Description
L:GU PRECISION ASER ONITOR FOR MANUFACTURE OF OPTICAL COATINGS
AND METHOD FOR ITS USE
Technical Field
Tre present invention relates to a method and apparatus for monitoring a manufacturing process, and more particularly, no a method ana apparatus for high precision monitoring of the manufacture of optical coatings.
Bac-cαround of the Invention
Thin film coatings deposited on glass or similar substrates are useα extensively in optical technology to tailor the behavior of optical components. Such coatings are used to increase or decrease reflectivity, to modify the polarization of light, or to filter or otherwise control the wavelength spectrum cf light Demg processed.
Coatings of dielectric materials (as opposed to metallic coatings) offer the highest and most flexible performance to the optical components manufacturer. These coatings frequently consist of multiple discrete layers of differing materials, wmcn are applied successively to the substrate. Such coatings are generally manufactured by vacuum deposition or sputtering of material onto the substrate. In order to achieve the desired component performance, the optical thickness of the individual layers of the coatings must be precisely controlled.
It has long been understood that the optical thickness of coating layers can be monitored during deposition by observing tne optical transmission through the part, and, hence, the coating being manufactured. U.S. Patent 4,024,291 describes an embodiment of this concept which is specifically for the control of vapor deposition. U.S. Patent 4,336,119 essentially describes
the application of the same measurement approach to coating deposition by reactive sputtering.
In all of the known optical monitoring approaches, light is emitted from a light source, transmitteα through or reflected from the part being monitored, and subsequently measured at an optical detector. Most optical coatings are designed as a stack of layers alternating between high and low index-of-refraction materials. These layers are usually 1/4 wavelength m optical thickness, or some multiple of 1/4 wavelength, although it is not necessary that they be. As the optical thickness of a layer that is currently being depositeα approaches 1/4 wavelengtn, the transmission (or reflectance) through the part reaches a turning point, either a maximum or a minimum. Depositior should be stopped accurately at the turning point, ana a new layer or another material begun.
Transmission through a partially complete coating may become quite small. For a narrow bandpass filter, transmission may be less than 1 percent, with accurate location of the turning points still required. The science of the optical monitoring approach requires a controlled wavelength spectrum of the light being measured, since the interaction between the coating's optical thickness and the light depends on wavelength. The allowable width of the optical spectrum used for the measurement depends strongly on the type and specification of the component being manufactured.
In the past, this function has been obtained by use of an incandescent light source, coupled with an optical monocnromator that filters out a portion of the broad spectrum emitted by the incandescent lamp. As the monochromator transmission passband is made narrower, the total optical power from the light source that is transmitted through the system is reduced proportionately. This effect, along with low transmission of a partial coating and the need for very high precision
measurements, places important practical limits on the minimum bandwidth that can be obtained from a given monitoring system. As the received optical power is reduced, measurement noise and error increase, reducing the useful precision of the monitor. Manufacture of some components requires a combination of very narrow bandwidth and very high precision that cannot oe easily obtained from "white light" optical monitors because of these effects .
It is possible to overcome the limitation on monitor bandwidth by using a laser light source m place of tne filtered incandescent source. This disclosure describes the implementation of a complete, high precision coating monitor system using a laser light source to obtain very narrow measurement bandwidth. The inventive dual-beam laser spectrometer apparatus described m detail subsequently provides variable nulling which can reduce the adverse effects of cnanges m the intensity of the laser light source and allows high-precision measurements of optical transmission through thin film coatings by means of the use of a precision tracking gain-programmable amplifier. Also, the appropriate use of optical frequency modulation reduces errors induced by parasitic optical interference within the measurement system.
Summary of the Invention
According to one aspect, the invention is an apparatus for monitoring the optical thickness of a layer of an optical coating that is being deposited on a medium. The apparatus includes a source of electromagnetic energy to produce electromagnetic energy having a spectral brightness substantially greater than a thermal source of electromagnetic energy, and a divider to divide the electromagnetic energy into a reference portion and a second portion.
The apparatus also includes a reference detector to receive the reference portion of the electromagnetic energy ana to produce a reference signal response thereto, a transmitter to transmit the second portion of the electromagnetic energy to the optical coating, a receiver to receive the second portion of the electromagnetic energy after the second portion of the electromagnetic energy has been affected by the optical coating and to produce a received energy signal m response thereto, and a detector to process the received energy signal and to produce a detector signal response thereto.
