WO2001028675A1 - Rapid aerogel production process - Google Patents
Rapid aerogel production process Download PDFInfo
- Publication number
- WO2001028675A1 WO2001028675A1 PCT/US2000/041377 US0041377W WO0128675A1 WO 2001028675 A1 WO2001028675 A1 WO 2001028675A1 US 0041377 W US0041377 W US 0041377W WO 0128675 A1 WO0128675 A1 WO 0128675A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- supercritical
- fluid
- pressure
- solvent
- extractor
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/157—After-treatment of gels
- C01B33/158—Purification; Drying; Dehydrating
- C01B33/1585—Dehydration into aerogels
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/0091—Preparation of aerogels, e.g. xerogels
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids
Abstract
Description
Claims
Priority Applications (11)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2001531499A JP2003512277A (en) | 1999-10-21 | 2000-10-20 | Rapid method for producing airgel |
IL14919500A IL149195A0 (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
CA002386897A CA2386897C (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
NZ518014A NZ518014A (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process comprising the application of pressure pulses to hasten the exchange of fluids within the gel |
AU26150/01A AU2615001A (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
KR1020027004531A KR20020062287A (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
BR0014797-4A BR0014797A (en) | 1999-10-21 | 2000-10-20 | Improved quick method for preparing an airgel product |
MXPA02003948A MXPA02003948A (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process. |
EP00989670A EP1230008A1 (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
NO20021855A NO20021855D0 (en) | 1999-10-21 | 2002-04-19 | Rapid aerogel production process |
HK03101533.9A HK1049295A1 (en) | 1999-10-21 | 2003-02-28 | Rapid aerogel production process |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US16046499P | 1999-10-21 | 1999-10-21 | |
US60/160,464 | 1999-10-21 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2001028675A1 true WO2001028675A1 (en) | 2001-04-26 |
Family
ID=22576981
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2000/041377 WO2001028675A1 (en) | 1999-10-21 | 2000-10-20 | Rapid aerogel production process |
Country Status (17)
Country | Link |
---|---|
US (2) | US6670402B1 (en) |
EP (1) | EP1230008A1 (en) |
JP (1) | JP2003512277A (en) |
KR (1) | KR20020062287A (en) |
CN (1) | CN1244397C (en) |
AU (1) | AU2615001A (en) |
BR (1) | BR0014797A (en) |
CA (1) | CA2386897C (en) |
HK (1) | HK1049295A1 (en) |
IL (1) | IL149195A0 (en) |
MX (1) | MXPA02003948A (en) |
NO (1) | NO20021855D0 (en) |
NZ (1) | NZ518014A (en) |
RU (1) | RU2002113291A (en) |
TR (1) | TR200201096T2 (en) |
WO (1) | WO2001028675A1 (en) |
ZA (1) | ZA200202432B (en) |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2013044081A1 (en) * | 2011-09-21 | 2013-03-28 | E. I. Du Pont De Nemours And Company | Energy efficient fermentation process integrated with an extraction process using a supercritical fluid |
US8557214B2 (en) | 2008-05-15 | 2013-10-15 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona | Porous metal oxide particles |
US9242900B2 (en) | 2009-12-01 | 2016-01-26 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Porous geopolymer materials |
US9296654B2 (en) | 2011-09-21 | 2016-03-29 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Geopolymer resin materials, geopolymer materials, and materials produced thereby |
US9308511B2 (en) | 2009-10-14 | 2016-04-12 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Fabricating porous materials using thixotropic gels |
US9365691B2 (en) | 2010-08-06 | 2016-06-14 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Fabricating porous materials using intrepenetrating inorganic-organic composite gels |
US10170759B2 (en) | 2013-06-21 | 2019-01-01 | Arizona Board Of Regents On Behalf Of Arizona State University | Metal oxides from acidic solutions |
WO2019211559A1 (en) | 2018-05-04 | 2019-11-07 | Saint-Gobain Isover | Thermal insulation material comprising partially oxidized graphite oxide particles |
EP3608291A4 (en) * | 2017-11-17 | 2020-04-22 | LG Chem, Ltd. | Method for manufacturing silica aerogel blanket by reusing supercritical waste liquid |
EP3677547A4 (en) * | 2017-11-17 | 2020-10-14 | LG Chem, Ltd. | Method for recycling supercritical waste liquid to be generated during process for manufacturing silica aerogel blanket |
