WO2000042633A1 - A method and apparatus of continuously monitoring and recording parameters associated with pulsed ion beam surface treatment processes - Google Patents

A method and apparatus of continuously monitoring and recording parameters associated with pulsed ion beam surface treatment processes Download PDF

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Publication number
WO2000042633A1
WO2000042633A1 PCT/US2000/000810 US0000810W WO0042633A1 WO 2000042633 A1 WO2000042633 A1 WO 2000042633A1 US 0000810 W US0000810 W US 0000810W WO 0042633 A1 WO0042633 A1 WO 0042633A1
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Prior art keywords
ion
diode
ion beam
waveform
gated integrator
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PCT/US2000/000810
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French (fr)
Inventor
Forest E. White
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Quantum Manufacturing Technologies, Inc.
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Priority to AU27253/00A priority Critical patent/AU2725300A/en
Publication of WO2000042633A1 publication Critical patent/WO2000042633A1/en

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    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/48Ion implantation
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process
    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05BCONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
    • G05B23/00Testing or monitoring of control systems or parts thereof
    • G05B23/02Electric testing or monitoring
    • G05B23/0205Electric testing or monitoring by means of a monitoring system capable of detecting and responding to faults
    • G05B23/0218Electric testing or monitoring by means of a monitoring system capable of detecting and responding to faults characterised by the fault detection method dealing with either existing or incipient faults
    • G05B23/0224Process history based detection method, e.g. whereby history implies the availability of large amounts of data
    • G05B23/0227Qualitative history assessment, whereby the type of data acted upon, e.g. waveforms, images or patterns, is not relevant, e.g. rule based assessment; if-then decisions
    • G05B23/0229Qualitative history assessment, whereby the type of data acted upon, e.g. waveforms, images or patterns, is not relevant, e.g. rule based assessment; if-then decisions knowledge based, e.g. expert systems; genetic algorithms
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/30Electron-beam or ion-beam tubes for localised treatment of objects
    • H01J37/304Controlling tubes by information coming from the objects or from the beam, e.g. correction signals
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/30Electron-beam or ion-beam tubes for localised treatment of objects
    • H01J37/317Electron-beam or ion-beam tubes for localised treatment of objects for changing properties of the objects or for applying thin layers thereon, e.g. for ion implantation
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/30Electron or ion beam tubes for processing objects
    • H01J2237/31Processing objects on a macro-scale
    • H01J2237/316Changing physical properties

Definitions

  • an AC power supply 1 provides AC current to a
  • FIG. 2 A typical ion diode assembly is illustrated in Figure 2. As shown in Figure 2, a
  • MAP diode is known in the art, and it may form ions by charging a gaseous medium or
  • Beam uniformity is an important parameter in ensuring adequate
  • cathode current 2) the linear induction adder voltage, 3) the outer ion beam current,
  • the pulsed beam apparatus preferably comprises an ion diode for generating an
  • gated integrator circuits each of which receives a single waveform; a gate interval
  • the gated integrator further comprises a plurality of gain control
  • parameters in a pulsed beam apparatus comprising the steps of: measuring a
  • the monitoring apparatus further comprises a gate interval timer
  • each gated integrator circuit each gain control circuit adjusting the gain of the single
  • Figure 4 illustrates a first embodiment of determining IBEST parameters
  • integrator circuit operates on each of the input signals and generates a plurality of
  • each integrator circuit preferably receives a single input.
  • A/D converter 64 which receives the trigger signal from a delay 66, where the
  • the average cathode current and the average diode voltage are used to calculate the average cathode voltage.
  • step S1 The measured values are continuously
  • This single value quantity can be subsequently used to calculate the above parameters on an average basis, which reflects the operation of

Abstract

A method and apparatus for continuously monitoring and recording parameters associated with pulse ion beam surface treatment (IBEST) processes or with other repetitively pulsed beam systems. The method includes measuring characteristics of an IBEST treatment process as pulsed waveforms, gating and integrating the measured pulsed waveforms over a predetermined period of time to produce a single value, converting the single value into an absolute digital value, and then using digital single value to calculate parameters indicative of the IBEST treatment process. The apparatus may include a gated integrator which receives and integrates the measured pulsed waveforms and a microprocessor which calculates the parameters indicative of the IBEST treatment process or of the performance of a general pulsed beam system. Alternatively, the apparatus may include a hard wired circuit which has a plurality of integrators and a series of circuit components for calculating the parameters indicative of the IBEST treatment process.

Description

A METHOD AND APPARATUS OF CONTINUOUSLY MONITORING AND RECORDING PARAMETERS ASSOCIATED WITH PULSED ION BEAM SURFACE TREATMENT PROCESSES
FIELD OF THE INVENTION
The present invention pertains to a method and apparatus for continuously
monitoring and recording parameters associated with pulsed ion beam surface
treatment (IBEST) processes or other similar beam treatment processes and systems.
More particularly, the present invention pertains to a method and apparatus which uses
a single value quantity for measured characteristics of an IBEST or other pulsed beam
process.
BACKGROUND OF THE INVENTION
Pulsed ion beam energy surface treatment (IBEST) processes are known to
improve the corrosion, wear, hardness and other characteristics of a material. The IBEST process uses intense, high energy (typically 50J - 10KJ), repetitively pulsed
annular ion beams to rapidly deliver energy into the upper layer of a material.