The apparatus further includes a first gam-programmable preamplifier to receive the reference signal and a first ga control signal and produce a first output signal m response tnereto, a second gam-programmable preamplifier to receive the detector signal and a second gam control signal and produce a second output signal in response thereto, and a comparator to receive the first and second output signals and produce a comparison signal representing their difference. In addition, the apparatus includes an electronic circuit to receive the comparison signal and to produce the first and second gam control signals and a transmission monitoring signal m response thereto, the electronic circuit operating to drive the comparison signal toward zero by controlling the first and second gam control signals, and generating the transmission monitoring signal by analyzing the changes in the first and second gam control signals needed to drive the comparison signal toward zero.
According to another aspect, the invention is an apparatus for controlling the deposited optical thicknesses of layers of an optical coating that is being deposited on a medium to a predetermined thickness in accordance with a predetermined coating design. The apparatus includes a source of electromagnetic energy to produce electromagnetic energy having
a spectral brightness substantially greater than a tnermal source of electromagnetic energy, a αivider to αivide the electromagnetic energy into a reference portic and a second portion, and a reference detector to receive tre reference portion of the electromagnetic energy and to produce a reference signal m response thereto.
The apparatus also includes a transmitter to transmit the second portion of the electromagnetic energy to the optical coating, a receiver to receive the second portion of the electromagnetic energy after the second portior of the electromagnetic energy has been affected by the optical coating and to produce a received energy signal in response thereto, and a detector to process the received energy signal and to produce a detector signal m response thereto. The apparatus further includes a first gam-programmable preamplifier to receive the reference signal and a first gam control signal and produce a first output signal in response thereto, a second gam-programmable preamplifier to receive the detector signal and a second gam control signal and produce a second output signal m response thereto, and a comparator to receive the first and second output signals ana produce a comparison signal representing their difference.
In addition, the apparatus includes an electronic circuit, coating deposition control circuit, and an optical coating depositor. The electronic circuit receives the comparison signal and produces the first and second gam control signals and a transmission monitoring signal m response thereto. The electronic circuit operates to drive the comparison signal toward zero by controlling the first and second ga control signals, and generates the transmission monitoring signal by analyzing the changes m the first and second gam control signals needed to drive the comparison signal toward zero. The coating deposition control circuit receives the
transmission monitoring signal, a deposition status information signal, and process design information and produces a process control signal m response thereto. The optical coating depositor αeposits the optical coating on the medium, the optical coating depositor being responsive to the process control signal, and produces the deposition status information signal, whereby the first and second ga control signals are indicative of the thickness of the optical coating on the medium, so that the optical coating depositor terminates deposition of the optical coating when the optical coating has the predetermined thickness.
According to a further aspect, the invention is a metnod for analyzing the thickness of an optical coating on a meαmm . The method includes the steps of a > producing electromagnetic energy having a spectral brightness substantially greatei than a thermal source of electromagnetic energy and b) dividing the electromagnetic energy into a reference portion and a second portion. The method also includes c) receiving the reference portion of the electromagnetic energy and producing a reference signal in response thereto, d) transmitting the second portion of the electromagnetic energy to the optical coating, e) receiving the second portion of the electromagnetic energy after the second portion of the electromagnetic energy has been affected by the optical coating and producing a received energy signal m response thereto, and f) processing the received energy signal and producing a detector signal m response thereto .
The method further includes the steps of g) receiving the reference signal and a first gam control signal and producing a first output signal m response thereto, h) receiving the received energy signal and a second gam control signal and producing a second output signal in response thereto, and I) receiving the reference and detector signals and producing a
comparison signal representing their difference. The method still further includes the steps of j ) receiving the comparison signal and producing the first and second gam control signals ana a transmission monitoring signal response thereto, K) anvmg the comparison signal toward zero by controlling the first and second gam control signals, and 1) generating the transmission monitoring signal by analyzing the changes m the first and second gam control signals needed to drive the comparison signal toward zero. According to a still further aspect, the invention is a method for depositing an optical coating on a medium, the optical coating having a predetermined thickness. The method includes the steps of a) providing a source of electromagnetic energy having a spectral brightness substantially greater than a thermal source of electromagnetic energy and b) dividing the electromagnetic energy into a reference portion and a second portion. The method also includes the steps of c) receiving the reference portion of the electromagnetic energy and producing a reference signal m response thereto, d) transmitting the electromagnetic energy to the optical coating, e) receiving the second portion of the electromagnetic energy after the second portion of the electromagnetic energy has been affected by the optical coating, and f) processing the electromagnetic energy received by the receiver and producing a detector signal m response thereto.