US10829382B2 (en) | 2017-01-20 | 2020-11-10 | Skysong Innovations | Aluminosilicate nanorods |
US10926241B2 (en) | 2014-06-12 | 2021-02-23 | Arizona Board Of Regents On Behalf Of Arizona State University | Carbon dioxide adsorbents |
EP3786112A4 (en) * | 2018-12-13 | 2021-07-21 | Lg Chem, Ltd. | Method for supercritical drying of silica hydrogel blanket |
Families Citing this family (132)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2002113291A (en) * | 1999-10-21 | 2004-03-27 | Эспен Системз, Инк. (Us) | METHOD FOR ACCELERATED PRODUCTION OF AEROGEL |
US6905555B2 (en) * | 2001-02-15 | 2005-06-14 | Micell Technologies, Inc. | Methods for transferring supercritical fluids in microelectronic and other industrial processes |
CN1288172C (en) * | 2001-11-12 | 2006-12-06 | 大金工业株式会社 | Process for producing fluoropolymer |
US6931888B2 (en) * | 2003-02-07 | 2005-08-23 | Ferro Corporation | Lyophilization method and apparatus for producing particles |
BRPI0410083B1 (en) | 2003-05-06 | 2017-12-05 | Aspen Aerogels, Inc. | TUBE-IN-TUBE TYPE APPARATUS FOR THERMAL ISOLATION OF A FLOW LINE |
MY141953A (en) * | 2003-11-10 | 2010-07-30 | Univ Malaysia Tech | Improvements in silica aerogels |
US20050119360A1 (en) * | 2003-11-28 | 2005-06-02 | Kabushiki Kaisha Kobe Seiko Sho | Method for producing porous material |
JP4928090B2 (en) * | 2004-04-28 | 2012-05-09 | 株式会社神戸製鋼所 | Airgel production method |
EP1757559A4 (en) * | 2004-04-28 | 2011-07-27 | Kobe Steel Ltd | Process for producing porous object and apparatus therefor |
WO2006016981A2 (en) * | 2004-07-12 | 2006-02-16 | Ferro Corporation | Production of porous materials by supercritical fluid processing |
US7560062B2 (en) * | 2004-07-12 | 2009-07-14 | Aspen Aerogels, Inc. | High strength, nanoporous bodies reinforced with fibrous materials |
US20070238008A1 (en) * | 2004-08-24 | 2007-10-11 | Hogan Edward J | Aerogel-based vehicle thermal management systems and methods |
US20070102055A1 (en) * | 2005-02-23 | 2007-05-10 | Aspen Aerogels, Inc. | Composites based on macro and nanoporous materials |
PT103257B (en) | 2005-04-05 | 2007-05-31 | Inst Superior Tecnico | METHOD OF SUBCRYTIC PRODUCTION OF SYMBOLS AND ALTERNATIVE AEROGISES HYBRID OF MODIFIED SILICA AND LATEX WITH ALCOXYSILAN GROUPS |
US8461223B2 (en) | 2005-04-07 | 2013-06-11 | Aspen Aerogels, Inc. | Microporous polycyclopentadiene-based aerogels |
US9469739B2 (en) | 2005-04-07 | 2016-10-18 | Aspen Aerogels, Inc. | Microporous polyolefin-based aerogels |
US9476123B2 (en) | 2005-05-31 | 2016-10-25 | Aspen Aerogels, Inc. | Solvent management methods for gel production |
WO2007011750A2 (en) | 2005-07-15 | 2007-01-25 | Aspen Aerogels, Inc. | Secured aerogel composites and method of manufacture thereof |
US7618608B1 (en) * | 2005-12-13 | 2009-11-17 | Keller Companies, Inc. | Aerogel and method of manufacturing same |
WO2007024925A2 (en) * | 2005-08-25 | 2007-03-01 | Keller Companies, Inc. | Aerogel and method of manufacturing same |
JP4758846B2 (en) * | 2005-11-18 | 2011-08-31 | 東京エレクトロン株式会社 | Drying apparatus, drying method, and drying program, and substrate processing apparatus, substrate processing method, and substrate processing program having the same |
US9328190B2 (en) * | 2006-01-18 | 2016-05-03 | Invista North America S.A.R.L. | Non-textile polymer compositions and methods |
KR100741698B1 (en) | 2006-02-28 | 2007-07-23 | 한국생산기술연구원 | Modified aerogel, coating composition comprising it and transparent theraml insulating material therefrom |
US7562534B2 (en) * | 2006-03-23 | 2009-07-21 | Praxair Technology, Inc. | Cryogenic aerogel insulation system |
US20070234589A1 (en) * | 2006-04-05 | 2007-10-11 | Peter Bernegger | Pressurized Drying/Dehydration Apparatus and Method |
WO2007140293A2 (en) | 2006-05-25 | 2007-12-06 | Aspen Aerogels, Inc. | Aerogel compositions with enhanced performance |
US20080014402A1 (en) * | 2006-07-17 | 2008-01-17 | Aspen Aerogels,Inc. | Aerogel insulation systems for pipelines |
US7750056B1 (en) | 2006-10-03 | 2010-07-06 | Sami Daoud | Low-density, high r-value translucent nanocrystallites |
KR100868989B1 (en) * | 2007-05-23 | 2008-11-17 | 엠파워(주) | Method of fabricating superhydrophobic silica chain powders |
KR100869384B1 (en) | 2007-07-09 | 2008-11-19 | 한국생산기술연구원 | Translucent aerogel monolith insulating materials having improved durability and overlap glasses prepared thereof |