Typically, the repetitive pulses have a frequency of less than 40Hz and a pulse width of
approximately 150 ns FWHM (full width half maximum). The pulsed annular ion beam
is focused, i.e. it converges toward a focal spot, on an object, and rapidly deposits
energy into a upper surface layer (approximately 0.1 μm - 20 μm in thickness) of an
object. The rapid infusion of energy into the upper surface layer of the material causes
near instantaneous melting of the thin upper layer of the material. After the ion beam has melted the thin upper layer, the ion beam is turned off, causing rapid cooling of the
melted layer by virtue of thermal conduction into the bulk of the material. The melted
layer rapidly cools, typically at a rate on the order of 109 degrees per second. The
rapid cooling causes re-solidification of the melted layer into a homogeneous, fine-
grained structure on the surface of the material. The homogeneous, fine-grained
surface layer has superior corrosion, wear, hardness and other characteristics as
compared to the upper surface layer of the original material.
A schematic block diagram of a typical IBEST treatment apparatus is illustrated
in Figure 1. As shown in Figure 1 , an AC power supply 1 provides AC current to a
pulse compression system 2 which compresses the AC current into a very short pulse,
i.e. on the order of 1 μs in width. The structure of the pulse compression system 2 is
known in the art, and it may include a series of serially connected capacitors and
magnetic inductive switches or SCRs (silicon controlled rectifiers). A typical pulse
compression system may be found in U.S. Patent No. 5,532,495 to Bloomquist et al. or
U.S. Patent No. 5,525,805 to Greenly. In Fig. 1 , the pulse compression system 2
provides the compressed pulses to a linear induction voltage adding (LIVA) system 3,
which stores at least two compressed pulses and adds the at least two compressed
pulses together by simultaneously discharging the at least two compressed pulses to
the ion diode unit 4. In this manner, a very short pulse (0.05 μs - 10μs FWHM) of ions
with up to 20KJ total ion energy at ion velocities corresponding to several MEV can be
delivered by the ion diode unit 4. The structure of the LIVA 3 is known in the art, and a
typical LIVA structure can be found in U.S. Patent No.s 5,532,495 or 5,525,805. As is apparent to those of ordinary skill in the art, the power applied to the ion diode unit 4
may be increased by adding stages to the LIVA 3.
A typical ion diode assembly is illustrated in Figure 2. As shown in Figure 2, a
cathode current is provided on the cathode 10 by an inductive field generated by the
anode 12 from the LIVA 3. The cathode current drives an ion diode assembly 14 to
produce an annular ion beam. The ion diode assembly may be a magnetically-confined
anode plasma (MAP) diode or any other suitable type of ion diode. The structure of the
MAP diode is known in the art, and it may form ions by charging a gaseous medium or
by surface arcing between a cathode and an anode. An example of a gaseous ion
forming MAP diode may be found in U.S. Patent No.s 5,532,495 or 5,525,805. The
ions are formed into a ring between an inner anode flux excluder 30 and an outer
anode flux excluder 32. When the voltage pulse from the LIVA is applied between the
cathode 10 and anode 11, ions are projected from between the inner and outer flux
excluders 30 and 32 toward the object to be treated 22. The annular ion beam passes
through an opening 16 in an outer wall 28 of the treatment chamber.
In connection with such an ion diode assembly, the annular ion beam current
may be characterized, for example, by measuring the beam current using outer and
inner B-dot Rogowski coil monitor located in the outer and inner anode flux excluders
30 and 32 respectively. The ion beam current density is preferably measured in
several locations, for example by a fixed Faraday cup 26 located on an outer surface of
a vacuum treatment chamber 18. A table 20 is located in the vacuum treatment
chamber 18 for holding the object to be treated 22. The ion beam current density may also be measured by a set of Faraday cups 24 placed at the plane of treatment
adjacent to the object being treated 22.
In order for the IBEST process to be most effective, the surface of a particular
material should be treated in a prescribed manner. Proper and adequate surface treatment of the workpiece depends upon providing an ion beam to the surface having
the proper characteristics, namely, the ion accelerating voltage, ion beam energy and
energy density should be within a desired range. The beam energy is a measure of the
amount of total energy transported by the ion beam. The energy density is a measure
of the amount of energy transported by the ion beam per unit area. Energy densities
measured at various locations in the footprint of the ion beam indicate the uniformity of
the ion beam profile. Beam uniformity is an important parameter in ensuring adequate
and uniform treatment across the surface of the workpiece. Accordingly, it is
advantageous to control the energy density of the ion beam which is incident on the
surface being treated. In addition, it is often useful to ensure that a particular surface
has been treated in the manner which has been prescribed by the operating system.
Therefore, continuous monitoring of beam parameters, especially those which are
indicative of the energy density of the ion beam, is desirable.
The IBEST treatment process may be characterized by three basic parameters:
1 ) the ion diode voltage; 2) the ion beam current; and 3) the spatial map of the energy
density of the ion beam in the vicinity where it is incident on the surface which is being
treated. The ion diode voltage is indicative of the kinetic energy of each ion in the
beam. The beam current is indicative of the number of ions which comprise the total beam. Using these parameters, the ion beam energy (the energy delivered by the ion beam) as well as the energy density of the ion beam can be ascertained. Additionally,
current density measurements at various locations near the item which is being treated
indicates the uniformity of the ion beam profile.