The method further includes the steps of g) receiving the reference and detector signals and a gam control signal, and producing a comparison signal in response to the reference and detector signals, h) transmitting the frequency control signal to the source of the electromagnetic energy to determine the instantaneous substantially single frequency of electromagnetic energy produced by the source of the electromagnetic energy, I) transmitting the amplitude modulation signal to the source of
the modulation to determine the instantaneous modulation of tne electromagnetic energy produced by the source of the electromagnetic energy, the amplitude modulation signal also oemg transmitted to the amplifier, ; transmitting the comparison signal to the amplifier, and k) receiving tne gam control signal and producing the comparison signal response thereto, whereby the source produces the electromagnetic energy at the predetermined frequency, and the gam control signal is transmitted, the ga control signal being indicative of the tnickness of the optical coating on the medium.
The method also includes the step of 1) depositing the octxcal coat g on the medium, the deposition being responsive to the gam control signal, whereby the first and second gam control signals are indicative of the thickness of the optical coating on the medium, so that the deposition of the optical coating terminates when the optical coatmg has the predetermined thickness.
According to yet another aspect, the invention is a method for controlling the deposited optical thickness of each layer of an optical coatmg that is being deposited on a medium to a predetermined thickness m accordance with a predetermined coatmg design. The method includes the steps of a) producing electromagnetic energy having a spectral brightness substantially greater than a thermal source of electromagnetic energy, and b) dividing the electromagnetic energy into a reference portion and a second portion. The method also includes the steps of c) receiving the reference portion of the electromagnetic energy and producing a reference signal m response thereto, d) transmitting the second portion of the electromagnetic energy to the optical coatmg layer, e) receiving the second portion of the electromagnetic energy after the second portion of the electromagnetic energy has been affected by the optical coating layer and producing a received
energy signal m response thereto, and f) processing the received energy signal ana producing a detector signal m response thereto.
The method further includes the steps of g receι/±ng tne reference signal and a first gam control
and producing a first output signal m response thereto, hi receiving the detector signal and a second gam control signal and producing a second output signal response thereto. The method also includes the steps of I) receiving the first ana second output signals and producing a comparison signal representing their d_fference, j ) receiving the comparison signal a^d producing the first and second ga control signals and a transmission moritormα signal in response thereto, the electronic circuit operating to drive the comparison signal towarα zero oy controlling the first and second gam control signals, and generating the transmission monitoring signal by analyzing the changes the first and second gam control signals needed to drive the comparison signal toward zero, and k) receiving the transmission monitoring signal, a deposition status information signal, and process design information and producing a process control signal m response thereto.
The method further includes the step of 1) depositing the optical coatmg layer on the medium response to the process control signal, and producing the deposition status information signal, whereby the first and second ga control signals are indicative of the thickness of the optical coatmg layer on the medium, so that deposition of the optical coatmg layer ceases when the optical coatmg layer has the predetermined thickness. According to a still further aspect, the invention is an apparatus for depositing an optical coatmg on a medium, the optical coat g having a predetermined thickness. The apparatus includes means for producing electromagnetic energy having a spectral brightness substantially greater than a thermal source
of electromagnetic energy and means for dividing the electromagnetic energy into a reference portion and a second portion. The apparatus also includes means for receiving the reference portion of the electromagnetic energy and for ^ producing a reference signal m response thereto, means for transmitting tne seconα portion of the electromagnetic energy to the optical coating, means for receiving the second portion of the electromagnetic energy after the second portion of the electromagnetic energy has been affected by the optical coatmg
1" and for producing a receiveα energy signal m response thereto, means for processing the received energy signal and for producing a detector signal m response thereto. In addition, the apparatus includes means for receivmα the reference s_gnaι and a first ga control signal and for producing a first output ι signal m response thereto, means for receiving the received energy signal and a second gam control signal and for producing a second output signal m response thereto and means for receiving the reference and detector signals and for producing a comparison signal representing their difference.