US8734931B2 (en) * | 2007-07-23 | 2014-05-27 | 3M Innovative Properties Company | Aerogel composites |
US8702672B2 (en) * | 2007-08-03 | 2014-04-22 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article |
US8197456B2 (en) * | 2007-08-03 | 2012-06-12 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article |
US8251969B2 (en) | 2007-08-03 | 2012-08-28 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article |
US7947027B2 (en) * | 2007-12-28 | 2011-05-24 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article |
US8012137B2 (en) * | 2007-08-03 | 2011-09-06 | Kimberly-Clark Worldwide, Inc. | Packaged body adhering absorbent article and method of applying such article to a wearer |
US8734413B2 (en) | 2007-08-03 | 2014-05-27 | Kimberly-Clark Worldwide, Inc. | Packaged body adhering absorbent article |
US8292862B2 (en) | 2007-08-03 | 2012-10-23 | Kimberly-Clark Worldwide, Inc. | Dynamic fitting body adhering absorbent article |
US8672911B2 (en) | 2007-08-03 | 2014-03-18 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article |
US8062275B2 (en) * | 2007-08-03 | 2011-11-22 | Kimberly Clark Worldwide, Inc. | Body adhering absorbent article and method for donning such article |
US8029489B2 (en) * | 2007-08-03 | 2011-10-04 | Kimberly-Clark Worldwide, Inc. | Body adhering absorbent article and method of adhering such article to a wearer |
KR100911845B1 (en) * | 2007-10-30 | 2009-08-11 | 한국과학기술연구원 | Carbon aerogels for supercapacitors and method for manufacturing the same |
US8240140B2 (en) | 2008-04-09 | 2012-08-14 | Sustainx, Inc. | High-efficiency energy-conversion based on fluid expansion and compression |
US8359856B2 (en) | 2008-04-09 | 2013-01-29 | Sustainx Inc. | Systems and methods for efficient pumping of high-pressure fluids for energy storage and recovery |
US8479505B2 (en) | 2008-04-09 | 2013-07-09 | Sustainx, Inc. | Systems and methods for reducing dead volume in compressed-gas energy storage systems |
US8474255B2 (en) | 2008-04-09 | 2013-07-02 | Sustainx, Inc. | Forming liquid sprays in compressed-gas energy storage systems for effective heat exchange |
US20100307156A1 (en) | 2009-06-04 | 2010-12-09 | Bollinger Benjamin R | Systems and Methods for Improving Drivetrain Efficiency for Compressed Gas Energy Storage and Recovery Systems |
EP2280841A2 (en) | 2008-04-09 | 2011-02-09 | Sustainx, Inc. | Systems and methods for energy storage and recovery using compressed gas |
US7802426B2 (en) | 2008-06-09 | 2010-09-28 | Sustainx, Inc. | System and method for rapid isothermal gas expansion and compression for energy storage |
US8225606B2 (en) | 2008-04-09 | 2012-07-24 | Sustainx, Inc. | Systems and methods for energy storage and recovery using rapid isothermal gas expansion and compression |
US8448433B2 (en) | 2008-04-09 | 2013-05-28 | Sustainx, Inc. | Systems and methods for energy storage and recovery using gas expansion and compression |
US8677744B2 (en) | 2008-04-09 | 2014-03-25 | SustaioX, Inc. | Fluid circulation in energy storage and recovery systems |
US8037678B2 (en) | 2009-09-11 | 2011-10-18 | Sustainx, Inc. | Energy storage and generation systems and methods using coupled cylinder assemblies |
US8250863B2 (en) | 2008-04-09 | 2012-08-28 | Sustainx, Inc. | Heat exchange with compressed gas in energy-storage systems |
US7958731B2 (en) | 2009-01-20 | 2011-06-14 | Sustainx, Inc. | Systems and methods for combined thermal and compressed gas energy conversion systems |
JP2009299760A (en) * | 2008-06-12 | 2009-12-24 | Imae Kogyo Kk | Thermal insulation device of heat apparatus |
US11147722B2 (en) * | 2008-11-10 | 2021-10-19 | Kimberly-Clark Worldwide, Inc. | Absorbent article with a multifunctional acrylate skin-adhesive composition |
US8157780B2 (en) | 2008-12-15 | 2012-04-17 | Kimberly-Clark Worldwide, Inc. | Absorbent article having line of weakness for folding the article |
BRPI0922279A2 (en) * | 2008-12-18 | 2018-06-05 | 3M Innovative Properties Co | "telequel hybrid hybrids". |
US10022468B2 (en) | 2009-02-02 | 2018-07-17 | Kimberly-Clark Worldwide, Inc. | Absorbent articles containing a multifunctional gel |
WO2010105155A2 (en) | 2009-03-12 | 2010-09-16 | Sustainx, Inc. | Systems and methods for improving drivetrain efficiency for compressed gas energy storage |
US8104274B2 (en) | 2009-06-04 | 2012-01-31 | Sustainx, Inc. | Increased power in compressed-gas energy storage and recovery |
