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United States Patent

Nyssen et al.

[19]

US005810266A [ii] Patent Number: [45] Date of Patent:

5,810,266 Sep. 22, 1998

[54] PROCESS AND AN APPARATUS FOR

PRODUCING FINELY DIVIDED SOLIDS
DISPERSIONS

[75] Inventors: Peter Roger Nyssen, Dormagen;

Klaus-Wilfried Wanken, Leverkusen;
Bernd Klinksiek, Gladbach, all ol
Germany

[73] Assignee: Bayer Aktiengesellschaft, Leverkusen, Germany

[21] Appl. No.: 710,991

[22] Filed: Sep. 25, 1996

[30] Foreign Application Priority Data

Oct. 2, 1995 [DE] Germany 195 36 845.2

[51] Int. CI. B02C 19/06

[52] U.S. CI 241/5; 241/16; 241/21;

241/39; 241/152.1

[58] Field of Search 241/1, 5, 16, 21,

241/39, 152.1, 171

[56] References Cited

U.S. PATENT DOCUMENTS

4,081,863 3/1978 Rees 336/176

4,186,772 2/1980 Handleman 241/5 X

4,592,302 6/1986 Motoyama et al 241/39 X

4,784,333 11/1988 Hikake et al 241/5

4,811,907 3/1989 Niemi et al 241/5

4,860,959 8/1989 Handleman 241/5 X

4,917,309 4/1990 Zander et al 241/16 X

5,111,998 5/1992 Kanda et al 241/39 X

5,129,586 7/1992 Artemjev et al 241/5

5,421,524 6/1995 Haddow 241/5

5,577,670 11/1996 Omata et al 241/5

5,628,464 5/1997 Smith et al 241/5

FOREIGN PATENT DOCUMENTS

2633288 2/1977 Germany .
2063695 6/1981 United Kingdom .
87/06854 11/1987 WIPO 241/5

Primary Examiner—-John M. Husar

Attorney, Agent, or Firm—Sprung Kramer Schaefer & Briscoe

[57] ABSTRACT

This invention relates to a process for producing finely divided dispersions of solids having an average particle size of 0.01 to 20 fim by the comminution of coarse particulate dispersions in a hole- or slit-type nozzle 4 having a specific bore length to diameter ratio at a pressure difference greater than 5 bar between the nozzle inlet and the nozzle outlet. The invention also relates to an apparatus for producing the finely divided dispersion.

11 Claims, 4 Drawing Sheets

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