner for combinatorial synthesis of zeolites and other materials |
US6368865B1 (en) | 1999-12-15 | 2002-04-09 | Uop Llc | Combinatorial process for performing catalytic chemical reactions |
WO2002030557A2 (en) * | 2000-10-02 | 2002-04-18 | Degussa Ag | Array of autoclaves |
WO2002068264A2 (en) | 2001-02-26 | 2002-09-06 | 3M Innovative Properties Company | Combinatorial library comprising pouches as packages for library members |
US6485692B1 (en) | 1998-12-04 | 2002-11-26 | Symyx Technologies, Inc. | Continuous feed parallel reactor |
EP1287882A2 (en) * | 1998-09-08 | 2003-03-05 | Symyx Technologies, Inc. | Method for screening a catalyst library |
US6576196B1 (en) | 1999-12-15 | 2003-06-10 | Uop Llc | Multiple parallel catalytic reactor assembly |
US6627445B1 (en) | 1999-12-15 | 2003-09-30 | Uop Llc | Process for simultaneously evaluating a plurality of catalysts |
US6770245B2 (en) | 1999-12-15 | 2004-08-03 | Uop Llc | Multiple parallel processing assembly |
US6776963B1 (en) | 1999-12-15 | 2004-08-17 | Uop Llc | Multiple parallel catalytic reactor assembly |
US6808685B2 (en) | 2001-09-17 | 2004-10-26 | Uop Llc | Apparatus and method for generating a plurality of isolated effluents |
WO2005042149A1 (en) * | 2003-10-31 | 2005-05-12 | Uop Llc | A process for preparing crystalline aluminosilicate compositions using charge density matching |
US6989131B2 (en) | 2002-03-12 | 2006-01-24 | Uop Llc | Catalytic reactor with integral evaporator |
US7018589B1 (en) | 2000-07-19 | 2006-03-28 | Symyx Technologies, Inc. | High pressure parallel reactor |
US7063982B1 (en) | 2002-03-12 | 2006-06-20 | Uop Llc | Process of vaporizing and reacting a liquid feed |
US7115231B1 (en) | 1998-06-09 | 2006-10-03 | Symyx Technologies, Inc. | Parallel reactor with knife-edge seal |
US7122159B2 (en) | 2002-04-29 | 2006-10-17 | Symyx Technologies, Inc. | High pressure parallel reactor with individually sealable vessels |
US7141217B2 (en) | 2002-12-05 | 2006-11-28 | Uop Llc | Elevated pressure apparatus and method for generating a plurality of isolated effluents |
US7341872B1 (en) | 2004-04-29 | 2008-03-11 | Uop Llc | Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials |
US7344891B2 (en) | 2002-03-12 | 2008-03-18 | Uop Llc | Process vessel with integral evaporator |
US7514263B2 (en) | 2001-04-02 | 2009-04-07 | 3M Innovative Properties Company | Continuous process for the production of combinatorial libraries of materials |
US7655191B2 (en) | 2007-05-14 | 2010-02-02 | Symyx Solutions, Inc. | Methods for chemical reactions in a parallel batch reactor |
US7807109B2 (en) | 2007-05-14 | 2010-10-05 | Freeslate, Inc. | Parallel batch reactor with pressure monitoring |
Families Citing this family (11)
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US7014049B2 (en) * | 1996-12-23 | 2006-03-21 | Glycorex Transplantation Ab | Device for bio-affinity material |
US6893877B2 (en) | 1998-01-12 | 2005-05-17 | Massachusetts Institute Of Technology | Methods for screening substances in a microwell array |
CN1348396A (en) | 1999-03-19 | 2002-05-08 | 金克克国际有限公司 | Multi-through hole testing plate for high throughput screening |
US20020151040A1 (en) | 2000-02-18 | 2002-10-17 | Matthew O' Keefe | Apparatus and methods for parallel processing of microvolume liquid reactions |
US8277753B2 (en) | 2002-08-23 | 2012-10-02 | Life Technologies Corporation | Microfluidic transfer pin |
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WO2005089945A1 (en) | 2004-03-12 | 2005-09-29 | Biotrove, Inc. | Nanoliter array loading |
DE102007047658A1 (en) * | 2007-10-05 | 2009-04-09 | Hte Ag The High Throughput Experimentation Company | Parallel reactor with pressure lock |
MX2010005882A (en) * | 2008-01-15 | 2010-12-02 | Uop Llc | Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials. |
JP2013240758A (en) * | 2012-05-21 | 2013-12-05 | Tokyo Univ Of Science | Reaction apparatus for performing combinatorial synthesis, combinatorial synthesis system, and combinatorial synthesis method |
FR3063995A1 (en) * | 2017-03-17 | 2018-09-21 | Arkema France | PROCESS FOR MULTI-REACTOR SYNTHESIS OF ZEOLITHE CRYSTALS WITH CONTROLLED GRANULOMETRY |
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-
1997
- 1997-02-20 NO NO970788A patent/NO304355B1/en not_active IP Right Cessation
-
1998
- 1998-02-20 EP EP98904447A patent/EP0968050B1/en not_active Expired - Lifetime
- 1998-02-20 CA CA002281773A patent/CA2281773C/en not_active Expired - Fee Related
- 1998-02-20 DE DE69801813T patent/DE69801813T2/en not_active Expired - Lifetime
- 1998-02-20 AU AU62317/98A patent/AU6231798A/en not_active Abandoned
- 1998-02-20 DK DK98904447T patent/DK0968050T3/en active
- 1998-02-20 JP JP53652198A patent/JP3372553B2/en not_active Expired - Fee Related
- 1998-02-20 WO PCT/NO1998/000051 patent/WO1998036826A1/en active IP Right Grant
- 1998-02-20 US US09/308,562 patent/US6821486B1/en not_active Expired - Fee Related
- 1998-02-20 AT AT98904447T patent/ATE206068T1/en not_active IP Right Cessation
- 1998-02-20 ES ES98904447T patent/ES2166143T3/en not_active Expired - Lifetime
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Also Published As
Publication number | Publication date |
---|---|
NO970788D0 (en) | 1997-02-20 |
CA2281773C (en) | 2003-06-17 |
US6821486B1 (en) | 2004-11-23 |
JP3372553B2 (en) | 2003-02-04 |
JP2001500429A (en) | 2001-01-16 |
EP0968050A1 (en) | 2000-01-05 |
AU6231798A (en) | 1998-09-09 |
DE69801813T2 (en) | 2002-05-16 |
ATE206068T1 (en) | 2001-10-15 |
DK0968050T3 (en) | 2002-01-07 |
ES2166143T3 (en) | 2002-04-01 |
NO304355B1 (en) | 1998-12-07 |
EP0968050B1 (en) | 2001-09-26 |
CA2281773A1 (en) | 1998-08-27 |
NO970788L (en) | 1998-08-21 |
DE69801813D1 (en) | 2001-10-31 |
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