WO2011056855A1 (en) | 2009-11-03 | 2011-05-12 | Sustainx, Inc. | Systems and methods for compressed-gas energy storage using coupled cylinder assemblies |
US8507071B1 (en) | 2010-02-11 | 2013-08-13 | Zeroloft Corporation | Sheet insulator with improved resistance to heat transfer by conduction, convection and radiation |
US8171728B2 (en) | 2010-04-08 | 2012-05-08 | Sustainx, Inc. | High-efficiency liquid heat exchange in compressed-gas energy storage systems |
US8191362B2 (en) | 2010-04-08 | 2012-06-05 | Sustainx, Inc. | Systems and methods for reducing dead volume in compressed-gas energy storage systems |
US8234863B2 (en) | 2010-05-14 | 2012-08-07 | Sustainx, Inc. | Forming liquid sprays in compressed-gas energy storage systems for effective heat exchange |
US8495872B2 (en) | 2010-08-20 | 2013-07-30 | Sustainx, Inc. | Energy storage and recovery utilizing low-pressure thermal conditioning for heat exchange with high-pressure gas |
US8952119B2 (en) * | 2010-11-18 | 2015-02-10 | Aspen Aerogels, Inc. | Organically modified hybrid aerogels |
US8906973B2 (en) | 2010-11-30 | 2014-12-09 | Aspen Aerogels, Inc. | Modified hybrid silica aerogels |
US8578708B2 (en) | 2010-11-30 | 2013-11-12 | Sustainx, Inc. | Fluid-flow control in energy storage and recovery systems |
US8945677B2 (en) * | 2011-01-25 | 2015-02-03 | Aspen Aerogels, Inc. | Electronic device manufacture using low-k dielectric materials |
US8758547B2 (en) | 2011-02-08 | 2014-06-24 | Kimberly-Clark Worldwide, Inc. | Method of manufacturing a body adhering absorbent article orientated in the cross-machine direction with reduced curl |
US8764922B2 (en) | 2011-02-08 | 2014-07-01 | Kimberly-Clark Worldwide, Inc. | Method of manufacturing a body adhering absorbent article orientated in the machine direction with reduced curl |
JP2014522460A (en) | 2011-05-17 | 2014-09-04 | サステインエックス, インコーポレイテッド | System and method for efficient two-phase heat transfer in a compressed air energy storage system |
US9133280B2 (en) * | 2011-06-30 | 2015-09-15 | Aspen Aerogels, Inc. | Sulfur-containing organic-inorganic hybrid gel compositions and aerogels |
US9218989B2 (en) | 2011-09-23 | 2015-12-22 | Raytheon Company | Aerogel dielectric layer |
US20130091836A1 (en) | 2011-10-14 | 2013-04-18 | Sustainx, Inc. | Dead-volume management in compressed-gas energy storage and recovery systems |
SI24001A (en) | 2012-02-10 | 2013-08-30 | Aerogel Card D.O.O. | Cryogenic device for transport and storage of liquefaction gas |
US9302247B2 (en) | 2012-04-28 | 2016-04-05 | Aspen Aerogels, Inc. | Aerogel sorbents |
US11053369B2 (en) | 2012-08-10 | 2021-07-06 | Aspen Aerogels, Inc. | Segmented flexible gel composites and rigid panels manufactured therefrom |
CN102964055B (en) * | 2012-10-17 | 2015-04-01 | 厦门纳美特新材料科技有限公司 | Ultra-fast preparation method for highly transparent aerogel glass |
BR112015021190B1 (en) | 2013-03-08 | 2021-10-05 | Aspen Aerogels, Inc | COMPOSITE OF AEROGEL AND LAMINATED PANEL |
FR3007025B1 (en) | 2013-06-14 | 2015-06-19 | Enersens | INSULATING COMPOSITE MATERIALS COMPRISING INORGANIC AEROGEL AND MELAMINE FOAM |
KR101460348B1 (en) * | 2013-10-02 | 2014-11-13 | 서울대학교산학협력단 | A mesoporous nickel-phosphorus-alumina aerogel catalyst, preparation method thereof and production method of hydrogen gas by steam reforming of liquefied natural gas using said catalyst |
US9434831B2 (en) | 2013-11-04 | 2016-09-06 | Aspen Aerogels, Inc. | Benzimidazole based aerogel materials |
CA2928347C (en) | 2013-11-04 | 2017-09-26 | Aspen Aerogels, Inc. | Benzimidazole based aerogel materials |
FR3018207B1 (en) | 2014-03-07 | 2016-03-18 | Enersens | METHOD FOR MANUFACTURING AEROGELS BY DIELECTRIC HEATING |
US11380953B2 (en) | 2014-06-23 | 2022-07-05 | Aspen Aerogels, Inc. | Thin aerogel materials |
MY179571A (en) | 2014-10-03 | 2020-11-11 | Aspen Aerogels Inc | Improved hydrophobic aerogel materials |
GB201502613D0 (en) * | 2015-02-17 | 2015-04-01 | Univ Newcastle | Aerogels |
DE102015107233A1 (en) * | 2015-05-08 | 2016-11-10 | Elringklinger Ag | Airgel and process for producing the ore |
WO2017075554A1 (en) * | 2015-10-29 | 2017-05-04 | Golfetto Michael | Methods freeze drying and composite materials |
US11072145B2 (en) | 2016-01-27 | 2021-07-27 | Aspen Aerogels, Inc. | Laminates comprising reinforced aerogel composites |
CN109019614B (en) * | 2016-05-28 | 2020-05-01 | 郑善 | Rare earth toughened silicon aerogel precursor |
FR3053263B1 (en) * | 2016-07-04 | 2018-08-31 | Keey Aerogrl | CONTINUOUS PROCESS FOR MANUFACTURING AEROGEL |