The parameters which may be monitored to yield the characteristics of the ion
beam and performance of the ion diode system, as indicated in Figure 3, include 1 ) the
cathode current, 2) the linear induction adder voltage, 3) the outer ion beam current,
and 4) the inner ion beam current. These measured parameters are detailed as
follows:
Cathode current (ik(t)): the total electrical current which flows into the ion diode
assembly from the modulator system.
Linear induction adder voltage (Vak(t)): the voltage delivered by the modulator
system which appears across the anode-cathode gap of the ion diode
assembly.
Outer ion beam current (i0(t)): the ion current which flows through an outer Rogowski coil located in the anode outer flux excluder of the ion diode
assembly.
Inner ion beam current (ij(t)): the ion current which flows through an inner Rogowski coil located in the anode inner flux excluder of the ion diode
assembly. These four parameters may subsequently be used to calculate: 1 ) the average
cathode current delivered to the ion diode assembly, 2) the average diode voltage
impressed across the ion diode assembly, 3) the impedance of the ion diode, and 4) the efficiency of the ion diode. In equation form, each of these parameters can be
written as follows:
tP Equation 1 : Average cathode current: Iκ(avg) = 1_ J IK(t)dt tp 0
tP Equation 2: Average diode voltage: Vak(avg) = 1_ J Vak(t)dt
Figure imgf000008_0001
Equation 3: Diode impedance: Zdiode (avg) = Va (avq) lκ (avg)
Equation 4: Ion diode efficiency: ηdiode = In (avg) - lι (avg) " lk(t) "
In these equations, tp is the pulsewidth of the ion beam. These calculated
parameters of the ion beam may subsequently be used to calculate the total energy in
the ion beam.
The energy density of the ion beam may be ascertained by measuring the
current density of the ion beam using the Faraday cups 26 and 24 located in the path of
the ion beam, as shown in Figure 2. Each Faraday cup samples a small potion of the
ion beam and produces a voltage output which is proportional to the current density of
the beam at the location where the ion beam is intercepted by the Faraday cup. Faraday cups are typically placed at several locations throughout the beam path.
Specifically, the Faraday cup 26 samples a small portion of the ion beam as it enters
the treatment chamber. Up to three other Faraday cups 26 may be placed in the
vicinity of the surface which is to be treated. The purpose of the Faraday cups 26 is to
measure the current density of the ion beam in the vicinity of the surface where a
treatment is to take place. Conventionally, the IBEST process uses a pulsed ion beam having a pulsewidth
of approximately 50 ns up to several μs FWHM. Since the IBEST process is a pulsed
process, each of the above noted parameters; voltage, currents and Faraday cup output waveforms, are also pulsed. Typically, the pulse waveforms are recorded and analyzed using high bandwidth digital oscilloscopes or other high speed digitization
instrumentation, as shown in Figure 3. Particularly, a high speed digitizer 36 receives
measured pulse waveforms of the cathode current from a measurement device 35a,
measured pulse waveform of the LIVA voltage from a measurement device 35b,
measured pulse waveforms of the outer ion beam current from a measurement device
35c, measured pulse waveforms of the inner ion beam current from a measurement
device 35d, and measured pulse waveforms from the Faraday cups 24 and 26. Each of
the measured pulse waveforms are digitized by the high speed digitizer 36 and
converted to relatively large arrays which contain both time and amplitude information.
The arrays are stored in a memory 38, which may be any type of commonly known
memory device. The waveforms are subsequently analyzed in a microprocessor 40 by
performing mathematical operations on the arrays using spreadsheets or other known
computer programs.
While such a technique is effective and offers a high level of accuracy, there are some disadvantages associated with it. First, the instrumentation required to digitize the measured signals is relatively expensive and adds to the cost of the IBEST system. Second, the digitized measured signals (data) become relatively large data files which require a large memory capacity to be stored and managed, further adding to the expense of the IBEST system. Third, the creation of large data files, the storage of such files, and the analysis of such large files to calculate the above parameters
requires a significant amount of time, which greatly limits the rate at which an IBEST
treatment process can be performed when data is being continuously collected and
analyzed. Accordingly, in an IBEST process or other repetitively pulsed beam process
in which it is necessary to monitor and record every treatment pulse, implementation of
this technique may significantly limit the repetition rate of the process itself, thus
increasing the time it takes to treat the material. Therefore, an economical method is
required to continuously monitor, characterize and record the above parameters.
SUMMARY AND OBJECTS OF THE INVENTION
It is an object of the invention to provide a cost effective method for monitoring IBEST or other repetitive pulsed beam process treatment parameters.
It is another object of the invention to allow continuous monitoring of IBEST or
other repetitive pulsed beam process treatment parameters without disrupting the
treatment process.
It is yet another object of the invention to allow feedback control of an IBEST or
other repetitive pulsed beam process treatment process.
To achieve the foregoing and other objects and in accordance with the purpose
of the present invention, as embodied and broadly described herein, the apparatus of
this invention may comprise a measurement device which measures a characteristic of
at least one of the pulsed beam apparatus and a beam as a waveform; a gated
integrator which integrates the waveform over a period of time to produce a single
value indicative of the waveform; and a microprocessor which calculates a parameter indicative of an operation of at least one of the pulsed beam apparatus and the beam
based on the single value.
The gated integrator preferably comprises a gated integrator circuit which
receives the waveform; and a gate interval timer which provides a pulse signal to the
gated integrator circuit which defines the period over which the received waveform is
integrated.