20 The apparatus also includes means for receiving the comparison signal and for producing the first and second gam control signals and a transmission monitoring signal in response thereto, means for driving the comparison signal toward zero by controlling the first and second gam control signals, and means
25 for generating the transmission monitoring signal by analyzing the changes m the first and second gam control signals needed to drive the comparison signal toward zero.
Detailed Description of the Preferred Embodiment of the 30 Invention
Figure 1 is a block diagram of the preferred embodiment of the invention. The apparatus 10 monitors the optical thickness of an optical coatmg being applied to a part 12 under test. The
apparatus 10 includes a laser 14, an acousto-optic modulator 16, reference photodetector 18, and an optical receiver 2C. Tne apparatus 10 also includes a gam-programmable nulling preamplifier 22, a phase-sensitive detector 24, and a computer 26. The laser 14, which is preferably a tunable single-frequency laser (such as a model 6328P external-cavity tunable αiode laser produced by New Focus), transmits a beam of light 30 to the acousto-optic modulator 16. The laser 14 can be any source of electromagnetic energy having spectral brightness substantially greater thar a thermal source of electromagnetic enerσ , (for example, an amplified spontaneous emission source, such as a model IQ-2300 from EXFO, Inc., with suitable filtering). The acousto-optic modulator 16 (for example, an IntraActicn model FCM401E5CA fiber-pigtailed acousto-optic modulator) modulates the beam of light 30 in accordance with a signal that it receives at a signal port 32. The acousto-optic modulator 16 produces a modulated beam of light 34 which is transmitted to an optical power divider 35. Tnose skilled m the arts would know that the modulated beam of light 34 might also be obtained directly from the laser 14 by modulating the laser' s αrive current to vary the laser' s output power or by some other form of direct modulation. In principle, those skilled in the arts would know that the modulator 16 could be electro-optic, mechanical, or liquid crystal. The optical power diviαer 35, which can be an MP Opticon model WA15080102CP0FC fiber power splitter, then transmits a reference portion of the modulated beam of light 34 to the reference photodetector 18 over a conduit 37 and a second portion of the modulated beam of light 34 over a conduit 41 (sucn as an optical fiber) to an optical transmitter 36. The optical transmitter 36 transmits a beam of light 38 (which can represent approximately 92 percent of the output power of the optical power divider 35) through the part 12, producing a beam of light 39. The beam of light 39 is
received by an optical receiver 40 which produces a received energy signal m response to the beam of light 39. The received energy signal is transmitted to the optical rece.^er 20 over a _me 42. Tne optical receiver 20 is preferably a photodiode ana the line 42 is preferably an optical conduit sucn as an optical fioer. The reference photodetector 18 and the optical receiver 20 produce reference and detector signals respectively m resoonse to the reference portion of the modulated beam of light 34 and m response to the received energy signal produced by the optical receiver 40. Optionally, the optical transmitter 36 can reflect the beam of light 38 from the part 12, producing the beam of light 39. The beam of light 39 can then be received b^ tr= optical receiver 40 to produce the detector signal.
The gain-programmable nulling preamplifier 22 receives the reference and detector signals respectively produced by the reference photodetector 18 and the optical receiver 20 over the respective lines 44 and 46. A first oscillator 47 produces an AM modulating signal. The AM modulating signal is transmitted over the line 48 to the signal port 32 on the acousto-optic modulator 16, where it impresses AM modulation on beam 34. The AM modulating signal is also transmitted over the line 50 to the phase-sensitive detector 24, which may be a Stanford Research Systems model 510 lock-m amplifier. The gam-programmable nulling preamplifier 22 also produces a response signal which is transmitted to the phase-sensitive detector 24 over the line 52. In response to the AM modulating signal and the response signal, the phase-sensitive detector 24 produces a comparison signal which is transmitted to the computer 26 over the line 54. Deposition status information and process design information is transmitted to the computer 26, as will be described supsequently . The computer 26 processes the output signal and produces a gam control signal m response. The gam control signal is transmitted to the gam-programmable nulling
preamplifier 22 over the line 56. The computer 26 also processes the output signal, the deposition status information and tne process design information, and produces both a transmission monitor siσnai and a process control signal m response.