US10316161B2 (en) | 2017-03-16 | 2019-06-11 | International Business Machines Corporation | Method of making highly porous polyhexahydrotriazines containing antimicrobial agents |
CN110475813A (en) * | 2017-04-13 | 2019-11-19 | 巴斯夫欧洲公司 | The method for preparing porous material |
KR102201310B1 (en) | 2017-09-12 | 2021-01-11 | 주식회사 엘지화학 | Method and apparatus for separating solvent |
KR102242253B1 (en) | 2017-11-13 | 2021-04-21 | 주식회사 엘지화학 | Method for recycling supercritical waste liquid generated during silica aerogel blanket manufacturing process |
CN107824129B (en) * | 2017-12-04 | 2024-03-12 | 陕西盟创纳米新型材料股份有限公司 | Drying system for producing aerogel by alcohol supercritical method |
CN107971299B (en) * | 2017-12-22 | 2023-04-11 | 厦门理工学院 | Supercritical carbon dioxide cleaning equipment and cleaning method thereof |
CN110385091B (en) * | 2018-04-19 | 2021-10-15 | 卢序 | Preparation method of aerogel powder and aerogel powder |
CN108955096B (en) * | 2018-05-22 | 2020-04-17 | 航天特种材料及工艺技术研究所 | Supercritical carbon dioxide drying method |
BR112020024176B1 (en) | 2018-05-31 | 2023-09-26 | Aspen Aerogels, Inc | REINFORCED AEROGEL COMPOSITION |
CN109019611B (en) * | 2018-08-17 | 2020-06-02 | 中南大学 | Block transparent silica aerogel and rapid preparation method and application thereof |
CN109160521B (en) * | 2018-09-10 | 2021-11-19 | 太原理工大学 | Molecular sieve and preparation method thereof, catalyst and preparation method and application thereof |
JP2022500536A (en) | 2018-09-12 | 2022-01-04 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | Continuous supercritical drying method for airgel particles |
US11047517B2 (en) | 2018-10-31 | 2021-06-29 | Praxair Technology, Inc. | Modular vacuum insulated piping |
KR102559049B1 (en) | 2018-12-20 | 2023-07-25 | 주식회사 엘지화학 | Method for preparing silica aerogel blancket |
MX2021010330A (en) | 2019-02-27 | 2021-11-04 | Aspen Aerogels Inc | Carbon aerogel-based electrode materials and methods of manufacture thereof. |
CA3134169A1 (en) | 2019-03-22 | 2020-10-01 | Aspen Aerogels, Inc. | Carbon aerogel-based cathodes for lithium-air batteries |
JP2022527195A (en) | 2019-03-22 | 2022-05-31 | アスペン アエロジェルズ,インコーポレイテッド | Carbon airgel cathode for lithium-sulfur batteries |
CN110075769B (en) * | 2019-05-24 | 2021-08-17 | 陕西科技大学 | Sol preparation process and device for making xeromyces dormancy breaking |
CN110395946B (en) * | 2019-05-27 | 2021-09-28 | 常州大学怀德学院 | Preparation method of aerogel-vitrified microsphere composite mortar for external wall heat insulation |
JP2023506094A (en) | 2019-12-02 | 2023-02-14 | アスペン アエロジェルズ,インコーポレイテッド | Components and systems for managing thermal runaway problems in electric vehicle batteries |
IL293574A (en) | 2019-12-02 | 2022-08-01 | Aspen Aerogels Inc | Aerogel-based components and systems for electric vehicle thermal management |
AU2021205263A1 (en) | 2020-01-07 | 2022-08-04 | Aspen Aerogels Inc. | Battery thermal management member |
MX2022012352A (en) | 2020-04-06 | 2022-10-27 | Aspen Aerogels Inc | Improved aerogel compositions and methods. |
JP2023539001A (en) | 2020-08-25 | 2023-09-13 | アスペン エアロゲルズ,インコーポレイティド | Polyimide bead material and its manufacturing method |
CN112500606B (en) * | 2020-12-02 | 2022-02-15 | 中国工程物理研究院激光聚变研究中心 | Method for preparing gradient density aerogel by adopting double diffusion convection |
KR20230116006A (en) | 2020-12-11 | 2023-08-03 | 아스펜 에어로겔, 인코포레이티드 | Aqueous process for producing polyamic acid gels, polymate gels, polyimide gels and porous carbon materials |
WO2022125825A2 (en) | 2020-12-11 | 2022-06-16 | Aspen Aerogels, Inc. | Carbon aerogel-based lithium metal anode materials and methods of manufacture thereof |
WO2022125839A1 (en) | 2020-12-11 | 2022-06-16 | Aspen Aerogels, Inc. | Water co-catalyst for polyimide process |
EP4259705A1 (en) | 2020-12-11 | 2023-10-18 | Aspen Aerogels Inc. | Water co-catalyst for polyimide process |
WO2022144736A1 (en) | 2020-12-30 | 2022-07-07 | Aspen Aerogels, Inc. | Fibrous carbon aerogels coated with nano-thin silicon as lithium battery anodes |
EP4292151A1 (en) | 2021-02-15 | 2023-12-20 | Aspen Aerogels Inc. | Fibrillar carbon-silicon composite materials and methods of manufacture thereof |
WO2023192443A1 (en) | 2022-04-01 | 2023-10-05 | Aspen Aerogels, Inc. | Carbon powder containing lithium iron phosphate cathode materials |
WO2023244287A1 (en) | 2022-06-15 | 2023-12-21 | Aspen Aerogels, Inc. | Aqueous process for preparing polyamic acids and polyamic acid related gel materials |