The gated integrator preferably further comprises a gain control circuit which
adjusts the gain of the single value according to an attenuation factor of the
measurement device.
The pulsed beam apparatus preferably comprises an ion diode for generating an
ion beam including a generally conical annular ion beam having inner and outer
peripheral regions and an apex approximately at an object to be irradiated, the ion
diode including a cathode, wherein the characteristic which is measured by the
measurement device includes at least one of the following: a current to the cathode, a
voltage across the diode, an ion beam current at the outer peripheral region, an inner
ion beam current at the inner peripheral region, and at least one ion density
measurement of the ion beam in the vicinity of the locations of the object to be
irradiated.
The pulsed beam apparatus preferably comprises an ion diode for generating an
ion beam including a generally conical annular ion beam having inner and outer
peripheral regions and an apex approximately at an object to be irradiated, the diode
including a cathode, and wherein the calculated parameter includes at least one of the
following: average cathode current, impedance of the diode, average diode voltage, fixed energy density of the ion beam, efficiency of the ion diode, and energy density
calculations of at least one location of an ion beam.
The measurement device preferably measures a plurality of characteristics of at
least one of the pulsed beam apparatus and the beam, and provides a plurality of
waveforms respectively, the gated integrator preferably further comprises a plurality of
gated integrator circuits, each of which receives a single waveform; a gate interval
timer which provides a pulse signal to each gated integrator circuit which defines the
period over which the received waveform is integrated.
Preferably the gated integrator further comprises a plurality of gain control
circuits, each gain control circuit of the plurality of gain control circuits corresponding to
each gated integrator circuit, each gain control circuit adjusting the gain of the single
value produced by a corresponding gated integrator circuit according to an attenuation
factor of the measurement device.
In yet another aspect of the invention, a method is provided for monitoring
parameters in a pulsed beam apparatus comprising the steps of: measuring a
characteristic of at least one of the pulsed beam apparatus and the beam as a
waveform; integrating the waveform over a period of time to produce a single value
indicative of the waveform; and calculating a parameter indicative of an operation of at least one of the pulsed beam apparatus and the beam based on the single value.
Preferably the pulsed beam apparatus comprises an ion diode for generating a
generally conical, annular ion beam having inner and outer peripheral regions and an
apex approximately at an object to be irradiated, the ion diode including a cathode, and
the step of measuring a characteristic preferably measures at least one of the following; a current to the cathode, a voltage across the diode, an ion beam current at the outer
peripheral region, an inner ion beam current at the inner peripheral region, and at least
one ion density measurement of the ion beam in the vicinity of the locations of the
object to be irradiated.
Preferably the pulsed beam apparatus comprises an ion diode for generating a
generally conical, annular ion beam having inner and outer peripheral regions and an
apex approximately at an object to be irradiated, the diode including a cathode, and the
step of calculating a parameter preferably calculates at least one of the following;
average cathode current, impedance of the diode, average diode voltage, fixed energy
density of the ion beam, efficiency of the ion diode, and energy density calculations of
at least one location of an ion beam.
Preferably the step of measuring a characteristic measures a plurality of
characteristic values as a plurality of waveforms respectively, the step of integrating
integrates the plurality of waveforms, and the step of calculating calculates a plurality of
parameters.
In yet another aspect of the present invention a monitoring apparatus for
monitoring parameters in a pulsed beam treatment apparatus is provided, the
monitoring apparatus comprising: a measurement device which measures a characteristic of at least one of the pulsed beam apparatus and the beam as a
waveform; a gated integrator circuit which integrates the waveform over a period of time
to produce a single value indicative of the waveform; and a logic circuit which
calculates a parameter indicative of an operation of at least one of the pulsed beam
apparatus and the beam based on the single value. Preferably the monitoring apparatus further comprises a gate interval timer
which provides a pulse signal to the gated integrator circuit which defines the period
over which the received waveform is integrated.
The monitoring apparatus preferably further comprises a gain control circuit
5 which adjusts the gain of the single value according to an attenuation factor of the
measurement device.
Preferably the monitoring apparatus further comprises a plurality of
measurement devices which measure a plurality of characteristics of at least one of the
pulsed beam apparatus and the beam, and provides a plurality of waveforms
o respectively; a plurality of gated integrator circuits which produce a plurality of single
values, wherein each gated integrator receives a single waveform and produces a
single value based on the received waveform; and a gate interval timer which provides
a pulse signal to each gated integrator circuit which defines the period over which the
received waveform is integrated.
5 The monitoring apparatus preferably further comprises a plurality of gain control
circuits, each gain control circuit of the plurality of gain control circuits corresponding to
each gated integrator circuit, each gain control circuit adjusting the gain of the single
value produced by a corresponding gated integrator circuit according to an attenuation
factor of the measurement device; and a plurality of logic circuits which calculate a o plurality of parameters indicative of an operation of at least one of the pulsed beam
apparatus and the beam based on the plurality of single values.
The invention is advantageous over the technique of digitizing measured pulse
waveforms and placing the digitized values into a large array because it provides a single average value for each measured characteristic. This single value quantity can
be subsequently used to calculate the above parameters on an average basis, which
reflects the operation of the treatment system and the overall effectiveness of the
treatment process. In this manner the gated integrator circuits of the present invention
eliminate the need for the high speed digitization instrumentation and a large memory
capacity for storing and managing large data arrays. More particularly, the
advantages of the present invention include: 1 ) the instrumentation required to
implement the present invention is relatively inexpensive compared to high-speed
digitization instrumentation; 2) the single value quantities produced by the present
invention significantly reduces the memory requirements for the data acquisition system
compared to the memory requirements for storing large arrays; and 3) the method
described in this disclosure is relatively fast because it does not require generating and managing an array. As a result, the overall treatment rate is not significantly limited by
the rate at which data can be collected by the data acquisition system.
