WO2009091393A3 - Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials - Google Patents

Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials Download PDF

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Publication number
WO2009091393A3
WO2009091393A3 PCT/US2008/051057 US2008051057W WO2009091393A3 WO 2009091393 A3 WO2009091393 A3 WO 2009091393A3 US 2008051057 W US2008051057 W US 2008051057W WO 2009091393 A3 WO2009091393 A3 WO 2009091393A3
Authority
WO
WIPO (PCT)
Prior art keywords
vessels
materials
vessel
base
multiautoclave
Prior art date
Application number
PCT/US2008/051057
Other languages
French (fr)
Other versions
WO2009091393A2 (en
Inventor
Brent J. Anderson
Ralph D. Gillespie
Maureen L. Bricker
Original Assignee
Uop Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Uop Llc filed Critical Uop Llc
Priority to CA2705605A priority Critical patent/CA2705605A1/en
Priority to MX2010005882A priority patent/MX2010005882A/en
Priority to PCT/US2008/051057 priority patent/WO2009091393A2/en
Publication of WO2009091393A2 publication Critical patent/WO2009091393A2/en
Publication of WO2009091393A3 publication Critical patent/WO2009091393A3/en

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00281—Individual reactor vessels
    • B01J2219/00283—Reactor vessels with top opening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00306—Reactor vessels in a multiple arrangement
    • B01J2219/00308—Reactor vessels in a multiple arrangement interchangeably mounted in racks or blocks
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00331—Details of the reactor vessels
    • B01J2219/00333—Closures attached to the reactor vessels
    • B01J2219/00344—Caps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B01J2219/00364—Pipettes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00477—Means for pressurising the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00479—Means for mixing reactants or products in the reaction vessels
    • B01J2219/00481—Means for mixing reactants or products in the reaction vessels by the use of moving stirrers within the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00479—Means for mixing reactants or products in the reaction vessels
    • B01J2219/00484—Means for mixing reactants or products in the reaction vessels by shaking, vibrating or oscillating of the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00495—Means for heating or cooling the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/00747—Catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • B01J2219/0075—Metal based compounds
    • B01J2219/00754—Metal oxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00756—Compositions, e.g. coatings, crystals, formulations

Abstract

A vessel arrangement having a base (22) and multiple vessels (28) suited for simultaneously conducting a plurality of isolated experimental reactions or treatments at atmospheric process conditions or elevated temperatures and pressure condition has been developed. A component of a first material is introduced into one independent vessel (28) through an opening in its top of the first vessel and another component of a second material is introduced into a different independent vessel through its top. Both vessels (28) are removably located about a base (22) at different first locations. Transformation of the components in the vessels occurs to produce different materials therein. After completion of the experiments a displacement medium (44) simultaneously urges the vessels (28) from their respective locations about the base (22). Typically at least one property of the materials from the vessels is determined either within the vessel or after recovery of the materials.
PCT/US2008/051057 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials WO2009091393A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CA2705605A CA2705605A1 (en) 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials
MX2010005882A MX2010005882A (en) 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials.
PCT/US2008/051057 WO2009091393A2 (en) 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US2008/051057 WO2009091393A2 (en) 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials

Publications (2)

Publication Number Publication Date
WO2009091393A2 WO2009091393A2 (en) 2009-07-23
WO2009091393A3 true WO2009091393A3 (en) 2009-12-30

Family

ID=40885842

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2008/051057 WO2009091393A2 (en) 2008-01-15 2008-01-15 Multiautoclave with set of vessels for combinatorial synthesis of zeolites and other materials

Country Status (3)

Country Link
CA (1) CA2705605A1 (en)
MX (1) MX2010005882A (en)
WO (1) WO2009091393A2 (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4068798A (en) * 1976-09-29 1978-01-17 E. I. Du Pont De Nemours And Company Method and apparatus for stopper removal
US4944923A (en) * 1986-06-18 1990-07-31 Wolfgang Schultz Autoclave for the pressure digestion of sample materials in analytical chemistry
US5785927A (en) * 1996-10-24 1998-07-28 Eli Lilly And Company Vessel handling system useful for combinatorial chemistry
US20030054384A1 (en) * 2000-01-11 2003-03-20 Maxygen, Inc. Integrated systems and methods for diversity generation and screening
US6602714B1 (en) * 1999-11-09 2003-08-05 Sri International Viscosity and mass sensor for the high-throughput synthesis, screening and characterization of combinatorial libraries
US6794052B2 (en) * 1994-10-18 2004-09-21 The Regents Of The University Of California Polymer arrays from the combinatorial synthesis of novel materials
US6817558B1 (en) * 2002-04-23 2004-11-16 Uop Llc Parallel sizing, dosing and transfer assembly and method of use
US6821486B1 (en) * 1997-02-20 2004-11-23 Sinvent As Multiautoclave for combinatorial synthesis of zeolites and other materials

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4068798A (en) * 1976-09-29 1978-01-17 E. I. Du Pont De Nemours And Company Method and apparatus for stopper removal
US4944923A (en) * 1986-06-18 1990-07-31 Wolfgang Schultz Autoclave for the pressure digestion of sample materials in analytical chemistry
US6794052B2 (en) * 1994-10-18 2004-09-21 The Regents Of The University Of California Polymer arrays from the combinatorial synthesis of novel materials
US5785927A (en) * 1996-10-24 1998-07-28 Eli Lilly And Company Vessel handling system useful for combinatorial chemistry
US6821486B1 (en) * 1997-02-20 2004-11-23 Sinvent As Multiautoclave for combinatorial synthesis of zeolites and other materials
US6602714B1 (en) * 1999-11-09 2003-08-05 Sri International Viscosity and mass sensor for the high-throughput synthesis, screening and characterization of combinatorial libraries
US20030054384A1 (en) * 2000-01-11 2003-03-20 Maxygen, Inc. Integrated systems and methods for diversity generation and screening
US6817558B1 (en) * 2002-04-23 2004-11-16 Uop Llc Parallel sizing, dosing and transfer assembly and method of use

Also Published As

Publication number Publication date
WO2009091393A2 (en) 2009-07-23
MX2010005882A (en) 2010-12-02
CA2705605A1 (en) 2009-07-23

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