WO2024050017A1 (en) | 2022-09-01 | 2024-03-07 | Bartels Joshua | High strength aerogel material and method |
WO2024073165A1 (en) | 2022-09-28 | 2024-04-04 | Aspen Aerogels, Inc. | Porous carbon materials comprising a carbon additive |
WO2024081368A1 (en) | 2022-10-13 | 2024-04-18 | Aspen Aerogels, Inc. | Compressed aerogel composite and method of making |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0586013A2 (en) * | 1992-09-01 | 1994-03-09 | ENICHEM S.p.A. | Method for preparing optical components and devices in their final or nearly final dimensions, and products obtained thereby |
EP0640564A1 (en) * | 1993-08-19 | 1995-03-01 | Siemens Aktiengesellschaft | Process for the preparation of a hydrophobic aerogel |
DE19810565A1 (en) * | 1998-03-11 | 1999-09-16 | Basf Ag | Economical drying of microporous particles containing fluid e.g. inorganic, organic or polymer gel |
Family Cites Families (17)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2427348A (en) * | 1941-08-19 | 1947-09-16 | Bell Telephone Labor Inc | Piezoelectric vibrator |
US2993005A (en) * | 1957-09-03 | 1961-07-18 | Monsanto Chemicals | Manufacture of aerogels |
DE3429671A1 (en) * | 1984-08-11 | 1986-02-20 | Basf Ag, 6700 Ludwigshafen | METHOD FOR PRODUCING AEROGELS |
DE3440018C1 (en) * | 1984-11-02 | 1986-03-20 | Kali-Chemie Ag, 3000 Hannover | Process for dewatering water-containing, inorganic oxide gels |
US4619908A (en) * | 1984-12-24 | 1986-10-28 | Stauffer Chemical Company | Non-aged inorganic oxide-containing aerogels and their preparation |
US5207814A (en) * | 1989-02-10 | 1993-05-04 | Enichem S.P.A. | Process for preparing monoliths of aerogels of metal oxides |
DE3914850A1 (en) * | 1989-05-05 | 1990-11-08 | Basf Ag | THERMAL INSULATING MATERIAL BASED ON PIGMENT-BASED SILICONE ACULATE ARRAY |
US5409683A (en) * | 1990-08-23 | 1995-04-25 | Regents Of The University Of California | Method for producing metal oxide aerogels |
JP2532907Y2 (en) * | 1992-02-10 | 1997-04-16 | 動力炉・核燃料開発事業団 | Wide pulse nozzle |
JP2725573B2 (en) * | 1993-11-12 | 1998-03-11 | 松下電工株式会社 | Manufacturing method of hydrophobic airgel |
US5473826A (en) * | 1994-08-19 | 1995-12-12 | Yazaki Corporation | Process for drying sol-gel derived porous bodies at elevated subcritical temperatures and pressures |
EP0783371B1 (en) * | 1994-09-22 | 1998-06-24 | F. Hoffmann-La Roche Ag | Heterogeneous catalysts |
FR2736342B1 (en) * | 1995-07-07 | 1999-01-29 | Univ Claude Bernard Lyon | PROCESS FOR THE MANUFACTURE OF MONOLITHIC SILICA AEROGELS AND THUS OBTAINED SILICA AEROGELS |
FR2766170B1 (en) * | 1997-07-17 | 1999-09-24 | Alsthom Cge Alcatel | IMPROVED PROCESS FOR PRODUCING SILICA POWDER |
US5958363A (en) * | 1998-10-29 | 1999-09-28 | The Regents Of The University Of California | Method for making monolithic metal oxide aerogels |
RU2002113291A (en) * | 1999-10-21 | 2004-03-27 | Эспен Системз, Инк. (Us) | METHOD FOR ACCELERATED PRODUCTION OF AEROGEL |
US6729042B2 (en) * | 2001-04-23 | 2004-05-04 | Aspen Systems, Inc. | Enhancement of fluid replacement in porous media through pressure modulation |
-
2000
- 2000-10-20 RU RU2002113291/15A patent/RU2002113291A/en not_active Application Discontinuation
- 2000-10-20 CA CA002386897A patent/CA2386897C/en not_active Expired - Fee Related
- 2000-10-20 MX MXPA02003948A patent/MXPA02003948A/en unknown
- 2000-10-20 CN CNB008147000A patent/CN1244397C/en not_active Expired - Fee Related
- 2000-10-20 US US09/693,390 patent/US6670402B1/en not_active Expired - Lifetime
- 2000-10-20 IL IL14919500A patent/IL149195A0/en not_active IP Right Cessation
- 2000-10-20 KR KR1020027004531A patent/KR20020062287A/en not_active Application Discontinuation
- 2000-10-20 WO PCT/US2000/041377 patent/WO2001028675A1/en not_active Application Discontinuation
- 2000-10-20 BR BR0014797-4A patent/BR0014797A/en not_active IP Right Cessation
- 2000-10-20 JP JP2001531499A patent/JP2003512277A/en active Pending
- 2000-10-20 NZ NZ518014A patent/NZ518014A/en unknown
- 2000-10-20 TR TR2002/01096T patent/TR200201096T2/en unknown
- 2000-10-20 EP EP00989670A patent/EP1230008A1/en not_active Withdrawn
- 2000-10-20 AU AU26150/01A patent/AU2615001A/en not_active Abandoned
-
2002
- 2002-03-26 ZA ZA200202432A patent/ZA200202432B/en unknown
- 2002-04-19 NO NO20021855A patent/NO20021855D0/en unknown
-
2003
- 2003-02-28 HK HK03101533.9A patent/HK1049295A1/en unknown
- 2003-07-16 US US10/620,933 patent/US20040087670A1/en not_active Abandoned