Additional objects, advantages and novel features of the invention will be set forth in part in the description which follows, and in part will become apparent to those
skilled in the art upon examination of the following or may be learned by practice of the
invention. The objects and advantages of the invention may be realized and attained
by means of the instrumentalities and combinations particularly pointed out in the
appended claims. BRIEF DESCRIPTION OF THE DRAWINGS
The accompanying drawings, which are incorporated in and form a part of the
specification, illustrate several embodiments of the present invention and, together with
the description, serve to explain the principles of the invention. In the drawings:
Figure 1 illustrates a schematic diagram of a typical IBEST treatment apparatus.
Figure 2 illustrates an IBEST surface treatment process. Figure 3 illustrates the prior art technique of determining IBEST parameters.
Figure 4 illustrates a first embodiment of determining IBEST parameters
according to the present invention.
Figure 5 illustrates the operation of a gated integrator circuit according to first
embodiment of the present invention.
Figure 6 illustrates a schematic diagram for determining IBEST parameters
according to a second embodiment of the present invention.
Figure 7 illustrates flow diagram describing the operation of the first and second
embodiments of the present invention.
DETAILED DESCRIPTION OF THE INVENTION
Reference will now be made in detail to the present preferred embodiments of the invention, examples of which are illustrated in the accompanying drawings.
Figure 4 illustrates a first embodiment of the monitoring system 46 of the present
invention. In this embodiment a gated integrator unit 42 receives measured pulsed
waveforms from the IBEST apparatus 5. The gated integrator unit 42 preferably receives measured pulse waveforms of the cathode current from the measurement
device 35a, measured pulse waveforms of the LIVA voltage from the measurement
device 35b, measured pulse waveforms of the outer ion beam current from the
measurement device 35c, measured pulse waveforms of the inner ion beam current
from the measurement device 35d, and measured pulse waveforms from the Faraday
cups 24 and 26. Other measured values may be included according to the particular
demands of the operator of the IBEST apparatus 5 (Fig. 1 ).
The cathode current ik(t) and the LIVA voltage Vak(t) may be determined by
techniques known to those of skill in the art. For example, the outer ion beam current i0(t) may be determined, e.g. using an outer Rogowski coil located in the anode outer
flux excluder 30 (Fig. 2) of the ion diode assembly, and the inner ion beam current ij(t)
may be determined, e.g. using an inner Rogowski coil located in the anode inner flux
excluder 32 (Fig. 2) or by other techniques known to those of skill in the art. The
Faraday cups 26 and 24 are known to those of skill in the art and may be used to
provide measurements of the current density of the ion beam, which in turn are used to
determine the energy density of the ion beam.
The gated integrator unit 42 may be a hard wired circuit, a programmable logic
array such as an EPROM, or it may be a software programmable apparatus. The gated
integrator unit 42 operates on each of the input signals and provides a plurality of
outputs to a microprocessor 44. The plurality of outputs may then be used to determine
the IBEST monitoring parameters, such as average cathode current, the impedance of
the ion diode assembly, the average diode voltage (LVIA voltage), the fixed energy
density of the ion beam, the efficiency of the ion diode assembly, and the energy density at the locations of each of the plurality of Faraday cups represented by number
24 in Figure 2. Other outputs may be included according to the particular demands of
the operator of the IBEST apparatus 5.
Preferably, the gated integrator unit 42 comprises of a plurality of gated
integrator circuits, i.e. one gated integrator circuit for each measured value. Each gated integrator circuit provides a single value quantity which represents the integral of
the measured pulsed waveform over a specified gate interval. These single value
quantities, which are associated with each measured pulsed waveform, may subsequently be processed to yield the above monitoring parameters, which in turn
provide an indication of the operation of the facility and the effectiveness of the
treatment process. In this embodiment, all of the integrator circuits are triggered
simultaneously from a common trigger signal.
An example of a gated integrator circuit according to the present embodiment of
the invention is illustrated in Figure 5. As shown in Figure 5, an input signal V(t) is
delivered to the input of a gated integrator 50. The gated integrator 50 provides at its
output an integrated measurement which is the integral of the input signal defined over
the time interval of the gate signal (t2-tι). The pulsewidth of the gate signal is
determined by a gate interval timer 56. A trigger input signal, which may be delayed by
an appropriate period by a trigger delay 54 according to the delay of the system relative
to the trigger, is used to initiate the start of the gate interval. The width of the gate
pulse is preferably adjusted to an appropriate value, which may be determined empirically by digitizing the waveforms and calculating at least one of the above
monitoring parameters, and optimizing the gate width which correlates best with the calculated data . The integrated measurement output from the gated integrator 50 is
sampled and held by a sample and hold circuit 52, which is triggered by a trigger signal
from the gate interval timer 56. After the integrated measurement is released from the
sample and hold circuit 52, according to the appropriate trigger pulse, the integrated
signal passes through an amplifier 58 which adjusts the gain of the integrated
measurement appropriately. Finally, the integrated measurement is provided to an A/D
converter 59 where the integrated measured signal is converted into an absolute digital
value.