A second oscillator 57 also produces an FM modulating signal which is sent to the tunable smgle-freα^ency laser 14 over the line 58 to control the frequency of the light produced by the tunable single-frequency laser 14.
Figure 2 is a block diagram of a portion of the preferred embodiment of the invention, showing further details of the gam-programmable nulling preamplifier 22. The σam-programmable nulling preamplifier 22 includes signal and reference preamplifiers 80 and 82, respectively, a α_ffere^tιal amplifier 84, ana a computer terface 86. Tne signai and reference preamplifiers 80 and 82 are low noise gam-programmable transimpedance preamplifiers. The transimpedance gam of the preamplifier 80 can be adjusted accord with the adjustment of a resistance within a range of 0 to 10.24 Gohms, and the ga of the preamplifier 82 can be adjusted in accord with the adjustment of a resistance within a range of 0 to 40.96 Mohms. Figure 2 also shows the reference photodetector 18, the optical receiver 20, the phase-sensitive detector 24 ana the computer 26. The reference photodetector 18 receives part of the modulated beam of light 34 from the conduit 37, and, on the conduit 42, optical receiver 20 receives the signal produced by the optical receiver 40 m response to the beam of light 39. The reference photodetector 18 transmits the signal it produces over line 44 to the reference preamplifier 82. The optical receiver 20 transmits the signal it produces to the signal preamplifier 80 over the line 46. In the present embodiment, the gam- programmable nulling preamplifier 22 and the differential amplifier 84 collectively constitute a comparator. The differential amplifier 84 receives an output signal produced by
the siqnal preamplifier 80 on its positive terminal and receives an output signal produced by the reference preamplifier 82 on its negative terminal. The differential amplifier 84 produces an output signal, which is transmitted to the phase-sensitive detector 24 over the line 52.
The signal produced by the phase-sensitive αetector 2^ is transmitted to the computer 26 over the line 54, and the ga control signal produced by the computer 26 is transmitted to the computer interface 86 over the line 56. In response, the computer interface 86 produces first and second gam control signals which are transmitted to the preamplifiers 80 and 82 over the respective lines 90 and 92.
The tunable single-frequency laser 14 preferably operates m the wavelength range of 1525 to 1630 nanometers and the FM dither signal on the line 58 causes the wavelength of the light produced by the tunable single-frequency laser 14 to vary approximately 0.05 nm peak-to-peak, although the amount of dither depends upon the part 12 or other operational aspects of the apparatus 10. The specific wavelength of the light proαuced by the tunable single-frequency laser 14 is chosen according to the design of the coatmg being deposited on the part 12. Conventional photodiode bias circuits 94 and 96 are used with the reference photodetector 18 and the optical receiver 20, respectively. The dual-beam laser spectrometer apparatus described, and its method of operation, both provide variable nulling which can reduce the adverse effects of changes in the intensity of tne tunable single-frequency laser 14 and allows high-precision measurements of optical transmission through thin film coatings by means of the use of a precision tracking gam-programmaole amplifier .
Also, the optical frequency modulation reduces errors induced by parasitic optical interference within the measurement
system. The apparent magnitude of the signal that is transmitted through (or reflected from) a layer will vary slightly with the frequency of the light source because of parasitic interference within the apparatus and the device being tested. If this effect is not compensated, slow drifts m the frequency of the light source will produce apparent drifts m the value of the observed transmission monitor signal. The variation of apparent transmission with the instantaneous frequency of the light source is a periodic, or multiperiodic, function. The characteristic period of the function is related to the geometric characteristics of the various sources of interference, especially the part under test.
The optimum value of the FM-modulation amplitude is the one that causes the frequency excursion of the light source to just cover one period of this parasitic interferometer transmission function. The practical performance of the coatmg monitor system can be significantly enhanced by optimizing the FM- modulation amplitude to correspond to one period of the dominant periodic function. This adjustment can be accomplished either with a manual optimization process, or automatically with a low- frequency servo loop that quantifies the short-term noise of the measured signal (which results substantially from the interaction of light source frequency with the parasitic interferometer behavior), and adjusts the FM-modulation extent to minimize that noise.
While the foregoing is a detailed description of the preferred embodiment of the invention, there are many alternative embodiments of the invention that would occur to those skilled in the art and which are within the scope of the present invention. Accordingly, the present invention is to be determined by the following claims.