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0586013A2 (en) * | 1992-09-01 | 1994-03-09 | ENICHEM S.p.A. | Method for preparing optical components and devices in their final or nearly final dimensions, and products obtained thereby |
EP0640564A1 (en) * | 1993-08-19 | 1995-03-01 | Siemens Aktiengesellschaft | Process for the preparation of a hydrophobic aerogel |
DE19810565A1 (en) * | 1998-03-11 | 1999-09-16 | Basf Ag | Economical drying of microporous particles containing fluid e.g. inorganic, organic or polymer gel |
Cited By (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8557214B2 (en) | 2008-05-15 | 2013-10-15 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona | Porous metal oxide particles |
US9308511B2 (en) | 2009-10-14 | 2016-04-12 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Fabricating porous materials using thixotropic gels |
US9242900B2 (en) | 2009-12-01 | 2016-01-26 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Porous geopolymer materials |
US9365691B2 (en) | 2010-08-06 | 2016-06-14 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Fabricating porous materials using intrepenetrating inorganic-organic composite gels |
WO2013044081A1 (en) * | 2011-09-21 | 2013-03-28 | E. I. Du Pont De Nemours And Company | Energy efficient fermentation process integrated with an extraction process using a supercritical fluid |
US9296654B2 (en) | 2011-09-21 | 2016-03-29 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Geopolymer resin materials, geopolymer materials, and materials produced thereby |
US9862644B2 (en) | 2011-09-21 | 2018-01-09 | Arizona Board Of Regents, A Body Corporate Of The State Of Arizona Acting For And On Behalf Of Arizona State University | Geopolymer resin materials, geopolymer materials, and materials produced thereby |
US10170759B2 (en) | 2013-06-21 | 2019-01-01 | Arizona Board Of Regents On Behalf Of Arizona State University | Metal oxides from acidic solutions |
US10926241B2 (en) | 2014-06-12 | 2021-02-23 | Arizona Board Of Regents On Behalf Of Arizona State University | Carbon dioxide adsorbents |
US11745163B2 (en) | 2014-06-12 | 2023-09-05 | Arizona Board Of Regents On Behalf Of Arizona State University | Carbon dioxide adsorbents |
US10829382B2 (en) | 2017-01-20 | 2020-11-10 | Skysong Innovations | Aluminosilicate nanorods |
EP3608291A4 (en) * | 2017-11-17 | 2020-04-22 | LG Chem, Ltd. | Method for manufacturing silica aerogel blanket by reusing supercritical waste liquid |
EP3677547A4 (en) * | 2017-11-17 | 2020-10-14 | LG Chem, Ltd. | Method for recycling supercritical waste liquid to be generated during process for manufacturing silica aerogel blanket |
US11760645B2 (en) | 2017-11-17 | 2023-09-19 | Lg Chem, Ltd. | Method for recycling supercritical waste liquid generated during process of producing silica aerogel blanket |
US11891306B2 (en) | 2017-11-17 | 2024-02-06 | Lg Chem, Ltd. | Method for producing silica aerogel blanket by reusing supercritical waste liquid |
WO2019211559A1 (en) | 2018-05-04 | 2019-11-07 | Saint-Gobain Isover | Thermal insulation material comprising partially oxidized graphite oxide particles |
EP3786112A4 (en) * | 2018-12-13 | 2021-07-21 | Lg Chem, Ltd. | Method for supercritical drying of silica hydrogel blanket |
US11365125B2 (en) | 2018-12-13 | 2022-06-21 | Lg Chem, Ltd. | Supercritical drying method for silica wet gel blanket |
Also Published As
Publication number | Publication date |
---|---|
JP2003512277A (en) | 2003-04-02 |
TR200201096T2 (en) | 2002-09-23 |
US6670402B1 (en) | 2003-12-30 |
CN1244397C (en) | 2006-03-08 |
AU2615001A (en) | 2001-04-30 |
RU2002113291A (en) | 2004-03-27 |
NZ518014A (en) | 2004-02-27 |
CA2386897A1 (en) | 2001-04-26 |
NO20021855L (en) | 2002-04-19 |
CN1382070A (en) | 2002-11-27 |
EP1230008A1 (en) | 2002-08-14 |
HK1049295A1 (en) | 2003-05-09 |
NO20021855D0 (en) | 2002-04-19 |
BR0014797A (en) | 2002-06-11 |
IL149195A0 (en) | 2002-11-10 |
ZA200202432B (en) | 2003-09-23 |
US20040087670A1 (en) | 2004-05-06 |
MXPA02003948A (en) | 2004-09-06 |
KR20020062287A (en) | 2002-07-25 |
CA2386897C (en) | 2007-08-07 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CA2386897C (en) | Rapid aerogel production process | |
JP6388918B2 (en) | Airgel production method and apparatus | |
Pajonk | Drying methods preserving the textural properties of gels | |
JP4503831B2 (en) | Method for producing a ceramic foam | |