Output signals, derived from each gated integrator circuit are used as inputs to
the microprocessor 44, shown in Figure 4. The microprocessor 44 preferably contains
software which implements all of the mathematical operations necessary to generate the above IBEST parameters. At this point, it should be apparent that single value
quantities are associated with a period of time for each measured pulsed waveform. These single value quantities are further processed to yield the desired operating and
treatment parameters of the particular IBEST apparatus. It should be noted that the
A/D converter 59 (Fig. 5) may also be included in the microprocessor 44.
In the microprocessor 44, the absolute digital value is multiplied by an
appropriate gauge factor to correct for the inherent attenuation of the measurement
devices. The gauge factors will vary for each measurement device, as is known to those of skill in the art. Then, various mathematical operations are performed to
calculate the above IBEST (or other repetitive pulsed beam process) parameters.
Typical mathematical operations, which may be performed are illustrated in equation
form as follows: tgate
Equation 5: Average cathode current: lk(avg) = J_ J ik(t)dt tgate 0
tgate
Equation 6: Average diode voltage: Vak(avg) = J_ J Vak(t)dt tgate 0
Equation 7: Diode impedance: Zdiode (avg) = Vak (avg) lκ (avg)
tgate tgate
J i0(t)dt - J i,(t)dt Equation 8: Average ion current: lι(avg) = __0 0 tπate
Equation 9: Ion diode efficiency: ηdiode = 100 x lι(avg)
Ik(avg)
tgate
Equation 10: Energy density: E(ion beam) = Vak (avg) jVFc..p (t)dt
0
A second embodiment of the present invention is illustrated in Figure 6. The
embodiment in Figure 6 differs from the first embodiment in that a gated integrator unit
60 shown in Figure 6 includes hard wired circuitry to calculate the IBEST parameters
directly, and thus does not require an additional microprocessor for such calculation.
As shown in Figure 6, a series of eight measured pulsed waveforms are
monitored by a data acquisition system 60. Particularly, each of a plurality of gated
integrator circuits 62 receives a different input, e.g. a measured pulse waveform from
the cathode current from measurement device 35a, a measured pulse waveform from
the LIVA voltage from measurement device 35b, a measured pulse waveform from the
outer ion beam current from measurement device 35c, a measured pulse waveform
from the inner ion beam current from measurement device 35d, and a measured pulse waveform from the Faraday cups 24 and 26. Other measured values may be included
according to the particular demands of the operator of the IBEST apparatus 5.
The cathode current ik(t) and the LIVA voltage Vak(t) may be determined by common techniques known to the of skill in the art. The outer ion beam current i0(t)
may be determined, e.g at the outer Rogowski coil located in the anode outer flux
excluder 30 (Fig. 2) of the ion diode assembly, and the inner ion beam current ij(t) may
be determined at the inner Rogowski coil located in the anode inner flux excluder 32
(Fig. 2), by again, using techniques known to those of skill in the art. The gated
integrator circuit operates on each of the input signals and generates a plurality of
parameters indicative of the operation of the IBEST treatment process. The plurality of
parameters preferably include average cathode current, the impedance of the ion diode assembly, the average voltage (LIVA voltage), the fixed energy density of the ion beam,
the efficiency of the ion diode assembly, and the energy density at the locations of
each of the plurality of Faraday cups represented by number 24 in Figure 2. Other
outputs may be included according to the particular demands of the operator of the
particular IBEST apparatus or other repetitive pulsed beam process.
As shown in the example of Figure 6, a series of integrator circuits 62 are
arranged to receive the series of measured pulse waveforms from the particular IBEST
apparatus, each integrator circuit preferably receives a single input. The gate interval
of each integrator circuit is defined by an internal timer circuit which, when triggered by an external trigger, provides a specified gate window. This gate window is
subsequently used to activate the integration of the input signal to the integrator circuit
62. In this embodiment, all of the integrator circuits are triggered simultaneously from a common trigger signal. Alternatively, the trigger of the integrator circuits do not need to
be simultaneous by using a fixed delay time for the A/D converters from the associated gated integrator channel trigger.
The integrator circuits 62 provide their respective outputs to a corresponding
A/D converter 64, which receives the trigger signal from a delay 66, where the
integrated measured signals are converted into an absolute digital value. The absolute
digital value is provided to a corresponding amplifier 68 where it is multiplied by an
appropriate gauge factor 69 to compensate for any attenuation attendant to the
measurement devices 61. In Fig. 6, the gauge factors have been collectively labeled
as 69 although the particular factors will typically vary from one another. At this point,
single value quantities are associated with each measured parameter. These single value quantities are further processed to yield the desired operating and treatment parameters of the typical IBEST apparatus.
Specifically, the integrated pulsed waveforms associated with the cathode
current and the diode voltage are divided by the gate interval received from a timer 96
(is this a timer?) at dividers 70 and 72 respectively, then preferably scaled down, e.g.
by 1000, at dividers 82 and 84 respectively, to yield the average cathode current and
diode voltage. The average cathode current and the average diode voltage are used to
calculate the average impedance of the ion diode by dividing the average diode voltage
by the average cathode current in a divider 80. The average ion current may for
example be calculated by subtracting the integral of the inner ion current from the
integral of the outer ion current by a subtractor 74, and then dividing the obtained
difference by the gate interval at a divider 76. Using the average ion current determined at the divider 76, the diode efficiency may be determined by dividing the
average ion current by the average cathode current at a divider 78, and then preferably
multiplying by a scale factor of 100 to determine a percentage of efficiency at a
multiplier 88. Finally, each of the integrated signals from the Faraday cups 24 and 26
may be multiplied by the average ion diode voltage to yield the energy density of the
ion beam at multipliers 86, 88, 90, 92 and 94. It is should be apparent that in the
illustrated embodiment, all of the calculations are done in the preferable manner using
single value quantities.