US5473826A (en) | Process for drying sol-gel derived porous bodies at elevated subcritical temperatures and pressures | |
JPH11500473A (en) | Method for rapid production of microporous and mesoporous materials | |
CN109019611B (en) | Block transparent silica aerogel and rapid preparation method and application thereof | |
US6729042B2 (en) | Enhancement of fluid replacement in porous media through pressure modulation | |
Woignier et al. | Aerogel processing | |
JP5432946B2 (en) | Airgel production equipment | |
JP4928090B2 (en) | Airgel production method | |
CN113666712A (en) | Reaction kettle and preparation method of silicon dioxide aerogel heat-insulation composite material | |
Rangarajan et al. | Production of aerogels | |
US6077876A (en) | Process for high temperature production of organic aerogels | |
Kumar et al. | Synthesis of high surface area silica by solvent exchange in alkoxy derived silica gels | |
Yoda et al. | Preparation of SiO2-TiO2 aerogels using supercritical impregnation | |
EP1551777B1 (en) | Method for preparation of bulk shaped foam articles | |
CN110553470A (en) | Supercritical drying method for preparing ultra-low density aerogel and product prepared by same | |
JP2021526122A (en) | Supercritical drying method for silica wet gel blanket | |
CN110339594B (en) | Direct preparation of SiO2Method for preparing monolithic aerogel column | |
CN116876097A (en) | Polysiloxane aerogel fiber and preparation method thereof | |
Rao et al. | Influence of Sol-Gel Parameters on Transparency and Monolithicity of Silica Aerogels |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
AK | Designated states |
Kind code of ref document: A1 Designated state(s): AE AL AM AT AU AZ BA BB BG BR BY CA CH CN CR CU CZ DE DK DM EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX NO NZ PL PT RO RU SD SE SG SI SK SL TJ TM TR TT TZ UA UG UZ VN YU ZA ZW |
|
AL | Designated countries for regional patents |
Kind code of ref document: A1 Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZW AM AZ BY KG KZ MD RU TJ TM AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE BF BJ CF CG CI CM GA GN GW ML MR NE SN TD TG |
|
121 | Ep: the epo has been informed by wipo that ep was designated in this application | ||
DFPE | Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101) | ||
WWE | Wipo information: entry into national phase |
Ref document number: 518014 Country of ref document: NZ |
|
WWE | Wipo information: entry into national phase |
Ref document number: 2386897 Country of ref document: CA |
|
WWE | Wipo information: entry into national phase |
Ref document number: 1020027004531 Country of ref document: KR Ref document number: 2000989670 Country of ref document: EP |
|
ENP | Entry into the national phase |
Ref document number: 2001 531499 Country of ref document: JP Kind code of ref document: A |
|
WWE | Wipo information: entry into national phase |
Ref document number: IN/PCT/2002/474/KOL Country of ref document: IN |
|
WWE | Wipo information: entry into national phase |
Ref document number: 149195 Country of ref document: IL |
|
WWE | Wipo information: entry into national phase |
Ref document number: PV2002-1387 Country of ref document: CZ Ref document number: PA/a/2002/003948 Country of ref document: MX Ref document number: 2002/01096 Country of ref document: TR |
|
WWE | Wipo information: entry into national phase |
Ref document number: 008147000 Country of ref document: CN |
|
WWE | Wipo information: entry into national phase |
Ref document number: 26150/01 Country of ref document: AU |
|
ENP | Entry into the national phase |
Ref document number: 2002 2002113291 Country of ref document: RU Kind code of ref document: A |
|
WWP | Wipo information: published in national office |
Ref document number: 1020027004531 Country of ref document: KR |
|
WWP | Wipo information: published in national office |
Ref document number: 2000989670 Country of ref document: EP |
|
REG | Reference to national code |
Ref country code: DE Ref legal event code: 8642 |
|
WWP | Wipo information: published in national office |
Ref document number: PV2002-1387 Country of ref document: CZ |
|
WWP | Wipo information: published in national office |
Ref document number: 518014 Country of ref document: NZ |
|
WWG | Wipo information: grant in national office |
Ref document number: 518014 Country of ref document: NZ |
|
WWW | Wipo information: withdrawn in national office |
Ref document number: 2000989670 Country of ref document: EP |