Figure 7 is a flow diagram which illustrates the operation of the present
invention. As shown in Figure 7, the desired characteristics of an exemplary IBEST
treatment process are measured in step S1. The measured values are continuously
measured and are in the form of pulsed waveforms. The pulsed waveforms are sampled by a gated integrator circuit and integrated over a predetermined period of
time, as shown in step S2. The predetermined period of time in the gated integrator is
controlled by a timing circuit, as shown in Figure 5. The integration of the waveforms
over the predetermined period of time produces a single value indicative of the area
under the curve of the waveform. This single value is converted to an absolute digital
value in step S3. The gain of the single value may be adjusted to compensate for
attenuation factors in the measurement device. This gain adjustment may be either
before or after the single value is converted to an absolute digital value. As shown in
step S4, the desired IBEST monitoring parameters are calculated based on the
absolute digital values. The calculation of the IBEST monitoring parameters is preferably performed according to equations 5-10 above. It should be noted that above method describes the operation of both the first and second embodiments.
The gated integrator unit 42 in both embodiments of the present invention
provides a single value quantity which is proportional to the area under the input signal
waveform over the gate interval. This single value quantity can be subsequently used to calculate the above parameters on an average basis, which reflects the operation of
the treatment system and the overall effectiveness of the treatment process. In this
manner the gated integrator circuits of the present invention eliminate the need for the
high speed digitization instrumentation and a large memory capacity for storing and managing large data arrays. More particularly, the advantages of the present invention include: 1 ) the instrumentation required to implement the present invention is relatively
inexpensive compared to high-speed digitization instrumentation; 2) the single value quantities produced by the present invention significantly reduces the memory
requirements for the data acquisition system compared to the memory requirements for
storing large arrays; and 3) the present method does not require generating and managing an array and is therefore relatively fast. As a result, the overall treatment
rate is not significantly limited by the rate at which data can be collected by the data
acquisition system.
Since the present invention provides the ability to quickly determine the data required to obtain the above parameters, the invention may be employed to continuously monitor and record parameters associated with an IBEST or other pulsed
beam treatment process during treatment of an item. Particularly, the forgoing
embodiments of the present invention may also be implemented in part of a feedback control loop in an IBEST or other pulsed beam treatment apparatus. In such an implementation, the various treatment parameters would be monitored, recorded and processed to indicate the effectiveness of the treatment process. This information
would then be used to automatically adjust various control parameters of the IBEST or
other pulsed beam treatment apparatus to produce the desired treatment conditions. The foregoing description of the preferred embodiments of the invention have
been presented for purposes of illustration and description. As alluded to throughout the specification, the present invention can also be used to measure, characterize and
control other repetitively pulsed beam systems such as those used to create electron beams, laser beams or ion beams formed by other methods. It is not intended to be exhaustive or to limit the invention to the precise form disclosed, and obviously many modifications and variations are possible in light of the above teaching. It is intended
that the scope of the invention be defined by the claims appended hereto.

Claims

CLAIMSWe claim:
1. A monitoring apparatus for monitoring parameters of a pulsed beam generated by a pulsed beam apparatus, the monitoring apparatus comprising: a measurement device which measures a characteristic of at least one of the pulse beam apparatus and a beam as a waveform;
a gated integrator which integrates the waveform over a period of time to produce a single value indicative of the waveform; and a microprocessor which calculates a parameter indicative of an operation of at
least one of the pulsed beam apparatus and the beam based on the single value.
2. The apparatus according to claim 1 , wherein the gated integrator further
comprises: a gated integrator circuit which receives the waveform; and
a gate interval timer which provides a pulse signal to the gated integrator circuit
which defines the period over which the received waveform is integrated.
3. The apparatus according to claim 2, wherein the gated integrator further
comprises: a gain control circuit which adjusts the gain of the single value according to an
attenuation factor of said measurement device.
1 4. The apparatus according to claim 1 , wherein said pulsed beam apparatus
2 comprises an ion diode for generating an ion beam including a generally conical
3 annular ion beam having inner and outer peripheral regions and an apex approximately
4 at an object to be irradiated, said ion diode including a cathode, wherein the
5 characteristic which is measured by the measurement device includes at least one of β the following: a current to the cathode, a voltage across the diode, an ion beam current
7 at said outer peripheral region, an inner ion beam current at said inner peripheral
8 region, and at least one ion density measurement of the ion beam in the vicinity of the
9 locations of the object to be irradiated.
1 5. The apparatus according to claim 1 , wherein said pulsed beam apparatus
2 comprises an ion diode for generating an ion beam including a generally conical
3 annular ion beam having inner and outer peripheral regions and an apex approximately
4 at an object to be irradiated, said diode including a cathode, and wherein the calculated
5 parameter includes at least one of the following: average cathode current, impedance
β of the diode, average diode voltage, fixed energy density of the ion beam, efficiency of 7 the ion diode, and energy density calculations of at least one location of an ion beam.
1 6. The apparatus according to claim 1 , wherein the measurement device
2 measures a plurality of characteristics of at least one of the pulsed beam apparatus
3 and the beam, and provides a plurality of waveforms respectively, the gated integrator
4 further comprising: a plurality of gated integrator circuits, each of which receives a single waveform; and
a gate interval timer which provides a pulse signal to each gated integrator
circuit which defines the period over which the received waveform is integrated.
7. The apparatus according to claim 6, wherein the gated integrator further comprises:
a plurality of gain control circuits, each gain control circuit of said plurality of
gain control circuits corresponding to each gated integrator circuit, each gain control
circuit adjusting the gain of the single value produced by a corresponding gated
integrator circuit according to an attenuation factor of said measurement device.
8. A method for monitoring parameters in a pulsed beam apparatus, the method comprising the steps of:
measuring a characteristic of at least one of the pulsed beam apparatus and a
beam as a waveform;
integrating the waveform over a period of time to produce a single value
indicative of the waveform; and
calculating a parameter indicative of an operation of at least one of the pulsed
beam apparatus and the beam based on the single value.
9. The method according to claim 8, wherein the pulsed beam apparatus
comprises an ion diode for generating a generally conical, annular ion beam having inner and outer peripheral regions and an apex approximately at an object to be
irradiated, said ion diode including a cathode, wherein the step of measuring a characteristic measures at least one of the following: a current to the cathode, a voltage
across the diode, an ion beam current at said outer peripheral region, an inner ion
beam current at said inner peripheral region, and at least one ion density measurement
of the ion beam in the vicinity of the locations of the object to be irradiated.
10. The apparatus according to claim 8, wherein the pulsed beam apparatus
comprises an ion diode which generates a generally conical, annular ion beam having
inner and outer peripheral regions and an apex approximately at an object to be
irradiated, said ion diode including a cathode, wherein the step of calculating a
parameter calculates at least one of the following: average cathode current, impedance
of the diode, average diode voltage, fixed energy density of the ion beam, efficiency of
the ion diode, and energy density calculations of at least one location of an ion beam.
11. The method according to claim 8, wherein the step of measuring a
characteristic measures a plurality of characteristic values as a plurality of waveforms
respectively, the step of integrating integrates the plurality of waveforms, and the step
of calculating calculates a plurality of parameters.
12. A monitoring apparatus for monitoring parameters in a pulsed beam
treatment apparatus, the monitoring apparatus comprising: a measurement device which measures a characteristic of at least one of the
pulsed beam apparatus and a pulsed beam as a waveform;
a gated integrator circuit which integrates the waveform over a period of time to
produce a single value indicative of the waveform; and
a logic circuit which calculates a parameter indicative of an operation of at least
one of the pulsed beam apparatus and the pulsed beam based on the single value.
13. The apparatus according to claim 12, wherein the gated integrator circuit
receives the waveform, and the monitoring apparatus further comprises;
a gate interval timer which provides a pulse signal to the gated integrator circuit
which defines the period over which the received waveform is integrated.
14. The apparatus according to claim 13, wherein the gated integrator circuit
receives the waveform, and the monitoring apparatus further comprises;
a gain control circuit which adjusts the gain of the single value according to an
attenuation factor of said measurement device.
15. The apparatus according to claim 12, wherein said pulsed beam
apparatus comprises an ion diode for generating a generally conical, annular ion beam
having inner and outer peripheral regions and an apex approximately at an object to be
irradiated, said ion diode including a cathode, wherein the characteristic which is
measured by the measurement device includes at least one of the following: a current
to the cathode, a voltage across the diode, an ion beam current at said outer peripheral region, an inner ion beam current at said inner peripheral region, and at least one ion
density measurement of the ion beam in the vicinity of the locations of the object to be
irradiated.
16. The apparatus according to claim 12, wherein said pulsed beam apparatus comprises an ion diode for generating a generally conical, annular ion beam
having inner and outer peripheral regions and an apex approximately at an object to be
irradiated, said ion diode including a cathode, and wherein the calculated parameter
includes at least one of the following: average cathode current, impedance of the
diode, average diode voltage, fixed energy density of the ion beam, efficiency of the ion
diode, and energy density calculations of at least one location of an ion beam.
17. The apparatus according to claim 12, wherein the monitoring apparatus
further comprises:
a plurality of measurement devices which measure a plurality of characteristics
of at least one of the pulsed beam apparatus and the pulsed beam, and provides a
plurality of waveforms respectively; a plurality of gated integrator circuits which produce a plurality of single values,
wherein each gated integrator receives a single waveform and produces a single value
based on the received waveform; and
a gate interval timer which provides a pulse signal to each gated integrator
circuit which defines the period over which the received waveform is integrated.
18. The apparatus according to claim 17, wherein the monitoring apparatus
further comprises:
a plurality of gain control circuits, each gain control circuit of said plurality of
gain control circuits corresponding to each gated integrator circuit, each gain control
circuit adjusting the gain of the single value produced by a corresponding gated
integrator circuit according to an attenuation factor of said measurement device; and
a plurality of logic circuits which calculate a plurality of parameters indicative of
an operation of at least one of the pulsed beam apparatus and the beam based on the
plurality of single values.
PCT/US2000/000810 1999-01-14 2000-01-14 A method and apparatus of continuously monitoring and recording parameters associated with pulsed ion beam surface treatment processes WO2000042633A1 (en)

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